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Zastosowanie technik chromatograficznych do badań charakterystyki fizykochemicznej czystych substancji i mieszanin

Treść / Zawartość
Identyfikatory
Warianty tytułu
EN
Study of physicochemical characteristic of pure substances and mixtures by means of chromatographic techniques
Języki publikacji
PL
Abstrakty
PL
W pracy przedstawiono metody wyznaczania charakterystyki fizykochemicznej substancji czystych i ich mieszanin z zastosowaniem technik chromatograficznych. Opisano metodę destylacji symulowanej oraz techniki odwróconej chromatografii cieczowej i gazowej. Przedstawiono metody wyznaczania parametrów rozpuszczalności, entalpii adsorpcji, współczynnika podziału, porowatości, właściwości kwasowo-zasadowych.
EN
The paper presents methods of determination of the physicochemical properties of pure substances and their mixtures by the use of chromatographic techniques. Simulated distillation, reversed gas and liquid chromatography have been described. Basic equation and relationship allowing to calculate solubility parameters, adsorption enthalpy and isotherm, partition coefficient, porosity and acid/based characteristic are also given.
Czasopismo
Rocznik
Strony
17--23
Opis fizyczny
Bibliogr. 37 poz.
Twórcy
  • Politechnika Gdańska, Wydział Chemiczny, Katedra Inżynierii Chemicznej i Procesowej
autor
  • Politechnika Gdańska, Wydział Chemiczny, Katedra Inżynierii Chemicznej i Procesowej
Bibliografia
  • 1. K. Shcherbakova, Y. I. Yashin, V. Andrej, Kiselev's contributions to the science of adsorption, molecular interaction and chromatography, Pure and Applied Chemistry 61 (1989) 1829.
  • 2. D. Butler i D. R. Williams, Particulate characterization: inverse gas chromatography w Encyclopedia of Separation Science, Londyn, Elsevier Science Ltd, 2000, pp. 3609-3614.
  • 3. F. T. Eggertsen, S. Groennings, J. J. Holst, Analytical distillation by gas chromatography programmed temperature operation, Analytical Chemistry 32 (1960) 904.
  • 4. L. E. Green, L. J. Schmauch, J. C. Worman, Simulated distillation by gas chromatography, Analytical Chemistry 36 (1964) 1512.
  • 5. PN-EN 15199-3, Oznaczanie rozkładu temperatur wrzenia metodą chromatografii gazowej- ropa naftowa.
  • 6. L. M. Meyer i R. L. Shearer, Simultaneous measurement of hydrocarbons and sulfur compounds using flame ionization and sulfur chemiluminescence detection for sulfur simulated distillation, Journal of High Resolution Chromatography 22 (1999) 386.
  • 7. J. L. Buteyn i J. J. Kosman, Multielement simulated distillation by capillary GC-AED, Journal Chromatography Science, 28 (1990) 19.
  • 8. W. P. Fitzgerald i S. G. Roussis, Gas chromatographic simulated distillation-mass spectrometry for the determination of the boiling point distributions of crude oils, Analytical Chemistry 72 (2000) 1400.
  • 9. E. M. Canto, M. B. De Souza, A. D. M. Lima i M. L. M. Valle, Using simulated distillation or density to maximize lubricants production from low density pole ethylene LDPE pyrolysis, Chemical Engineering Transactions 26 (2012) 219.
  • 10. A. G. Goossens, Prediction of molecular weight of petroleum fractions, Industrial & Engineering Chemistry Research 35 (1996) 985.
  • 11. G. Boczkaj, A. Przyjazny, M. Kamiński, A new procedure for the determination of distillation temperature distribution of high-boiling petroleum products and fractions, Analytical and Bioanalytical Chemistry 399 (2011) 3253.
  • 12. G. Boczkaj, M. Kamiński, Research on the separation properties of empty-column gas chromatography (EC-GC) and conditions for simulated distillation (SIMDIS), Analytical and Bioanalytical Chemistry 405 (2013) 8377.
  • 13. G. Boczkaj, M. Momotko, A. Przyjazny, M. Kamiński, Studies of separation performance of silanized silica gel for simulated distillation, Journal of Separation Science, 2015. DOI: 10.1002/jssc.201501127.
  • 14. G. Boczkaj, A. Przyjazny, M. Kamiński, Size-exclusion chromatography for the determination of the boiling point distribution of high-boiling petroleum fractions, Journal of Separation Science 38 (2015) 741.
  • 15. M. Momotko, G. Boczkaj, Use of simulated distillation for analysis of petroleum-derived products (Zastosowanie destylacji symulowanej do analizy produktów naftowych), Przemysł Chemiczny 4 (2015) 594.
