PL EN


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
Tytuł artykułu

Optimization and validation of an HPLC-UV method for analysis of corosolic, oleanolic, and ursolic acids in plant material: Application to Prunus serotina Ehrh

Autorzy
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
A simple reversed-phase high-performance liquid chromatographic (RP-HPLC) method has been developed and validated for simultaneous analysis of three triterpene acids (corosolic, oleanolic, and ursolic acids) in extracts from inflorescences, leaves, and fruits of Prunus serotina Ehrh. (American black cherry). Separation of the acids was accomplished on a C 18 column (5 µm, 250 mm × 4.6 mm i.d.) and recorded at 210 nm. The greatest resolution was achieved with 90:10 (υ/υ) methanol-1% aqueous orthophosphoric acid as mobile phase at a flow rate of 0.6 mL min -1 . The correlation coefficients for all the calibration plots ( r > 0.998) showed linearity good over the range tested. The relative standard deviation of the method was less than 3.3% for intra and inter-day assays, and average recovery was between 95.9 and 100.9%. Sensitivity was high; detection limits were between 0.034 and 0.067 µg mL -1 . Total amounts of triterpene acids were 0.451-0.928, 0.031, and 0.911-1.455% in the inflorescences, fruits, and leaves of P. serotina , depending on the time of harvesting.
Rocznik
Strony
643--659
Opis fizyczny
Bibliogr. 43 poz., rys., tab.
Twórcy
autor
  • Medical University of Łódź Department of Pharmacognosy, Faculty of Pharmacy 1 Muszyński St 90-151 Łódź Poland, molszewska@pharm.am.lodz.pl
Bibliografia
  • [1] Rehder, Manual of Cultivated Trees and Shrubs, Hardy in North America Exclusive of Subtropical and Warmer Temperate Regions, Macmillan, New York, 1947, p. 477
  • [2] A. Ordaz-Galindo, P. Wesche-Ebeling, R.E. Wrolstad, L. Rodriguez-Saona, and A. Argaiz-Jamet, Food Chem., 65 , 201 (1999)
  • [3] J.E.F. Reynolds (Ed.) Martindale, The Extra Pharmacopoeia XXIX, The Pharmaceutical Press, London, 1989, p. 1629
  • [4] A. Osol, G.E. Farrar, K.B. Beyer, J.H. Brown, D.K. Detweiler, R. Pratt, H.W. Youngken, and H.C. Wood (Ed.) The Dispensatory of the United States of America, J.B. Lippincott, Philadelphia, Montreal, 1995, pp. 273–275
  • [5] H.W.A. Biesseles, A.C. van der Kerk-van Hoof, J.J. Kettenes-van den Bosch, and C.A. Salemnik, Phytochemistry, 13 , 203 (1974)
  • [6] F.B. Power and C.W. Moore, J. Chem. Soc., 97 , 1099 (1910)
  • [7] M. Olszewska, Acta Chromatogr., 19 , 253 (2007)
  • [8] A.M. Diaz, M.J. Abad, L. Fernandez, C. Recuero, L. Villaescusa, A. Silvan, and P. Bermejo, Biol. Pharm. Bull., 23 , 1307 (2000)
  • [9] E. Nadinic, S. Gorzalczany, A. Rojo, C. van Baren, S. Debenedetti, and C. Acevedo, Fitoterapia, 70 , 166 (1999)
  • [10] R.M.E. Richards, D.G. Durham, and X. Liu, Planta Med., 60 , 471 (1994)
  • [11] G.M. Woldemichael, M.P. Singh, W.M. Maiese, and B.M. Timmermann, Z. Naturforsch., 58c , 70 (2003)
  • [12] Y. Kashiwada, T. Nagao, A. Hashimoto, Y. Ikeshiro, H. Okabe, L.M. Cosentino, and K.H. Lee, J. Nat. Prod., 63 , 1619 (2000)
  • [13] E.C. Torres-Santos, D. Lopes, R. Rodrigues Oliveira, J.P.P. Carauta, C.A. Bandeira Falcao, M.A.C. Kaplan, and B. Rossi-Bergmann, Phytomedicine, 11 , 114 (2004)
  • [14] J. Liu, J. Ethnopharmacol., 49 , 57 (1995)
