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Effect of curing temperature on flexural properties of silica-based geopolymer-carbon reinforced composite

Wybrane pełne teksty z tego czasopisma
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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: The aim of this paper is to find out the curing temperature at which we can achieve the best mechanical properties and adhesion between silica-based geopolymer matrix (Q1) and carbon HTS 5631 1600tex 24K fibre. Design/methodology/approach: The carbon fibre was impregnated with silica-based geopolymer by means of home-made “impregnation machine”. This equipment was designed based on simulating the real pultrusion or filament winding technique. Composite samples were made manually in silicon mould and cured under hot vacuum bagging technique at different temperatures. Flexural properties were determined under three-point bending mode in accordance with British Standard BS EN ISO 14125:1998. The sections perpendicular to fibres and surfaces of the composites were analysed by means of scanning electron microscope (SEM) to estimate the adhesion between geopolymer matrices and fibre reinforcement. Findings: Relatively wide range of curing temperature from 70oC to 100oC at which we can obtain high flexural properties, maximal values of flexural strength 570 MPa, flexural modulus 65 GPa and relative deformation of composite was 0.98% when the composite was cured and dried at 75oC. Adhesion of the geopolymer matrix to carbon fibre was very good and hardly to determine the differences by SEM image observation within the range of optimal curing temperature. Research limitations/implications: The curing time was too long to provide the geopolymerization process before it had been completed, this factor caused that it should be carried out in the future and we may use liquid absorption to determine how many cavities are in the composites. Practical implications: The research presents original information on the influence of different curing temperatures on mechanical properties and micro-structure of silica-based geopolymer matrix – carbon composite. The results are useful for further investigations. Originality/value: Determining the optimal curing temperature and micro-structure of silica-based geopolymer system to make it easy to find the curing time and other conditions to get the best properties of this type of materials.
Rocznik
Strony
492--497
Opis fizyczny
Bibliogr. 22 poz., rys., tabl.
Twórcy
autor
autor
autor
autor
  • Department of Material Science, Faculty of Mechanical Engineering, Technical University of Liberec, Studentská 2, 461 17 Liberec, Czech Republic, hung.tulcz@yahoo.com
Bibliografia
  • [1] J. Davidovits, Geopolymer Chemistry & Applications. Second Edition, Institute Géopolymèr - France, 2008.
  • [2] J. Davidovits, 30 Years of Successes and Failures in Geopolymer Applications - Market trends and Potential breakthroughs, Proceeding of Geopolymer 2002 Conference, Australia, 2002, 1-16.
  • [3] J. Davidovits, Geopolymer chemistry and sustainable Development - The Poly(sialate) terminology : a very useful and simple model for the promotion and understanding of green-chemistry. Proceeding of Geopolymer 2005th World Congress. Geopolymer Institute, France, 2006, 9-16.
  • [4] L. M. Sheppar, Geopolymer Composites: A Ceramics Alternative to Polymer Matrices, Proceedings of the 105th Annual Meeting and Exposition of the American Ceramic Society, 2007.
  • [5] R. E. Lyon, P. N. Balaguru, A. Foden, U. Sorathia, J. Davidovits, M. Davidovics, Fire-resistant aluminosilicate composites, Journal of Fire and Materials 21(1997) 67-73.
  • [6] P. Duxson, A. Fernández-Jiménez, J. Provis, G. Lukey, A. Palomo, J. van Deventer, Geopolymer technology: the current state of the art, Journal of Materials Science, 42 (2007) 2917-2933.
  • [7] C. G. Papakonstantinou, P. Balaguru, R. E. Lyon, Comparative study of high temperature composites, Journal of Composites Part B: Engineering, 32 (2001) 637-649.
  • [8] C. G. Papakonstantinou, P. N. Balaguru, Use of geopolymer matrix for high temperature resistant hybrid laminates and sandwich panels, Proceeding of Geopolymer 2005th World Congress, Geopolymer Institute, France, 2006, 201-207.
  • [9] D. Khale, R. Chaudhary, Mechanism of geopolymerization and factors influencing its development: a review, Journal of Materials Science, 42 (2007) 729-746.
  • [10] W. Hufenbach, M. Gude, A. Czulak, J. Śleziona, A. Dolata- Grosz, M. Dyzia, Development of textile-reinforced carbon fibre aluminium composites manufactured with gas pressure infiltration methods, Journal of Achievements in Materials and Manufacturing Engineering 35/2 (2009) 177-183.
  • [11] M. Anurag, C. Deepika, J. Namrata, K.Manish, S. Nidhi, D. Durga, Effect of concentration of alkaline liquid and curing time on strength and water absorption of geopolymer concrete. ARPN Journal of Engineering and Applied Sciences, 3 (2008) 14-18.
  • [12] H. Xu, J. S. J. van Deventer, Effect of Source Materials on Geopolymerization, Journal of Industrial & Engineering Chemistry Research, 42 (2003) 1698-1706.
  • [13] J. J. Brooks, Prediction of setting time of fly ash concrete, ACI Materials Journal 99 (2002) 591-597.
  • [14] H. Djwantoro, B. V. Rangan, Development and properties of low-calcium fly ash-based geopolymer concrete, Geopolymer Institute, France, 2006.
  • [15] J. C. Swanepoel, C. A. Strydom, Utilisation of fly ash in a geopolymeric material, Journal of Applied Geochemistry, 17 (2002) 1143-1148.
  • [16] A. Palomo, M. W. Grutzeck, M. T. Blanco, Alkali-activated fly ashes: A cement for the future, Journal of Cement and Concrete Research, 29 (1999) 1323-1329.
  • [17] J. S. Sindhunata, J .S. J van Deventer, G. C. Lukey, H. Xu, Effect of Curing Temperature and Silicate Concentration on Fly Ash-Based Geopolymerization, Industrial & Engineering Chemistry Research, 45 (2006) 3559-3568.
  • [18] K. Wang, S. P. Shah, A. Mishulovich, Effects of curing temperature and NaOH addition on hydration and strength development of clinker-free CKD-fly ash binders, Journal of Cement and Concrete Research, 34 (2004) 299-309.
  • [19] A. Palomo, S. Alonso, A. Fernandez-Jimenez, I. Sobrados, J. Sanz, Alkaline activation of fly ashes: NMR study of the reaction products, Journal of the American Ceramic Society 87 (2004) 1141-1145.
  • [20] D. H. Tran, D. Kroisova, O. Bortnovsky, P. Louda, D. Penica, Effect of curing condition on mechanical properties of fibres and composites based on geopolymer matrices, Proceeding of International Student Conference of Material Science, Liberec - Czech Republic, 2008.
  • [21] British Standard, Fiber-reinforced plastic composites - Determination of flexural properties, 2003.
  • [22] J. Hammell, P. Balaguru, R. Lyon, J. Davidovits, Influence of reinforcement types on the flexural properties of geopolymer composites, Proceeding of Geopolymer Conference, 1999, 155-164.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BOS2-0021-0050
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