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Tytuł artykułu

Physical purification of diatomite based on laminar-flow centrifugal separation

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Treść / Zawartość
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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Natural diatomaceous earth or diatomite of good quality becomes rare and a demand for it increases every year. In this paper, we develop a novel method based on laminar-flow centrifugal separation to purify mid- and low-grade diatomite for industrial production purposes. Effects of the drum cone angle, drum speed, feeding concentration, feeding flow rate and feeding time on separation were investigated experimentally. The interdependency of these variables was studied using a response surface experiment. Operating conditions of a laminar-flow centrifugal separator were further optimized. Results showed that the feeding flow rate had a great influence on a silicon dioxide content of diatomaceous in concentrate and tailing. The optimal separation results were achieved as 87.5 wt.%, of SiO2 content of diatomaceous in concentrate and 6.98 wt.% in tailing. The optimal operating conditions included the drum cone angle of 0.0087 rad, the drum speed of 89.62 rad/s, the feeding concentration of 24.66 wt.%, the feeding flow rate of 2.33×10–4 m3/s, and the feeding time of 90 s. A scanning electron microscopy (SEM) clearly indicated that the pore blockage on the surface of diatoms was cleared out. The variation about the breakage rate of diatom shells was lower than 5% through the pilot purification production line. The characterization of original diatomite and derived products after purification were determined by X-ray diffraction (XRD). The results indicated that the impurity content of purified diatomite was improved significantly.
Rocznik
Strony
705--718
Opis fizyczny
Bibliogr. 29 poz., rys., tab.
Twórcy
autor
  • School of Chemical and Environmental Engineering, China University of Mining and Technology (Beijing), Beijing 100083, China
autor
  • School of Chemical and Environmental Engineering, China University of Mining and Technology (Beijing), Beijing 100083, China
autor
  • School of Chemical and Environmental Engineering, China University of Mining and Technology (Beijing), Beijing 100083, China
Bibliografia
  • 1. CUI, T. S., WU H. H., ZHOU Z. G., 1996, Research on mineral processing technology of low grade diatomite of Shuangjiang in Yunnan, Journal of Guilin institute of technology, 16(3), 313–316.
  • 2. DING H., LIN H., CUI T. S., 1995, Yunan Low grade diatomite purifying, Multipurpose utilization of mineral resources, (4), 12–14.
  • 3. FRANCA S. C. A, MILLQVIST M. T., LUZ A. B., 2003, Beneficiation of Brazilian diatomite for the filtration application industry, Minerals & Metallurgical Processing, 20 (1), 42–46.
  • 4. GU J. C., 2003, The study on the mechanism in purification of diatomite ore by microwave Strengthening (Doctoral dissertation), Sichuan University, Chengdu, China.
  • 5. GU J. C., LIU Y. C., ZHANG Y. X., 2003, Research on purifying the diatomite, Non-metallic Mines, 26(1), 46–47.
  • 6. IBRAHIM S. S., SELIM A. Q., 2011, Evaluation of Egyptian diatomite for filter aid applications, Physicochemical Problems of Mineral Processing, 47, 113–122.
  • 7. IBRAHIM S. S., SELIM A. Q., 2012, Heat treatment of natural diatomite, Physicochemical Problems of Mineral Processing, 48(2), 413−424.
  • 8. KOYUNCU M., 2012, Colour removal from aqueous solution of tar-chromium green 3g dye using natural diatomite, Physicochemical Problems of Mineral Processing, 48(2), 485–494.
  • 9. LI J., 1974, Laminar-flow centrifugal separator, Nonferrous Metals (Extractive Metallurgy), (2), 5–13.
  • 10. LI Y., ZHENG S. L., XIA Q. L., DU Y. C., 1997, Study of preparing fine pure active silica powder from diatomite, Conservation and utilization of mineral resources, (6), 17–19.
  • 11. MA S. Y., ZHOU Y. Y., LI X. J., 2012, Technology research of magnetic separation on iron-removal of Jilin diatomite, China Non-Metallic Minerals Industry, 96(3), 13–15.
  • 12. MARTINOVIC S., VLAHOVIC M., BOLJANAC T., PAVLOVIC L., 2006, Preparation of filter aids based on diatomite, Internal Journal of Mineral Processing, 80, 255–260.
  • 13. MENG X. Y., 1999, Study on dressing of clayey diatomite, Conservation and utilization of mineral resources, (1), 36–37.
  • 14. MOHAMED I. A., 2009, Characterization and process development of the Nile diatomaceous sediment, Internal Journal of Mineral Processing, 92, 128–136.
  • 15. OSMAN S., REMZI G., CEM O., 2009, Purification of diatomite powder by acid leaching for use in fabrication of porous ceramics, International Journal of Mineral Processing, 93, 6–10.
  • 16. QIU D. Y., SHENG G. Y., WU X. H., 2001, China Patent No. 01129546, Beijing: State Intellectual Property Office of the P. R. C.
  • 17. SHI D. M., ZHANG Z. H., 1993, Experiment research on Yunan Xundian diatomite purifying, Non-metallic Mines, 16(1), 7–10.
  • 18. SHI X. Z., YU D. S., WANG F. X., 2001, China Patent No. 00112041, Beijing: State Intellectual Property Office of the P. R. C.
  • 19. VIDENOV N., SHOUMKOV S., DIMITROV Z., 1993, Beneficiation of diatomites by high gradient magnetic separation, International Journal of Mineral Processing, 39(3–4), 291–298.
  • 20. WANG L. J., ZHENG S. L., CHEN J. T., SHU F., 2006, Study on purification & adsorption of diatomite, Non-metallic Mines, 29(2), 3–5.
  • 21. WANG X. M., 1980, Experiment report on producing activated white clay from diatomite, Zhejiang Chemical Industry, 4, 36–41.
  • 22. WANG X. Q., WANG Q. H., 1995, China Patent No. 94108311, Beijing: State Intellectual Property Office of the P. R. C.
  • 23. WANG Z. M., MA X. F., SUN W. T., WANG X. X., 1995, Research on acid treatment to purify the diatomite and the waste acid utilization, Non-metallic Mines, 18(1), 16–19.
  • 24. YUAN P., 2001, Study on purification of diatomite and its surface hydroxyl groups and acid sites (Doctoral dissertation), Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou, China.
  • 25. YANG Y. K., ZHANG Y. N., 1991, China Patent No. 90100675, Beijing: State Intellectual Property Office of the P. R. C.
  • 26. ZHENG S. L., 1994, Purification research on clayey diatomite in China, Non-metallic Mines, 17(4), 24–51.
  • 27. ZHENG S. L., 2009, Non-metallic mineral preparation and application (2nd ed.), Beijing: Chemical Industry Press, 141–142.
  • 28. ZHENG S. L., LI Y., DU Y. C., XIA Q. L., 1997, Purification technology research on clayey diatomite for one mine in Jilin, Non-metallic Mines, 20(4), 49–50.
  • 29. ZHENG S. L., WANG L. J., SHU F., CHEN J. T., 2006, Effect of calcining and sulfuric acid treatment on properties of diatomite, Journal of the Chinese Ceramic Society, 34(11), 82–68.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-a5a1c416-5b1e-47ef-9703-763484bb2ce6
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