The Influence of γ' Precipitates on the Structural Stability of FeNi-CoAlTa and FeNiCoAlTaB Single Crystals After Cyclic Superelastic Deformation

• Autorzy: Wójcik Anna , Chulist Robert , Szewczyk Arkadiusz , Dutkiewicz Jan , Maziarz Wojciech

Identyfikatory

DOI

10.24425/amm.2023.145488

• Języki publikacji: EN

Abstrakty

EN

Two single crystals with compositions Fe-Ni-Co-Al-Ta and Fe-Ni-Co-Al-Ta-B were selected and fabricated by Bridgman method. Subsequently, ingots were homogenized, oriented and subjected to a two-step heat treatment process in order to obtain fine and coherent γ' precipitates. Subsequently, superelastic cycling experiments were performed at 77 K. The next step included detailed microstructural characterization using transmission electron microscopy and high-energy synchrotron X-ray diffraction measurements together with Rietveld refinement. The results show that the number of fully reversible superelastic strains is very sensitive to the size of γ' precipitates. The smaller (3 nm) γ' precipitates ensured more superelastic response compared to material with larger γ' particles size (5 nm), in which the material did not receive its original shape after 10 cycles even after being heated.

Słowa kluczowe

EN

Fe-based shape memory alloys; superelastic effect; cyclic deformation; TEM

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2023
• Tom: Vol. 68, iss. 3
• Strony: 1157--1164
• Opis fizyczny: Bibliogr. 30 poz., fot., rys., tab.

Twórcy

autor

Wójcik Anna

• Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Krakow, Poland

• https://orcid.org/0000-0002-1774-751X

autor

Chulist Robert

• Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Krakow, Poland

• https://orcid.org/0000-0001-6680-9636

autor

Szewczyk Arkadiusz

• Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Krakow, Poland

• https://orcid.org/0000-0001-7658-0628

autor

Dutkiewicz Jan

• Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Krakow, Poland

• https://orcid.org/0000-0001-5206-1153

autor

Maziarz Wojciech

• Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Krakow, Poland

• https://orcid.org/0000-0001-8363-9640

Bibliografia

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Uwagi

The work was financed by the Institute of Metallurgy and Materials Science of the Polish Academy of Sciences within the statutory work Z-12/2021.