  • [15] L.I. Somowa, A. Nadar, P. Rammanan, and F.O. Shode, Phytomedicine, 10 , 115 (2003)
  • [16] H.G. Jeong, Toxicol. Lett., 105 , 215 (1995)
  • [17] C. Farina, M. Pinza, and G. Pifferi, Farmaco, 53 , 22 (1998)
  • [18] M.C. Aguirre, C. Delporte, N. Backhouse, S. Erazo, M.E. Letelier, B.K. Cassels, X. Silva, S. Alegria, and R. Negrete, Bioorg. Med. Chem., 14 , 5673 (2006)
  • [19] C.-M. Ma, S.-Q. Cai, J.-R. Cui, R.-Q. Wang, P.-F. Tu, M. Hattori, and M. Daneshtalab, Eur. J. Med. Chem., 40 , 582 (2005)
  • [20] L. Shi, W. Zhang, Y.Y. Zhou, Y.N. Zhang, J.Y. Li, L.H. Hu, and J. Li, Eur. J. Pharm., 584 , 21 (2008)
  • [21] X. Wen, J. Xia, K. Cheng, L. Zhang, P. Zhang, J. Liu, L. Zhang, P. Ni, and H. Sun, Bioorg. Med. Chem. Lett., 17 , 5777 (2007)
  • [22] K. Yamada, M. Hosokawa, S. Fujimoto, H. Fujiwara, Y. Fujita, N. Harada, C. Yamada, M. Fukushima, N. Ueda, T. Kaneko, F. Matsuyama, Y. Yamada, Y. Seino, and N. Inagaki, Diab. Res. Clin. Pract., 80 , 48 (2008)
  • [23] Y. Yamaguchi, K. Yamada, N. Yoshikawa, K. Nakamura, J. Haginaka, and M. Kunitomo, Life Sci., 79 , 2474 (2006)
  • [24] G. Janicsak, M. Veres, M. Kallai, and I. Mathe, Chromatographia, 58 , 295 (2003)
  • [25] M.C. Perez-Camino and A. Cert, J. Agric. Food Chem., 47 , 1558 (1999)
  • [26] G. Takeoka, L. Dao, R. Teranishi, R. Wong, S. Flessa, L. Harden, and R. Edwards, J. Agric. Food Chem., 48 , 3437 (2000)
  • [27] J.H. Chen, Z.H. Xia, and R.X. Tan, J. Pharm. Biomed. Anal., 32 , 1175 (2003)
  • [28] B. Claude, P. Morin, M. Lafosse, and P. Andre, J. Chromatogr. A, 1049 , 37 (2004)
  • [29] J.P. Fan and C.H. He, J. Pharm. Biomed. Anal., 41 , 950 (2006).
  • [30] F. Gbaguidi, G. Accrombessi, M. Moudachirou, and J. Quetin-Leclercq, J. Pharm. Biomed. Anal., 39 , 990 (2005)
  • [31] L. Novotny, M.E. Abdel-Hamid, H. Hamza, I. Masterova, and D. Grancai, J. Pharm. Biomed. Anal., 31 , 961 (2003)
  • [32] C. Zhou, K. Chen, C. Sun, Q. Chen, W. Zhang, and X. Li, Biomed. Chromatogr., 21 , 755 (2007)
  • [33] M.C.H. Tavares, J.H. Yariwake Vigelas, and F.M. Lancas, Phytochem. Anal., 12 , 134 (2001)
  • [34] P. Yang, Y. Li, X. Liu, and S. Jiang, J. Pharm. Biomed. Anal., 43 , 1331 (2007)
  • [35] H. Liu, Y. Shi, D. Wang, G. Yang, A. Yu, and H. Zhang, J. Pharm. Biomed. Anal., 32 , 479 (2003)
  • [36] D.H. Kim, K.M. Han, I.S. Chung, D.K. Kim, S.H. Kim, B.M. Kwon, T.S. Jeong, M.H. Park, E.M. Ahn, and N.I. Baek, Arch. Pharm. Res., 28 , 550 (2005)
  • [37] Y.L. Li, G. Wang, J.Y. Xue, and Y.Z. Cen, Zhongguo Zhong Yao Za Zhi, 32 , 605 (2007)
  • [38] P. Liu, H.Q. Duan, Q. Pan, Y.W. Zhang, and Z. Yao, Zhongguo Zhong Yao Za Zhi, 31 , 1875 (2006)
  • [39] S. Taniguchi, Y. Imayoshi, E. Kobayashi, Y. Takamatsu, H. Ito, T. Hatano, H. Sagatami, H. Tokuda, H. Nishino, D. Sugita, S. Shimura, and T. Yoshida, Phytochemistry, 59 , 315 (2002)
  • [40] P.T. Tuong, B.S. Min, W. Jin, M. Na, J. Lee, R. Seong, Y.M. Lee, K. Song, Y. Seong, H.K. Lee, K. Ba, and S.S. Kang, Biol. Pharm. Bull., 29 , 830 (2006)
  • [41] S.B. Mahato and A.P. Kundu, Phytochemistry, 37 , 1517 (1994)
  • [42] H. Kojima and H. Ogura, Phytochemistry, 28 , 1703 (1989)
  • [43] L.R. Snyder, J.J. Kirkland, and J.L. Glajch, Practical HPLC Method Development, 2nd edn, Wiley, New York, 1988, pp. 23–27 and 714–720.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BATE-0001-0049
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.