The Study of Selected Properties of Ti EB PVD Coating Deposited Onto Inner Tube Surface at Low Temperature

• Autorzy: Kottfer D. , Ferdinandy M. , Kaczmarek L. , Trebuňa P. , Hvizdoš P.

Identyfikatory

DOI

10.1515/amm-2016-0016

• Języki publikacji: EN

Abstrakty

EN

This study investigates the selected properties of the thin Ti coating applied by activated evaporation EB PVD technique. This technique was used for the deposition of Ti thin coating onto inner surface of OKhN3 MFA steel tubes. Deposition process was carried out at temperature 200°C. Conventional type of coatings - monolayer Ti - was analyzed by standard techniques for surface status and quality assessment - coating thickness, chemical composition by EDX analysis, adhesion, hardness, roughness, and growth direction of columns at room temperature. Ti monolayer achieved roughness Ra equal from 0.42 μm to 0.47 μm. The resulting hardness was from 2 GPa to 8.5 GPa depending on the sample location inside the vacuum chamber. Placing of the coated surface also affected the direction of grain growth of Ti coating columns. The angles α of grain growth were found to be from 40° to 60°. Angle α increased two to three times more than the incidence angle β (from 12° to 28°) of evaporated Ti particles. Values of the adhesion measured along the Ti growth direction were mostly higher (up to 10%) or the same as those measured perpendicular to it.

Słowa kluczowe

EN

Ti coating; properties; hardness; Young's modulus; growth direction of coating columns

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2016
• Tom: Vol. 61, iss. 1
• Strony: 67--74
• Opis fizyczny: Bibliogr. 22 poz., rys., schem., tab., wykr.

Twórcy

autor

Kottfer D.

• Technical University of Kosice, Mäsiarska 74, Department of Technology and Materials, Faculty of Mechanical Engineering, 040 01 Košice, Slovak Republic

autor

Ferdinandy M.

• Slovak Academy of Sciences, Institute of Materials Research, Watsonova 47, 040 01 Košice, Slovak Republic

autor

Kaczmarek L.

• Technical University of Lodz, Institute of Material Science and Engineering, 90-924 Lodz, Stefanowskiego 1/15, Poland

autor

Trebuňa P.

• Technical University of Kosice, Department of Industrial Engineering and Management, Faculty of Mechanical Engineering, Nemcovej 32, 04200 Košice, Slovak Republic

autor

Hvizdoš P.

• Slovak Academy of Sciences, Institute of Materials Research, Watsonova 47, 040 01 Košice, Slovak Republic

Bibliografia

• [1] E. Vassallo, R. Caniello, A. Cremona, D. Dellasega, E. Miorin, Titanium interlayer to improve the adhesion of multilayer amorphous boron carbide coating on silicon substrate, Applied Surface Science 266, 170- 175 (2013).
• [2] K. Perzynski, Ł. Major, Ł. Madej, M. Pietrzyk, Analysis of the Stress Concentration in the Nanomultilayer Coatings Based on Digital Representation of the Structure, Arhives of Metallurgy and Materials 56, 2 393-399 (2011).
• [3] D. Kottfer, Thin coatings on internal cylindrical surfaces (in slovak), Habilitation, Technical university of Košice, Faculty of mechanical engineering, 2010, p.92,
• [4] S. Kataria, R. Ramaseshan, S. Dash, A. K. Tyagi, Nanoindentation and Scratch Studies on Magnetron Sputtered Ti Thin Films, J. Nanosci. Nanotechnol. 9, 5476-5479 (2009).
• [5] S. Kataria, N. Kumar, S. Dash, A. K. Tyagi, Tribological and deformation behaviour of titanium coating under different sliding contact conditions, Wear 269 797-803 (2010).
• [6] N. Chelliah, S. V. Kailas, Synergy between tribo-oxidation and strain rate response on governing the dry sliding wear behaviour of titanium, Wear 266, 704-712 (2009).
• [7] B. Bhushan, B. K. Gupta, Handbook of tribolohy, McGraw- Hill Inc. ISBN 0-07-005249-2 p. 1069 (1991).
• [8] T. Jamal, R. Nimmagada, R. F. Bunshah, Friction and Adhesive Wear of Titanium Carbide and Titanium Nitride Overlay Coatings, Thin Solid Films 73 (1980) 245-254
• [9] N. X. Randall, Finer particle size allows better coating characterisation with the Calotest, Applications bulletin, Dokument AB No5, CSM Instruments, Advanced Mechanical Surface Testing, October 1997.
• [10] N. X. Randall, Development and application of a multifunctional nanotribological tool, PhD Thesis, University of Neuchâtel, Switzerland,1997.
• [11] K. Chu, Y. H. Lu, Y. G. Shen, Structural and mechanical properties of titanium and titanium diboride monolayers and Ti/TiB2 multilayers, Thin Solid Films 516, 5313-5317 (2008).
• [12] J. Xu, M. Kamiko, H. Sawada, Y. Zhou, R. Yamamoto, L. Yu, I. Kojima, Structure, hardness, and elastic modulus of Pd/Ti nanostructured multilayer films, J. Vac. Sci. Technol. B 21,6., Nov-Dec (2003).
• [13] G. S. Kim, S. Y. Lee, J. H. Hahn, B. Y. Lee, J. G. Han, J.H. Lee, S. Y. Lee, Effects of the thickness of Ti buffer layer on the mechanical properties of TiN coatings, Surface and Coatings Technology 171, 83-90 (2003).
• [14] A. A. Voevodin, M. A. Capano, S. J. P. Laube, M. S. Donley, J. S. Zabinski, Design of a Ti/TiC/DLC functionally gradient coating based on studies of structural transitions in Ti-C thin films, Thin Solid Films 298, 107-115 (1997).
• [15] K. Miyoshi, B. Pohlchuck, Kenneth W. Street, J. S. Zabinski, J. H. Sanders, A. A. Voevodin, R. L. C. Wu, Sliding wear and fretting wear of diamond like carbon-based, functionally graded nanocomposite coatings, Wear 225-229, 65-73 (1999).
• [16] Haman Hedaiatmofidi, Alireza Sabour Rouh Aghdam, Shahrokh Ahangarani, Mansour Bozorg, Mahboube Azadi, Maryam Valiei, Deposition of Titanium Layer on Steel Substrate Using PECVD Method: A Parametric Study, Materials Sciences and Applications 5, 140-148 (2014).
• [17] A. A. Voevodin, J. S. Zabinski, C. Muratore, Recent Advances in Hard, Tough, and Low Friction Nanocomposite Coatings, Tsinghua Science and Technology 10(6), 665-679, December (2005).
• [18] R. L. Boxman, V. N. Zhitomirsky, Vacuum arc deposition devices, Rev. Sci. Instrum77, 2, 021-101 (2006).
• [19] A. Matthews, A. R. Lefkow, Problems in the physical vapour deposition of titanium nitride, Thin Solid Films 126, 283-291 (1985).
• [20] R. Messier, A. P. Giri, R. A. Roy, Revised structure zone model for thin film physical structure, J. Vac. Sci. Technol. A 2 (2), April.-June (1984).
• [21] W. Ensinger: Low energy ion assist during deposition - an effective tool for controlling thin film microstructure, Nuclear Instruments and Methods in Physics Research B 127/ I28, 796-808 (1997).
• [22] Standard ASTM D7187: Test Method for Measuring Mechanistic Aspects of Scratch/Mar Behavior of Paint Coatings by a Nanoscratching. Conshohocken: ASTM International (2005).

Uwagi

PL

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę