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Purpose: Alumina-zirconia ceramics with nano 12 mol% CeO2 stabilized ZrO2 were presented as new ceramics with improvement fracture behavior: better crack growth resistance and limited susceptibility to slow crack growth. This ceramics exhibits good cutting properties. Design/methodology/approach: The controlled crack growth of specimens with double notch was carried with using Zwick testing machine. The specimens with double notch were loaded with rate of 1micrometre min to the -1. The loading of the specimens has been broken at the moment of crack propagation. The procedure has been repeated many times up to obtaining definite increase of crack length. In situ observation of crack growth from notch up to failure was possible due to special device with microscopical objective heads in vertical configuration coupled with CCD camera fitted to Zwick 1446 testing machine. A load-relaxation technique method was used for determination a relationship of a crack growth velocity (v) versus stress intensity factor (KI) and calculation the parameters of SCG. Findings: Many newly developed ceramics that are designed for high-temperature applications or electronic devices possess a low crack growth resistance. It is a drawback in widely usage of these materials in industry. Application of the ZrO2nano stabilized with 12 mol% CeO2 in alumina-zirconia ceramics improves the fracture toughness and decreases the susceptibility to slow crack growth in comparison to pure alumina ceramics. Observation of the controlled crack growth in the tested ceramics reveals the existence of increasing R-curve in the alumina-zirconia ceramics with nano ceria stabilized zirconia. Practical implications: Due to improvement of fracture behavior of the alumina-zirconia ceramics with nano12 mol% CeO2 stabilized ZrO2 could be used in "dry cutting" machining. Originality/value: A combination of in situ microscopic long-through thickness crack growth observation during three point bending (3PB) of a single edge notched beam (SENB) enabled measurement of the R-curve. In presented work a new load relaxation method was worked out for determination susceptibility tested ceramics to slow crack growth.
Wydawca
Rocznik
Tom
Strony
41--44
Opis fizyczny
Bibligr. 12 poz., rys., tab.
Twórcy
autor
autor
- Materials Engineering Department, Institute of Advanced Manufacturing Technology, ul. Wrocławska 37 a, 30-011 Kraków, Poland, magdalena.szutkowska@ios.krakow.pl
Bibliografia
- [1] M. Szutkowska, Modified indentation methods for fracture toughness determination of alumina ceramics, 13th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME'2005, Gliwice-Wisła, 2005, 651-654.
- [2] B.F. Sorensen, A. Horsewell, O. Jorgensen, A.N. Kumar, Fracture resistance measurement method for in situ observation of crack mechanisms, Journal of American Ceramic Society 81/3 (1998) 661-669.
- [3] J.J. Alcala, M. Anglada, Fatigue and static crack propagation in yttria-stabilized tetragonal zirconia polycrystals: Crac-growth micro mechanisms and precracking effects, Journal of American Ceramic Society 80/11 (1997) 2759-2772.
- [4] M. Szutkowska, M. Boniecki, M. Bucko, R-curve behaviour of alumina matrix ceramics with long cracks, Proceedings of 11th International Ceramics Congress CIMTEC'2006, Sicily, Italy, 2006, 1652-1657.
- [5] L.A. Dobrzański, Fundamentals of Materials Science ar. Physical Metallurgy. Engineering Materials with Fundamentals of Materials Design, WNT, Warszawa, 2002 (in Polish).
- [6] M.Szutkowska, Fracture resistance behavior of alumina-zirconia composites, Journal of Materials Processing Technology 153-154 (2004) 868-874.
- [7] D. Munz, T. Fett, Ceramics. Mechanical properties, failure behaviour, materials selection. 1st ed. Berlin: Springer 1999.
- [8] Z. Librant, M. Boniecki, A. Gładki, and al. Properties of ceramics derived from direct observations of crack, Bulletin of the Polish Academy of Sciences, 4/47 (1999) 365-377.
- [9] T. Fett, An analysis of the three-point bending bar by use of the weight function method. Engineer Fracture Mechanics 3 (1991) 683-686.
- [10] T. Fett, D. Munz, Subcritical crack growth of macrocracks in alumina with R-curve behaviour, Journal of American Ceramic Society 75 (1992) 958-963.
- [11] M. Boniecki, Z. Librant, H. Tomaszewski, W. Recko, Fracture work of alumina and zirconia ceramics and alumina-zirconia composites. Electronic Materials 2/26 (1998) 5-17 (in Polish).
- [12] M. Szutkowska, M. Boniecki, Subcritical crack growth in zirconia-toughned alumina (ZTA) ceramics, Materials Processing Technology 175 (2006) 416-420.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BOS3-0017-0013