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Abstrakty
Baseline separation of latanoprost and its isomers 15(S)-latanoprost (impurity I) and 5,6-trans-latanoprost (impurity II) has been achieved for the first time by HPLC on an NH2 column with heptane-2-propanol-acetonitrile 93:6:1 (v/v), with addition of a small amount of water, as mobile phase. Validation of the method is described.
Słowa kluczowe
Czasopismo
Rocznik
Tom
Strony
157--164
Opis fizyczny
Bibliogr. 14 poz., rys., tab.
Twórcy
autor
autor
autor
autor
autor
- Institute of Physical Chemistry, Polish Academy of Sciences, Kasprzaka 44/52, 01-224 Warsaw, Poland Pharmaceutical Research Institute, Rydygiera 8, 01-793 Warsaw, Poland E-mail: annab@ichf.edu.pl
Bibliografia
- [1] J. Stjernschantz and B. Resul, Drugs Fut., 17, 691 (1992)
- [2] B. Resul, J. Stjernschantz, K. No, Ch. Liljebria, G. Selen, M. Astin, M. Karlsson, and L.Z. Bito, J. Med. Chem., 36, 243 (1993)
- [3] S.F.E. Nilsson, M. Samuelsson, A. Bill, and J. Stjernschantz, Exp. Eye Res., 48, 707 (1989)
- [4] B. Sjőquist, S. Basu, K. Bergh, and P. Byding, Exp. Eye Res., 59, 146 (1994)
- [5] M. Abramovitz, M. Adam, Y. Boie, et al., Biochim. Biophys. Acta, 1483, 285 (2000)
- [6] Ch. Linden, E. Nuika, and A. Alm, Brit. J. Ophthalmol., 81, 370 (1997)
- [7] S. Nagasubramanian, G.P. Sheth, R.A. Hitchings, and J. Stjernschantz, Ophthalmology, 100, 1305 (1993)
- [8] Impurities in New Drug Substances. Q3A (R1), International Conference on Harmonisation of Technical Requirements for Registration of Pharmaceuticals for Human Use
- [9] A.R. Whorton, K. Carr, M. Smigel, L. Walker, K. Ellis, and J.A. Oates, J. Chromatogr. 163, 64 (1979)
- [10] S. Ahuja, Selectivity and Detectability Optimization in HPLC, John Wiley and Sons, New York, 1989
- [11] S.M. Plaised, T.A. Zwier, and B.G. Snider, J. Chromatogr., 281, 151 (1983)
- [12] V. Radulescu, C. Doneanu, C. Mandruta, and F. Cocu, Rev. Roum. Chim., 42, 1129 (1997)
- [13] M. Ashfaq, I.U. Khan, and M.N. Asghar, Anal. Lett., 39, 2235 (2006)
- [14] P.V. Morgan, S. Proniuk, J. Blanchard, and R.J. Noecker, J. Glaucoma, 10, 401 (2001).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BATE-0001-0013