Optimization of Olea europaea Stone-Activated Carbon Preparation Using Response Surface Methodology for Thiamphenicol Removal in a Fixed Bed Column

Samghouli, Nora; Bencheikh, Imane; Azoulay, Karima; El Hajjaji, Souad; Labjar, Najoua

doi:10.12912/27197050/190084

Artykuł - szczegóły

Tytuł artykułu

Optimization of Olea europaea Stone-Activated Carbon Preparation Using Response Surface Methodology for Thiamphenicol Removal in a Fixed Bed Column

Autorzy

Samghouli Nora , Bencheikh Imane , Azoulay Karima , El Hajjaji Souad , Labjar Najoua

Treść / Zawartość

Pełne teksty:

04_Samghouli_Optimization_EEET_2024_9.pdf

Pobierz

Identyfikatory

DOI

10.12912/27197050/190084

Warianty tytułu

Języki publikacji

Abstrakty

The study addresses the persistent issue of thiamphenicol (THI) accumulation in aquatic environments and its detrimental impact on biological systems. While activated carbon is commonly used for removing such organic micropollutants in advanced wastewater treatment, this research explores the innovative use of olive stones as a feedstock for activated carbon production. The novelty of this study lies in the optimization of the activated carbon preparation process using a fractional factorial design with five critical factors: concentration, heating rate, activation temperature, activation time, and impregnation ratio. By employing the methylene blue method to determine the specific surface area (SSA), the optimal conditions were identified: a phosphoric acid solid-liquid ratio of 1:2 (74.52%), a heating temperature of 550 °C at a rate of 10 °C/min, and an activation period of 120 minutes, resulting in an SSA of 53.07 m²/g. The subsequent THI adsorption tests in a fixed-bed column revealed that THI removal efficiency was inversely proportional to flow rate and initial THI concentration, while positively correlated with bed height. This study fills a critical gap by demonstrating an effective, sustainable method for producing activated carbon from agricultural waste, optimizing the process parameters for maximum efficiency in micropollutant removal.

Słowa kluczowe

olive fruit stone activated carbon response surface methodology thiamphenicol adsorption fixed-bed column

Wydawca

Lubelski Oddział Polskiego Towarzystwo Inżynierii Ekologicznej
Lublin University of Technology
WNGB Wydawnictwo Naukowe

Czasopismo

Ecological Engineering & Environmental Technology

Rocznik

2024

Tom

Vol. 25, iss. 9

Strony

37--53

Opis fizyczny

Bibliogr. 75 poz., rys., tab.

Twórcy

autor

Samghouli Nora

nora.samghouli@um5r.ac.ma

LS3MN2E-CERNE2D, Faculty of Sciences, Mohammed V University in Rabat, Av Ibn Battouta, B.P. 1014, Rabat 10000, Morocco

https://orcid.org/0000-0002-4338-6260

autor

Bencheikh Imane

LS3MN2E-CERNE2D, Faculty of Sciences, Mohammed V University in Rabat, Av Ibn Battouta, B.P. 1014, Rabat 10000, Morocco

https://orcid.org/0000-0002-6666-7209

autor

Azoulay Karima

LS3MN2E-CERNE2D, Faculty of Sciences, Mohammed V University in Rabat, Av Ibn Battouta, B.P. 1014, Rabat 10000, Morocco

https://orcid.org/0000-0001-5884-7819

autor

El Hajjaji Souad

souad.elhajjaji@fsr.um5.ac.ma

LS3MN2E-CERNE2D, Faculty of Sciences, Mohammed V University in Rabat, Av Ibn Battouta, B.P. 1014, Rabat 10000, Morocco

https://orcid.org/0000-0003-1467-704X

autor

Labjar Najoua

LS3MN2E-CERNE2D, ENSAM, Mohammed V University in Rabat, Av Ibn Battouta, B.P. 1014, Rabat 10000, Morocco

https://orcid.org/0000-0002-9273-2799

Bibliografia

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Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-a2a92b5d-b918-4b8b-a719-a93cef1ee15e