  • 16. F. Thielmann, Introduction into the characterization of porous materials by inverse gas chromatography, Joural of Chromatography A 1037 (2004) 115.
  • 17. K. Czech, P. M. Słomkiewicz, Zastosowanie pakietów oprogramowania komputerowego do wyznaczania izoterm adsorpcji metodą inwersyjnej chromatografii gazowej, Camera Separatoria 3 (2011) 329.
  • 18. M. M. Chehimi, M. L. Abel, C. Perruchot, M. Delamar, S. F. Lascelles, S. P. Armes, The determination of the surface energy of conducting polymers by inverse gas chromatography at infinite dilution, Synthetic Metals, 104 (1999) 51.
  • 19. G. M. Dorris, D. G. Gray, Adsorption, spreading pressure, and London force interactions of hydrocarbons on cellulose and wood fiber surfaces, Journal of Colloid Interface Science 71 (1979) 93.
  • 20. G. M. Dorris, D. G. Gray, Adsorption of n-alkanes at zero coverage on cellulose paper and wood fibers, Journal of Colloid Interface Science 77 (1980) 353.
  • 21. T. J. Bandosz, J. Jagiełło, B. Andersen, J. A. Schwarz, Inverse gas chromatography study of modified smectite surface, Clays Clay Minerals 40 (1992) 306.
  • 22. A. Voelkel i J. Fall, Influence of prediction method of the second virial coefficient on inverse gas chromatographic parameters, Journal of Chromatography A 721 (1995) 139.
  • 23. C. Tsonopoulos, An empirical correlation of second virial coefficients, American Institute of Chemical Engineers 20 (1974) 263.
  • 24. K. S. Pitzer, R. F. Curl, The volumetric and thermodynamic properties of fluids. 3. Empirical equation for the 2nd virial coefficient, Journal of the American Chemical Society 79 (1957) 2369.
  • 25. A. Voelkel, J. Fall, Application of inverse gas chromatography to the examination of annealing processes of semi-synthetic base oils, Journal of Chromatography A 982 (2002) 245.
  • 26. A. Voelkel, J. Janas, J. A. Garcia-Dominguez, Inverse gas chromatography in characterization of surfactants. Determination of binary parameter, Journal of Chromatography A 654 (1993) 135.
  • 27. F. Mutelet, V. Butet, J. Jean-Noel, Application of Inverse Gas Chromatography and Regular Solution Theory for Characterization of Ionic Liquids, Industrial & Engineering Chemistry Research 44 (2005) 4120.
  • 28. M. K. Kozłowska, U. Domańska, M. Lempert, M. Rogalski, Determination of thermodynamic properties of isotactic poly(1-butene) at infinite dilution using density and inverse gas chromatography, Journal of Chromatography A 1068 (2005) 297.
  • 29. R. Y. M. Huang, P. Shao, G. Nawawi, X. Feng, C. M. Burns, Measurements of partition, diffusion coefficients of solvents in polymer membranes using rectangular thin-channel column inverse gas chromatography (RTCCIGC), Journal of Membrane Science. 188 (2001) 205.
  • 30. J. A. Widegren, T. J. Bruno, Enthalpy of adsorption for hydrocarbons on concrete by inverse gas chromatography, Journal of Chromatography A 1218 (2011) 4474.
  • 31. K. E. Miller, T. J. Bruno, Enthalpy of fuel gas odorants on surrogate soil surface by gas chromatography, Journal of Chromatography A 975 (2002) 311.
  • 32. T. C. Davis, J. Petersen, Inverse gas-liquid chromatographic studies of asphalt. Comparison with analyses by fractionation, Analytical Chemistry 39 (1967) 1852.
  • 33. T. C. Davis, J. C. Petersen, W. E. Haines, Inverse gas-liquid chromatography a new approach for studying petroleum asphalts, Analytical Chemistry 38 (1966) 241.
  • 34. T. C. Davis, J. C. Petersen, An adaptation of inverse gas-liquid chromatography to asphalt oxidation studies, Analytical Chemistry 38 (1966) 1938.
  • 35. M. Al-Bokari, D. Cherrak, G. Guiochon, Determination of the porosities of monolithic columns by inverse size-exclusion chromatography, Journal of Chromatography A 975 (2002) 275.
  • 36. P. DePhillips, A. M. Lenhoff, Pore size distributions of cation-exchange adsorbents determined by inverse size-exclusion chromatography, Journal of Chromatography A 883 (2000) 39.
  • 37. P. M. Słomkiewicz, B. Szczepanik, M. Garnuszek, Determination of adsorption isotherms of aniline and 4-chloroaniline on halloysite adsorbent by inverse liquid chromatography, Applied Clay Science 114 (2015) 221.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-a5f4c3a6-9432-45f4-8721-95f5309b0803
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