Identyfikatory
Warianty tytułu
Języki publikacji
Abstrakty
The aim of this work was to characterize the microstructure of LMO type ceramics. The ceramics obtained by the free sintering at two temperatures 1473 K and 1573 K and two sintering times 6 and 12 h was the test material. One series was also obtained by the hot pressing method for a comparison. In all the cases the material synthesis was conducted by the solid-state reaction method at 1173 for 24 h. Photographs of the specimen fractures were taken by a scanning electron microscope to characterize the microstructure of the ceramics obtained in a more detailed way. The VISILOG 4 system, enabling to calculate a lot of parameters characterizing the material microstructure, such as e.g.: a number of grains on the unit area, an average grain size, shape indexes of the grains in question, was used as well. It allows determining a grain size distribution, and a frequency of presence of grains with the specific shape index. By analyzing a set of the parameters obtained an influence of the technological conditions on the microstructure of the material in question, and on its properties and applicability at the same time can be determined.
Słowa kluczowe
Wydawca
Czasopismo
Rocznik
Tom
Strony
857--862
Opis fizyczny
Bibliogr. 10 poz., rys.
Twórcy
autor
- University of Silesia, Faculty of Computer Science and Material Science, Institute of Technology and Mechatronics, 12 Żytnia Str., 41-200 Sosnowiec, Poland
autor
- University of Silesia, Faculty of Computer Science and Material Science, Institute of Technology and Mechatronics, 12 Żytnia Str., 41-200 Sosnowiec, Poland
Bibliografia
- [1] R. von Helmholdt, J. Wecker, B. Holzapfel, L. Schultz, K. Samwer, Physical Review Letters 71 (14), 2331- 2333 (1993).
- [2] S. Jin, T.H. Tiefel, M. McCormack, R. A. Fastnacht, R. Ramesh, L.H. Chen, Science 264, 413 - 415 (1994).
- [3] Q. Zhang, F. Saito, J. Alloys Compd. 297, 99 -103 (2000).
- [4] L. Balcells, R. Enrich, J. Mora, A. Calleja, J. Fontcuberta, X. Obradors, Applied Physics Letters 69 (10), 1486 - 1488 (1996).
- [5] A.M. Haghiri-Gosnet, J. P. Renard, Journal of Physics D: Applied Physics 36, R127 - 150 (2003).
- [6] S. P. Jang, J. Mater. Sci. 43, 6799 - 6833 (2008).
- [7] B. C. H. Steele, A. Heinzel, Nature 414, 345 - 352 (2001).
- [8] D. Marrero-Lopez, J. Pena-Martınez, D. Perez-Coll, P. Nunez, J. Alloys Compd. 422, 249 - 257 (2006).
- [9] J. Cybo, J. Chmiela, A. Maszybrocka, S. Stach, Solidification of metals and alloys 2(44), 409 - 416 (2000).
- [10] G. Górny, M. Rączka, L. Stobieski, L. Wojna, R. Pampuch, Solid State Ionics, 101-103, 953 - 58 (1997).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-ad31fff4-2965-4282-9198-74fe5a3c7ad6