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Researches on New Crystalline Form of Some Insensitive High Explosives in PBX

Wybrane pełne teksty z tego czasopisma
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
In this paper, the results of researches on crystallization of insensitive high explosives were described. 3-Nitro-1,2,4-triazol-5-one (NTO) and nitroguanidine (NQ) were selected. The laboratory methods of preparation were presented. The influence of different solvents and other parameters on crystallization process was investigated. The results of the particle size distribution in the crystals obtained were presented. The suitability of NTO and NQ for their application in plastic bonded explosives (PBX) was checked.
Słowa kluczowe
EN
NTO   NQ   PBX  
Rocznik
Strony
63--73
Opis fizyczny
Bibliogr. 18 poz.
Twórcy
autor
  • Institute of Industrial Organic Chemistry, 6 Annopol Str., 03-236 Warsaw, Poland
  • Institute of Industrial Organic Chemistry, 6 Annopol Str., 03-236 Warsaw, Poland
autor
  • Military University of Technology, 2 Kaliskiego Str., 00-908 Warsaw 49, Poland
  • Military University of Technology, 2 Kaliskiego Str., 00-908 Warsaw 49, Poland
autor
  • ZTS Nitron S.A., 1 Zawadzkiegi Str., 42-693 Krupski Młyn, Poland
Bibliografia
  • [1] Cudziło S., Trzcinski W. A., Otrzymywanie i badanie parametrow detonacyjnych 3-nitro-l,2,4-triazol-5-on (NTO),Biul WAT, 2000,XLIX,Nr 12.
  • [2] Cetner W., Preparatyka materiałów wybuchowych i produktów pośrednich, Skrypt WAT, Warszawa 1986.
  • [3] Kim K-J. et al., Seeded Batch Cooling Crystalization of 3-Nitro-l ,2,4-triazol-5-one, Proc. 32nd International Annual Conference of ICT, Ignition, Combustion and Detonation, Karlsruhe, July 3-6,2001,125/1-125/7.
  • [4] Gimenez P. et a!., An Extensive Study of Pressed NTO, Proc. Tenth International Symposium on Detonation, Boston, July 12-16,1993,276-283.
  • [5] Kim K-J. et al, Recrystallization of NTO Crystals in a Bath Cooling Crystallizer, Proc. 29'h International Annual Conference of ICT, Energetic Materials. Production, Processing and Characterization, Karlsruhe, June 30 - July 3, 1998, 64/1-64/6.
  • [6] Sanchez J. A., Roemer E L., Stretz L. A., Spherical Nitroguanidine Process, US Pat. 4967000,1990.
  • [7] Thiel K-D., Heinisch H., Process for the Production of Spherulitic Particles, US Pat. 5696407,1997.
  • [8] Engel W., Heinisch H., Process for the Preparation of Compact Nitroguanidine, US Pat. 4 544 769,1985.
  • [9] Chapmann L. B., NTO Development at Los Alamos, Proc. Ninth Symposium (International) on Detonation, Portland, August 28 -September 1,1989,1001-1008.
  • [10] Cudziło S. el al., Wojskowe materiały wybuchowe, Częstochowa 2000,
  • [11] Kienyin L., Gilardi R., NTO polymorphs, Structure and Properties of Energetic Materials, Symp. Proceedings, vol. 296, Materials Research Society, Pittsburgh, Pensylvania 1993.
  • [12] Lee K-Y., Coburn M. D.. 3-Nitro-1,2,4-triazoIe-5-one a Less Sensitive Explosive, Los Alamos National Laboratory Report No. LA-10303-MS, Feb 1985.
  • [13] Fouche F. C., van Schalkwyk G. C., TNT-Based Insensitive Munitions, Proc. 27th Annual Conference of lCT, Energetic Materials - Technology, Manufacturing and Processing, Karlsruhe, June 25-28,1996,69/1-69/12.
  • [14] Dudek K., Marecek P., Jalovy Z., Some Properties of Cast TNAZ Mixtures, Proc. 33rd International Annual Conference of ICT, Energetic Materials. Synthesis, Production and Application, Karlsruhe, June 25-28, 2002, 53/1-53/7.
  • [15] Koo K-K, et al, A Preliminary Study on Recrystallization of NTO, Proc. Twenty Third International Pyrotechnics Seminar, Tsukuba 30 September - 4 October, 1997,357-368.
  • [16] J. Kohler, R, Meyer, Explosives, 4 rev. and extended ed., Wiley-VCH, Weincheim 1993.
  • [17] Tang Y., The Effect of NQ and TATB to the Insensitivity of HMX, Proc. 33rd International Annual Conference of ICT, Energetic Materials. Synthesis, Production and Application, Karlsruhe, June 25-28, 2002, 54/1-54/7.
  • [18] von Ripper E., Krien G,, Uber a-und p-Nitroguanidin, Explosivstoffe, 1969,17, 7, 145-151.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BAT1-0036-0081
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