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Abstrakty
A simple, rapid, and selective method has been developed for the separation and determination of Cr(VI) from Al(III), Cr(III), Mn(II), Fe(III), Co(II), Ni(II), Cu(II), Zn(II), Se(IV), Sr(II), Zr(IV), Cd(II), La(III), Ce(III), Hg(II), and U(VI). Separation was accomplished in 12.5 cm migration distance and 14 min migration time on titanic silicate ion-exchange plates with 0.4 M ammonium oxalate - 2.2 M aqueous ammonia, 1:1 (v/v), as mobile phase. Quantitative measurement of the separated zones of Cr(VI) was achieved by scanning densitometry at ? = 545 nm.
Słowa kluczowe
Czasopismo
Rocznik
Tom
Strony
170--176
Opis fizyczny
Bibliogr. 23 poz., rys., tab.
Twórcy
autor
- Chemistry Faculty, University of Tarbiat Moallem, 49, Mofatteh Avenue, Tehran-15614, Iran
autor
- Chemistry Faculty, University of Tarbiat Moallem, 49, Mofatteh Avenue, Tehran-15614, Iran
Bibliografia
- [1] E. Berman, Toxic Metals and their Analysis, Heyden and Son, London, 1980, p. 76
- [2] H. L. Hardy, in: A. Hamilton and H. L. Hardy (Eds) Industrial Toxicology, Publishing Sciences Group, Acton, 1974
- [3] W. W. Payne, Arch. Environ. Health, 1, 20 (1960)
- [4] A. Tessier and D. R. Turner (Eds), Metal Speciation and Bioavailability in Aquatic Systems, John Wiley and Sons, Chichester, 1995
- [5] S. W. Husain and S. Rasheedzad, Mikrochim. Acta, 1, 11 (1978)
- [6] S. W. Husain and S. Rasheedzad in: A. Frigerio and L. Renoz (Eds), Recent Developments in Chromatography and Electrophoresis, Elsevier, Amsterdam, 1979, pp. 239–245
- [7] S. W. Husain and V. Ghoulipour, J. Planar Chromatogr., 2, 474 (1989)
- [8] V. Ghoulipour and S. W. Husain, J. Planar Chromatogr., 13, 354 (2000)
- [9] V. Ghoulipour and S. W. Husain, Anal. Sci., 16, 1079 (2000)
- [10] S. W. Husain, Z. Ishghy, and M. Chaloosi, J. Planar Chromatogr., 3, 271 (1990)
- [11] S. W. Husain, Z. Ishghy, and M. Chaloosi, in H. Traitler, O. I. Vorshilova, and R. E. Kaiser (Eds), Proc. 6th Int. Symp. Planar Chromatography, Institute für Chromatography, Bad Dürkheim, 1991, pp. 137–141
- [12] S. W. Husain and Z. Ishghy, J. Liq. Chromatogr., 15, 1681 (1992)
- [13] G. T. Desai and D. R. Baxi, Indian J. Technol., 16, 204 (1978)
- [14] A. Clearfield, A. I. Bortun, and L. N. Bortun, in: J. A. Greig (Ed.), Ion Exchange Developments and Applications, Royal Society of Chemistry, Cambridge, 1996, p. 338
- [15] V. Ghoulipour and S. W. Husain, J. Planar Chromatogr., 12, 378 (1999)
- [16] E. Papp, A. Farkas, K. H. Otta, and E. Mincsovics, J. Planar Chromatogr., 13, 328 (2000)
- [17] K. Ferenczi-Fodor, A. Nagy-Turak, and Z. Vegh, J. Planar Chromatogr., 8, 349 (1995)
- [18] ICH Guideline Q2B, Validation of Analytical Procedures: Methodology (CPMP ICH/281/95)
- [19] A. M. Ure and C. M. Davidson (Eds), Chemical Speciation in the Environment, Blackie Academic and Professional, Glasgow, 1995
- [20] K. Isshiki, Y. Sohrin, H. Karatami, and E. Nakayama, Anal. Chim. Acta, 224, 55 (1989)
- [21] E. Beceiro-Gonzalez, J. Barciela-Garcia, P. Bermejo-Barrera, and A. Bermejo-Barrera, Fresenius’ Z. Anal. Chem., 344, 301 (1992)
- [22] M. Sperling, S. Xu, and B. Welz, Anal. Chem., 64, 3101 (1992)
- [23] R. K. Mugo and K. J. Orians, Anal. Chim. Acta, 271, 1 (1993)
Typ dokumentu
Bibliografia
Identyfikator YADDA
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