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Warianty tytułu
Języki publikacji
Abstrakty
A reversed-phase chiral liquid chromatographic method had been developed and validated for resolution of the enantiomers of racemic fudosteine. The effects on the separation of the amounts of anhydrous cupric sulfate and L -phenylalanine, the methanol content, mobile phase pH, and temperature were investigated. The method was validated for linearity, repeatability, intermediate precision, sample recovery, solution stability, and limits of detection (LOD). L -Phenylalanine and anhydrous cupric sulfate as chiral ligand-exchange complexes were used for separation, isomer identification, related substance investigation, and analysis of fudosteine enantiomers in fudosteine bulk drugs and fudosteine tablets.
Słowa kluczowe
Czasopismo
Rocznik
Tom
Strony
585--594
Opis fizyczny
Bibliogr. 15 poz., rys., tab.
Twórcy
autor
autor
autor
autor
autor
autor
autor
autor
autor
- Nanjing Medical University School of Pharmacy Nanjing City 210029 P.R. China, xueminzhou001_001@yahoo.cn
Bibliografia
- [1] H. Komatsu, S. Yamaguchi, N. Komorita, K. Goto, S. Takagi, H. Ochi, and T. Okumoto, Pulm. Pharmacol. Ther., 18 , 121 (2005)
- [2] L. Li, X.Y. Chen, X.J. Dai, H. Chen, and D.F. Zhong, J. Chromatogr. B, 856 , 171 (2007)
- [3] J. Wen, Y.W. Wu, L.L. Zhang, Y.P. Qi, G.R. Fan, Y.T. Wu, and Z. Li, J. Chromatogr. B, 867 , 153 (2008)
- [4] S. Kumari, S. Prabhakar, M. Vairamani, C.L. Devi, G.K. Chaitanya, and K. Bhanuprakash, J. Am. Soc. Mass Spectrom., 18 , 1516 (2007)
- [5] L. Strekowski, M.T. Cegla, V. Honkan, H. Buczak, W.R. Winkeljohn, A.L. Baumstark, and W.D. Wilson, Bioorg. Med. Chem. Lett., 15 , 2720 (2005)
- [6] G.S. Yang, S.L. Yuan, X.J. Lin, Z.N. Qi, C.B. Liu, H.Y. Aboul-Enein, and G. Félix, Talanta, 64 , 320 (2004)
- [7] Y.J. Choi and S. Jung, Carbohydr. Res., 339 , 1961 (2004)
- [8] Z. Mustapha, B. Isabelle, R. Corinne, H. Somnath, H. Mohamed, F. Jennifer, D. Jean-Luc, and P. Eric, J. Chromatogr. A, 1185 , 291 (2008)
- [9] G.J. Ma, B.L. Gong, and C. Yan, Chin. J. Anal. Chem., 36 , 275 (2008)
- [10] H.I. Wen, S. Huang, and W.Y. Liu, Chin. J. New Drugs, 13 , 1135 (2004)
- [11] M. Shen, Qilu. Pharm. Affai., 24 , 464 (2005)
- [12] X.L. Song and W. Zhang, Chin. J. Pharm. Anal., 25 , 1143 (2005)
- [13] Q.J. Lin and Z.M. Chen, Chin. J. Pharm., 38 , 872 (2007)
- [14] G.M. Ran, L. Yang, L.Q. Yan, K. Liu, and X.J. Guo, Chin. J. Pharm. Anal., 25 , 1561 (2005)
- [15] Y. Wang and T.J. Hang, Pro. Pharm. Sci., 29 , 421 (2005).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BATE-0001-0044