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Characteristic of vacuum sintered stainless steels

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: In the present study duplex stainless steels were sintered in vacuum. using rapid cooling form the mixture of prealloyed and alloying element powders The purpose of this paper was to describe the obtained microstructures after sintering as well as the main mechanical properties of sintered stainless steels. Design/methodology/approach: In presented work duplex stainless steels were obtained through powder metallurgy starting from austenitic 316L or ferritic 410L prealloyed stainless steels powders by controlled addition of alloying elements powder. Prepared mixes were sintered in a vacuum furnace in 1250°C for 1h. After sintering rapid cooling (6°C/s) using nitrogen under pressure was applied. Sintered compositions were subjected to structural examinations by scanning and optical microscopy and EDS analysis as well as X-ray analysis. Mechanical properties were studied through tensile tests and Charpy impact test. Findings: It was demonstrated that austenitic-ferritic microstructures with regular arrangement of both phases and absence of precipitates can be obtained with properly designed powder mix composition as well as sintering cycle with rapid cooling rate. Obtained sintered duplex stainless steels shows good mechanical properties which depends on phases ratio in the microstructure and elements partitioning (Cr/Ni) between phases. Research limitations/implications: Basing on alloys characteristics applied cooling rate and powder mix composition seems to be a good compromise to obtain balanced sintered duplex stainless steel microstructures. Practical implications: Mechanical properties of obtained sintered duplex stainless steels structures are rather promising, especially with the aim of extending their field of possible applications. Originality/value: The utilization of vacuum sintering process with rapid cooling after sintering combined with use of elemental powders added to a stainless steel base powder shows its advantages in terms of good microstructural homogeneity.
Rocznik
Strony
126--134
Opis fizyczny
Bibliogr. 20 poz., rys., tabl.
Twórcy
autor
autor
  • Division of Materials Processing Technology, Management and Computer Techniques in Materials Science, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland, zbigniew.brytan@polsl.pl
Bibliografia
  • [1] P. K. Samal, J. B. Terrell, Mechanical properties improvement of PM 400 series stainless steels via nickel addition, Metal Powder Report December 2001 (2001) 28-34.
  • [2] A. J. Rawlings, H. M. Kopech, H. G. Rutz, The effect of service temperature on the properties of ferritic P/M stainless steels, Proceedings of the International Conference “Powder Metallurgy & Particulate Materials” PM2TEC’97, Chicago, USA, 1997.
  • [3] M. Rosso, M. Actis Grande, D. Ornato, Sintering of duplex stainless steels and their properties, Powder Metallurgy Progress 2 (2002) 10-17.
  • [4] F. Velasco, A. Bautista, A. González-Centeno, High-temperature oxidation and aqueous corrosion performance of ferritic, vacuum-sintered stainless steels prealloyed with Si, Corrosion Science 51 (2009) 21-27.
  • [5] C. Garcia, F. Martin, P. de Tiedra, Y. Blanco, J.M. Ruiz- Roman, M. Aparicio, Electrochemical reactivation methods applied to PM austenitic stainless steels sintered in nitrogen– hydrogen atmosphere, Corrosion Science 50 (2008) 687-697.
  • [6] K. Sikorski, A. Szymańska, D. Kowalczyk, J. Kazior, K. J. Kurzydłowski, Effect of silicon addition on the microstructure and mechanical properties of 316L austenitic stainless steel, Proceedings of the European Powder Metallurgy Association, Euro PM,2005, vol. 1, 2005, 419-424.
  • [7] L. A. Dobrzański, Z. Brytan, M. Actis Grande, M. Rosso, E.J. Pallavicini, Properties of vacuum sintered Duplex Stainless Steels, Journal of Materials Processing Technology 157-158 (2004) 312-316.
  • [8] L. A. Dobrzański, Z. Brytan, M. Actis Grande, M. Rosso, Sintered Duplex Stainless Steels Corrosion Properties, Materials Science Forum 534-536 (2007) 721-724.
  • [9] M. Actis Grande, D. Ugues, L.A. Dobrzański, Z. Brytan, M. Rosso, Properties of vacuum sintered duplex stainless steels, Proceedings of the Powder Metallurgy World Congress and Exhibition, PM’2004, Vienna, 2004, vol. 3, 395-399.
  • [10] M. Campos, A. Bautista, D .Caceres, J. Abenojar, J. M. Torralba, Study of the interfaces between austenite and ferrite grains in P/M duplex stainless steels, Journal of the European Ceramic Society 23 (2003) 2813-2819.
  • [11] P. Datta, G. S. Upadhyaya, Sintered duplex stainless steels from premixes of 316L and 434L powders, Materials Chemistry and Physics 67 (2001) 234-242.
  • [12] J. Kazior, T. Pieczonka, A. Molinari, Properties of AISI 316L, AISI 434L and duplex stainless steel, Proceedings of the 8th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME’1999, Gliwice–Rydzyna–Rokosowo–Pawłowice, 1999, 289-293.
  • [13] M. Campos, P. Sarasola, J. M. Torralba, Sintering evolution of duplex stainless steels obtained from austenitic and ferritic stainless steels powders mixtures, Proceedings of the 9th International Scientific Conference „Achievements in Mechanical and Materials Engineering” AMME’2000, Gliwice–Sopot–Gdańsk, 2000, 83-86.
  • [14] L. A. Dobrzański, Z. Brytan, M. Actis Grande, M. Rosso, Corrosion resistance of sintered duplex stainless steel evaluated by electrochemical method, Journal of Achievements in Materials and Manufacturing Engineering 17 (2006) 317-320.
  • [15] H. Krztoń, D. Kolesnikow, J. Paducha, R. Molenda, Processing and properties of sinters prepared from 316L steel nanopowders, Journal of Achievements in Materials and Manufacturing Engineering 21/2 (2007) 73-76.
  • [16] C. Garcia, F. Martin, Y. Blanco, M.P. de Tiedra, M.L. Aparicio, Corrosion behaviour of duplex stainless steels sintered in nitrogen, Corrosion Science 51 (2009) 76-86.
  • [17] S. S. Panda, V. Singh, A. Upadhyaya, D. Agrawal, Sintering response of austenitic (316L) and ferritic (434L) stainless steel consolidated in conventional and microwave furnaces, Scripta Materialia 54 (2006) 2179-2183.
  • [18] C. J. Munez, M. V. Utrilla, A. Urena, Effect of temperature on sintered austeno-ferritic stainless steel microstructure, Journal of Alloys and Compounds 463 (2008) 552-558.
  • [19] M. Rosso, M. Actis Grande, High density sintered stainless steels with improved properties, Journal of Achievements in Materials and Manufacturing Engineering 21/2 (2007) 97-102.
  • [20] L. A. Dobrzański, Z. Brytan, M. Actis Grande, M. Rosso, Properties of duplex stainless steels made by powder metallurgy, Archives of Materials Science and Engineering 28/4 (2007) 217-223.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BOS2-0020-0020
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