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Headspace-solvent microextraction for identification of volatile components of Myrtus communis L.

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Headspace-solvent microextraction (HS-SME) and hydrodistillation coupled with GC-MS have been used for isolation and identification of the volatile components that characterize Myrtus communis L. aroma. In the HS-SME method a suspended micro-drop of n -butanol was used as solvent. The effect of six different parameters on extraction efficiency, including sample weight, drop volume, extraction temperature, conditioning time, extraction time, and ionic strength were optimized using a simplex optimization method. The volatile components were studied both by HS-SME and an ordinary hydrodistillation method and the major components identified were 1,8-cineol, #945-pinene, limonene, and linalool.
Rocznik
Strony
139--149
Opis fizyczny
Bibliogr. 16 poz., rys., tab.
Twórcy
autor
autor
  • Lorestan University Department of Chemistry, Faculty of Science Khoramabad Iran Agriculture and Natural Resource Research Center P.O. Box 348 Khoramabad Iran, payman_hashemi@yahoo.com
Bibliografia
  • [1] H. Lord and J. Pawliszyn, J. Chromatogr. A, 902 , 17–63 (2000)
  • [2] M. Riu-Aumatell, M. Castellari, E. Lopez-Tamames, S. Galassi, and S. Buxaderas, Food Chem., 87 , 627–637 (2004)
  • [3] J.F. Cavalli, X. Fernandez, L. Lizzani-Cuvelier, and A.M. Loiseau, Food Chem., 88 , 151–157 (2004)
  • [4] A. Besharati-Seidani, A. Jabbari, and Y. Yamini, Anal. Chim. Acta, 530 , 155–161 (2005)
  • [5] A.R. Fakhari, P. Salehi, R. Heydari, S. Nejad Ebrahimi, and P.R. Haddad, J. Chromatogr. A, 1098 , 14–18 (2005)
  • [6] A. Besharati-Seidani, A. Jabbari, and Y. Yamini, Anal. Chim. Acta, 530 , 155–161 (2005)
  • [7] J. Cao, M. Qi, Y. Zhang, S. Zhou, Q. Shao, and R. Fu, Anal. Chim. Acta, 561 , 88–95 (2006)
  • [8] D. Ciccarelli, A.C. Andreucci, A.M. Pagni, and F. Garbari, Flora, 200 , 326–331 (2005)
  • [9] A. Cakir, Biochem. Syst. Ecol., 32 , 809–816 (2004).
  • [10] P. Weyerstahl, H. Marscall, and A. Rustaiyan, Flavour Fragr. J., 9 , 333–337 (1994)
  • [11] G. Flamini, P.L. Cioni, I. Morelli, S. Maccioni, and R. Baldini, Food Chem., 85 , 599–604 (2004)
  • [12] M. Vanhaelen and R. Vanhaelen-Faster, Planta Med., 39 , 164–167 (1980)
  • [13] D. Yadegarinia, L. Gachkar, M.B. Rezaei, M. Taghizadeh, S. Alipoor Astaneh, and I. Rasooli, Phytochemistry, 67 , 1249–1255 (2006)
  • [14] M. Curini, A. Bianchi, F. Epifano, R. Bruni, L. Torta, and A. Zambonelli, Chem. Nat. Compd., 39 , 191–194 (2003)
  • [15] I. Rasooli, M.L. Moosavi, M.B. Rezaee, and K. Jaimand, J. Agric. Sci. Technol., 4 , 127–133 (2002)
  • [16] P. Hashemi, M.M. Abolghasemi, A.R. Fakhari, S. Nejad Ebrahimi, and S. Ahmadi, Chromatographia, 66 , 283–286 (2007).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BATE-0002-0012
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