PZT-Type Ceramics Doped with Manganese, Antimony, Lanthanum and Tungsten - Technology and Physical Properties

• Autorzy: Bochenek D. , Niemiec P. , Ćwikiel E. , Goryczka T.

Identyfikatory

DOI

10.24425/amm.2020.132828

• Języki publikacji: EN

Abstrakty

EN

The work three ceramic compositions based on PbZr_0.49 Ti_0.51O₃ doped with manganese (Mn), antimony (Sb), lanthanum (La) and tungsten (W) were obtained. The introduction of a set of admixtures was aimed at improving the sinterability of ceramic materials and optimizing its electrophysical parameters. Multi-component materials of the PZT-type with a general formula: Pb(PbZr_0.49 Ti_0.51)_0.94 Mn_0.021 Sb_0.016 LayW_z O₃ (where y from 0.008 to 0.012 and z from 0.012 to 0.014) were prepared by the conventional mixed oxide method. After mixing and drying the powder mixtures were calcined in air at 850°C for 4 h, while densification of the powders was carried out by the free sintering method at 1150°C for 2 h. The final steps of technology were grinding, polishing, annealing and putting silver paste electrodes onto both surfaces of the samples for electrical testing. XRD, SEM, EDS, dielectric, ferroelectric, piezoelectric properties and DC electrical conductivity of the obtained ceramic compositions were carried out. X-ray tests of the crystal structure conducted at room temperature have shown that all obtained the PZT-type materials were a single phase (perovskite type) without the presence of a foreign phase. Symmetry of the crystal lattice was identified as space group P4mm. Temperature dielectric studies have shown high values of dielectric permittivity and low dielectric loss. The presented physical properties of ceramic samples based on PZT confirm their predisposition for application in modern microelectronic and micromechatronic applications.

Słowa kluczowe

EN

PZT type ceramics; perovskite type materials; ferroelectrics; doped

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2020
• Tom: Vol. 65, iss. 2
• Strony: 827--837
• Opis fizyczny: Bibliogr. 40 poz., fot., rys., tab., wzory

Twórcy

autor

Bochenek D.

• University of Silesia in Katowice, Faculty of Science and Technology, Institute of Materials Engineering, 75 Pułku Piechoty 1a, 41-500 Chorzów, Poland

autor

Niemiec P.

• University of Silesia in Katowice, Faculty of Science and Technology, Institute of Materials Engineering, 75 Pułku Piechoty 1a, 41-500 Chorzów, Poland

autor

Ćwikiel E.

• University of Silesia in Katowice, Faculty of Science and Technology, Institute of Materials Engineering, 75 Pułku Piechoty 1a, 41-500 Chorzów, Poland

autor

Goryczka T.

• University of Silesia in Katowice, Faculty of Science and Technology, Institute of Materials Engineering, 75 Pułku Piechoty 1a, 41-500 Chorzów, Poland

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Uwagi

PL

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).