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Izolacja α-tokoferolu z bawełnianych kosmetotekstyliów
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Abstrakty
Cotton fabrics were treated with cosmetic substances based on α-tocopherol and cyclodextrine. Isolation of α-tocopherol from cotton cosmetotextiles was performed using three different techniques: stirring, Soxhlet and microwave extraction. High performance liquid chromatography (HPLC) was optimised and applied for the quantification of α-tocopherols in the isolates. The results revealed that all techniques are applicable for the isolation of α-tocopherol from cotton cosmetotextiles. The HPLC method proved to be the most convenient for the quantification of α-tocopherol from cotton fabrics.
W pracy obrabiano tkaniny bawełniane substancjami kosmetycznymi na bazie tokoferolu i cyklodekstryny. Izolację tokoferolu z kosmetotekstyliów bawełnianych przeprowadzono stosując trzy różne techniki: mieszanie, Soxhleta i ekstrakcję mikrofalową. Do oznaczenia ilościowego tokoferoli w izolatach zastosowano wysokosprawną chromatografię cieczową (HPLC). Wyniki wykazały, że wszystkie techniki mają zastosowanie do izolacji α-tokoferolu z kosmetotekstyliów bawełnianych. Metoda HPLC okazała się najbardziej dogodna do ilościowego oznaczenia α-tokoferolu z tkanin bawełnianych.
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38--42
Opis fizyczny
Bibliogr. 21 poz., rys., tab.
Twórcy
autor
- University of Zagreb, Faculty of Textile Technology, Department of Textile Chemistry and Ecology, Zagreb, Croatia
autor
- University of Zagreb, Faculty of Textile Technology, Department of Textile Chemistry and Ecology, Zagreb, Croatia
autor
- University of Zagreb, Faculty of Textile Technology, Department of Textile Chemistry and Ecology, Zagreb, Croatia
Bibliografia
- 1. Singh MK, Varun VK, Behera BK. Cosmetotextiles: State of Art. FIBRES & TEXTILES in Eastern Europe 2011; 19, 4(87): 27–33.
- 2. Adamowicz E, Śmigielski K, Frydrysiak M. Microencapsulation of active substances and fragrances in textile material applications. Tekstil 2015; 64(3-4): 128–132.
- 3. BSI. Textiles — Cosmetotextiles: PD CEN/TR 15917:2009. 2009.
- 4. Matijević I, Bischof S, Pušić T. Cosmetic preparations on textiles: Cosmetotextiles. Tekstil 2016; 65(1–2): 13–24.
- 5. Yenilmez E, Başaran E, Yazan Y. Release characteristics of vitamin E incorporated chitosan microspheres and in vitro–in vivo evaluation for topical application. Carbohydr Polym [Internet]. 2011; Mar 1; 84(2): 807–11. [cited 2015 Jul 9].
- 6. Lupo MP. Cosmetics. Clin Dermatol. 2001; 19(01): 467–73.
- 7. Matijević I, Bischof S, Sutlović A, Pušić T. Determination of a -tocopherol in cosmetotextiles – UV / VIS spectrophotometric method. In: Dekanić T, Tarbuk A, editors. Book of Proceedings: 8th Central European Conference on Fiber-grade Polymers, Chemical Fibers and Special Textiles. Zagreb: University of Zagreb, Faculty of Textile Technology; 2015. pp. 121–6.
- 8. Pušić T, Bischof S, Matijević I, Vujasinović E. Cellulose fabrics carriers of vitamin E. In: Frangueiro R, editor. 2nd international conference on natural fibers. Azores/Portugal: University of Minho; 2015. pp. 1–6.
- 9. Pušić T, Gujić N, Iskerka B, Matijević I, Vojnović B, & Vujasinović E. Durability of wellnes finising. In Dragčević Z, editor. Book of Proceedings: 6th International textile, clothing design conference – Magic World of Textiles. Dubrovnik: University of Zagreb, Faculty of Textile Technology; 2012. pp. 272-277.
- 10. Vujasinović E, Pušić T, Vojnović B, Matijević I, Iskerka B, Gujić N. Qualitative characterization of vitaminized cotton textiles. In Dragčević Z, editor. Book of Proceedings: 6th International textile, clothing design conference – Magic World of Textiles. Dubrovnik: University of Zagreb, Faculty of Textile Technology; 2012. pp. 601- 606.
- 11. Edison B. Analysis of Tocopherols by High Performance Liquid Chromatography. EJournal Chem [Internet]. 2009; 6(2): 395–8. Available from: http://link.springer.com/10.1385/0-89603-236-1:169
- 12. EN 12822:2014. Foodstuffs – Determination of vitamin E by high performance liquid chromatography – Measurement of α-, ß-, γ- and δ-tocopherol
- 13. Lamp AM. Analysis of tocopherols and tocotrienols by HPLC. E-Journal of Chemistry. Advance online publication (2009). Retrived from: http://lipidlibrary.aocs.org/Analysis/content.cfm?ItemNumber=40389, 05.03.2017.
- 14. Bischof S, Pušić T, Matijević I. Application of HPLC for quantification of α -tocopherol in cosmeto-cotton fabrics. In: Zimniewska M, editor. The 90th Textile Institute World Conference. Poznan: The Textile Institute, Poznan; 2016. pp. 1–9.
- 15. Hategekimana J, Zhong F. Degradation of Vitamin E in Nanoemulsions during Storage as Affected by Temperature, Light and Darkness. Int J Food Eng. 2015; 11(2): 1–8.
- 16. Solichová D, Korecká L, Svobodová I, Musil F, Bláha V, Žd’ánský P, et al. Development and validation of HPLC method for the determination of α-tocopherol in human erythrocytes for clinical applications. Anal Bioanal Chem. 2003; 376(4): 444–7.
- 17. Zu’bi ALN. Voltammetric and HPLC Determination of Some Textile Dyes By Voltammetric and HPLC Determination of Some Textile Dyes. AnـNajah National University Faculty of Graduate Studies; 2003.
- 18. Cooper J, Marchand J. Improving the Speed and Quantitative Performance for the Analysis of Allergenic and Carcinogenic Dyes in Consumer Products [Internet]. 2015. Available from: http://www.waters.com/webassets/cms/library/docs/720004492en.pdf
- 19. Jandera P, Chucácek. Gradient elution in column liquid chromatography theory and practice. Vol. 31, TrAC Trends in Analytical Chemistry. 1985. XXI.
- 20. Markovic M, Jovic M, Stankovic D, Mutic J, Roglic G, Manojlovic D. Toxicity Screening after Electrochemical Degradation of Reactive Textile Dyes. Polish J Environ Stud [Internet]. 2014; 23(6): 2103–9. Available from: http://www.pjoes.com/doi/10.15244/pjoes/28298
- 21. Anton Paar GmbH. Multiwave 3000 Microwave Platform System. 2008.nRetrived from: http://photos.labwrench.com/equipmentManuals/1807-437.pdf, 28.07.2017.
Uwagi
PL
Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).
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Bibliografia
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