PL EN


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
Tytuł artykułu

Ion beam assisted deposition of Ti–Si–C thin films

Wybrane pełne teksty z tego czasopisma
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: Deposition of hard thin multilayer coatings is a common practice in improving the performance of tools for many different applications. From this aspect Ti3SiC2, due to its lamellar structure and unique combination of properties is a potential interlayer material candidate for thermo-mechanical application. Design/methodology/approach: Multiphase Ti–Si–C thin films were deposited by the ion beam assisted deposition (IBAD) technique from a single Ti3SiC2 compound target on an AISI 316L steel substrate. To optimize the deposition process, Monte Carlo simulations were performed; the range of the deposition parameters was determined and then experimentally verified. Scanning and transmission electron microscopies were used to examine the microstructure and quality of the deposited films. Mechanical properties were determined by nanoindentation tests. Findings: The deposited film was flat, smooth and dense with small crystalline particles. The hardness HIT of coated substrates was in the range 2.7 to 5.3 GPa. The average calculated value reduced elastic modulus EIT for coated substrates was 160 GPa. The hardness and reduced elastic modulus for uncoated substrates were HIT = 4.4 GPa and EIT = 250 GPa, respectively. Practical implications: PVD techniques enable low substrate temperature deposition, preferred due to the thermal limitations of the metallic substrates commonly used in industrial applications. The aim of this work is low temperature deposition of Ti-Si-C film, from a single Ti3SiC2 compound target, on 316L steel substrate, using the IBAD technique, known for excellent film connection to the substrate. Originality/value: Ion beam assisted deposition parameters were calculated and experimentally verified.
Rocznik
Strony
87--90
Opis fizyczny
Bibliogr. 15 poz., rys., tabl.
Twórcy
autor
autor
  • Institute of Technology, Pedagogical University, ul. Podchorążych 2, 30-084 Kraków, Poland, atwardow@ap.krakow.pl
Bibliografia
  • [1] M. W. Barsoum, T. El-Raghy, C. J. Rawn, W. D. Porter, H. Wang, E. A. Payzant, C. R. Hubbard, Thermal properties of Ti3SiC2, Journal of Physics and Chemistry of Solids 60/4 (1999) 429-439.
  • [2] M. W. Barsoum, The MN+1AXN Phases: A New Class of Solids, Thermodynamically Stable Nanolaminates, Progress in Solid State Chemistry 28 (2000) 201.
  • [3] L. Jaworska, L. Stobierski, A. Twardowska, D. Królicka, Preparation of materials based on Ti-Si-C system using high temperature-high pressure method, Journal of Materials Processing Technology 162-163 (2005) 184-189.
  • [4] P. Eklund, T. Joelsson, H. Ljungcrantz, O. Wilhelmsson, Zs. Czigány, H. Högberg, L. Hultman, Microstructure and electrical properties of Ti-Si-C-Ag nano-composite thin films, Surface and Coatings Technology 201 (2007) 6465-6469.
  • [5] T. Zehnder, J. Matthey, P. Schwaller, A. Klein, P. A. Steinmann, J. Patscheider, Wear protective coatings consisting of TiC–SiC–a-C:H deposited by magnetron sputtering, Surface and Coating Technology 163-164 (2003) 238.
  • [6] A. R. Phani, J. E. Krzanowski, Structure and mechanical properties of Ti-Si-C coatings deposited by magnetron sputtering, Journal of Vacuum Science and Technology A 19 (2001) 2252.
  • [7] J. J. Hu, J. E. Bultman, S. Patton, J. S. Zabinski, Pulsed Laser Deposition and Properties of Mn+1AXn Phase Formulated Ti3SiC2, Thin Films, Tribology Letters 16 (2004) 113.
  • [8] W. Gulbinski, T. Suszko, A. Gilewicz, B. Warcholinski, Z. Kuklinski, Structure and high-temperature tribological behaviour of Ti-Si-C nanocomposite thin films, Surface and Coatings Technology 200 (2006) 4179-4184.
  • [9] J. Alami, P. Eklund, J. Emmerlich, O. Wilhelmsson, U. Jansson, H. Hogberg, L. Hultman, U. Helmersson, High-power impulse magnetron sputtering of Ti-Si-C thin films from a Ti3SiC2 compound target, Thin Solid Films 515 (2006) 1731-1736.
  • [10] P. H. Mayrhofer, C. Mitterer, L. Hultman, H. Clemens, Microstructural design of hard coatings, Progress in Materials Science 51 (2006) 1032–1114.
  • [11] J. F. Ziegler: www.srim.org
  • [12] B. Rajchel, M. Drwięga, E. Lipińska, M. Wierba, Adaptation of the 70 kV INP ion implanter to the IBAD technique, Nuclear Instruments and Methods in Physics Research B89 (1994) 342-345.
  • [13] T. Y. Huang, C. C Chen, Synthesis of nanolaminated Ti3SiC2 from Ti-Ti5Si3 and CNTs, Materials Science and Engineering A 466 (2007) 148-155.
  • [14] T. El-Raghy, N.W. Barsoum, A. Zavaliangos, S. Kalidindi, Processing and mechanical properties of Ti3SiC2 II. Effect o grain size and deformation temperature, Journal of American Ceramic Society 82 (1999) 2855.
  • [15] R. Pampuch, J. Lis, L. Sobierski, M. Tymkiewicz, Solid combustion synthesis of Ti3SiC2, Journal European Ceramic Society 5 (1989) 283.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BOS2-0021-0012
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.