Non-destructive method of determination of elastic properties and adhesion coefficient of different coating materials

• Autorzy: Kubisztal M. , Chrobak A. , Haneczok G.
• Języki publikacji: EN

Abstrakty

EN

Purpose: The paper presents a non-destructive method of determination of Young’s modulus and adhesion coefficient of different coating materials (metallic coatings, polymer, composite etc.). Some of the results obtained by applying this method are discussed in detail. Design/methodology/approach: The presented method consists in measuring the dynamic response of the examined material in the form of a flat rectangular bar subjected to external periodic mechanical stress i.e. the so called vibrating reed technique. General equations describing elastic properties of the sample consisting of a substrate and a deposited coating are derived and discussed in detail. Findings: It was shown that the application of the proposed approach to the metallic, polymeric and composite coatings allowed to obtain a quantitative data concerning the change of both the elastic properties and the adhesion coefficient with a change of: coating thickness, measurement temperature, chemical composition of coating, surface preparation or in the case of epoxy resin coatings with a change of curing time or curing temperature. Research limitations/implications: The proposed method can be applied in many scientific problems in the field of coating materials (e.g. elastic properties of porous coating, crystallization of amorphous coating, adhesion of different polymeric coatings). Practical implications: It was shown that the described method can be successfully used in optimisation of some technological processes of deposition of different coatings on metallic substrate. Originality/value: The paper presents methodology of a non-destructive approach to determination of elastic properties and adhesion coefficient of coating materials with an overview of some applications already publish and also the new ones. Especially interesting are the results concerning the influence of surface preparation on adhesion coefficient which are published for the first time.

Słowa kluczowe

EN

coating materials; elastic properties; Young's modulus; adhesion coefficient; free vibrations

PL

materiały powłokowe; właściwości sprężyste; moduł Younga; współczynnik przyczepności; drgania swobodne

• Wydawca: International OCSCO World Press
• Czasopismo: Journal of Achievements in Materials and Manufacturing Engineering
• Rocznik: 2010
• Tom: Vol. 43, nr 2
• Strony: 634--643
• Opis fizyczny: Bibliogr. 18 poz., rys., wykr.

Twórcy

autor

Kubisztal M.

• Institute of Materials Science, Silesian University, ul. Bankowa 12, 40-007 Katowice, Poland

autor

Chrobak A.

• Institute of Physics, Silesian University, ul. Uniwersytecka 4, 40-007 Katowice, Poland

autor

Haneczok G.

• Institute of Materials Science, Silesian University, ul. Bankowa 12, 40-007 Katowice, Poland

Bibliografia

• [1] M. Kubisztal, Elastic properties of the coatings on metallic substrate, Silesian University PhD work, Katowice, 2009 (in Polish).
• [2] A.S. Nowick, B.S. Berry, Anelastic Relaxation in Crystalline Solids, Academic Press, New York, 1972.
• [3] B.S. Berry, W.C. Pritchet, Vibrating reed internal friction apparatus for films and foils, IBM Journal of Research and Development 19 (1975) 334-343.
• [4] B.S. Berry, in: D. Gupta, P.S. Ho (Eds.), Diffusion Phenomena in Thin Films and Microelectronic Materials, Noyes, Park Ridge, New York, 1988, 73-141.
• [5] Q. Su, S.Z. Hua, M. Wuttig, Nondestructive dynamic evaluation of thin NiTi film adhesion, Journal of Adhesion Science and Technology 8 (1994) 625-633.
• [6] M. Wuttig, C.M. Su, Dynamic mechanical properties of thin-layer materials, Proceedings of the Damping of Multiphase Inorganic Materials Symposium, ASM Materials Week, Chicago, Illinois, USA, 1992, 159-163.
• [7] M. Kubisztal, G. Haneczok, A. Chrobak, B. Rams, D. Miara, J. Rasek, Elastic properties of epoxy system coatings on aluminum substrate, Surface and Coatings Technology 204 (2009) 120-124.
• [8] A. Chrobak, M. Kubisztal, J. Kubisztal, G. Haneczok, Adhesion coefficient and elastic properties of composite coatings on metallic substrate, Surface and Coatings Technology 204 (2010) 2077-2080.
• [9] M. Weller, in: R. Schaller, G. Fantozzi, G. Gremaud (Eds.), Mechanical Spectroscopy Qí1 2001, vol. 366–368, TTP, Uetikon-Zuerich, 2001, 549-559.
• [10] M. Kubisztal, G. Haneczok, A. Chrobak, J. Kubisztal, A. Budniok, Patent application P383058, 2007 (in Polish).
• [11] M. Kubisztal, J. Kubisztal, A. Chrobak, G. Haneczok, Young’s modulus and adhesion coefficient of amorphous Ni-P coatings on a metal substrate, Journal of Adhesion Science Technology 21/11 (2007) 1009-1019.
• [12] R.C. Agarwala, V. Agarwala, Electroless alloy/composite coatings: A review, Sadhana 28 (2003) 475-493.
• [13] M. Kubisztal, G. Haneczok, A. Chrobak, A. Kubik, J. Rasek, Study of epoxy resin curing process by applying internal friction technique, Materials Science and Engineering A 521(2009) 283-286.
• [14] Polish Standard PN-ISO 4588, 1999.
• [15] Polish Standard PN-EN 1465, 2003.
• [16] M. Kubisztal, J. Kubisztal, A. Chrobak, G. Haneczok, A. Budniok, J. Rasek, Elastic properties of Ni and Ni+Mo coatings electrodeposited on stainless steel substrate, Surface and Coatings Technology 202 (2008) 2292-2296.
• [17] J. Kubisztal, A. Budniok, A. Lasia, Study of the hydrogen evolution reaction on nickel-based composite coatings containing molybdenum powder, International Journal of Hydrogen Energy 32 (2007) 1211-1218.
• [18] J. Kubisztal, A. Budniok, Study of the oxygen evolution reaction on nickel-based composite coatings in alkaline media, International Journal of Hydrogen Energy 33 (2008) 4488-4494.