Application of LC-MSD and GC-ECD Techniques in the Analysis of Post-explosion Residues of Explosives with Content of 1,3,5-Trinitroso-1,3,5-triazinane

• Autorzy: Varga R. , Zeman S. , Vágenknecht J. , Koložvári M.
• Języki publikacji: EN

Abstrakty

EN

The paper deals with possible applications of the connection of liquid chromatography with atmospheric pressure chemical ionization (APCI) mass spectrometry (Agilent 1100 series LS-MSD system) and gas chromatography with electron capture detector (GC-ECD) in the analysis of some common available or improvised explosives. The analysis of selected types of individual explosives, 2,4,6-trinitrotoluene (TNT), 1,3,5-trinitroso-1,3,5-triazinane (TMTA) and analysis of their mixtures (TNT/TMTA and RDX/TMTA) in their post-explosion residues on the basis of generated characteristic mass spectra by using LC-MSD system is the aim of this work. Post-explosion analysis of TMTA and its explosive mixtures can be similarly complicated, like that of the well-known plastic explosive on the basis of pentaerythritol tetranitrate, Semtex-1A.

Słowa kluczowe

EN

explosive; LC-APCI/MS; GC-ECD; 1,3,5-trinitroso-1,3,-triazinane; TMTA; trace analysis; 2,4,6-trinitrotoluene; TNT

• Czasopismo: Central European Journal of Energetic Materials
• Rocznik: 2005
• Tom: Vol. 2, nr 3
• Strony: 85--96
• Opis fizyczny: Bibliogr. 14 poz.

Twórcy

autor

Varga R.

• Institute of Energetic Materials University of Pardubice CZ-532 10 Pardubice, Czech Republic

autor

Zeman S.

• Institute of Energetic Materials University of Pardubice CZ-532 10 Pardubice, Czech Republic

autor

Vágenknecht J.

• Institute of Energetic Materials University of Pardubice CZ-532 10 Pardubice, Czech Republic

autor

Koložvári M.

• Institute of Forensic Science of the Slovak Police Corps Sklabinska l SK-8l2 72 Bratislava, Slovak Republic

Bibliografia

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