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Purpose: The present work compares the hot deformation behaviour at 800°C and microstructure evolution after the isothermal compression test of hydrogen containing specimens with that of non-hydrogenated Ti-6Al-4V alloy. Design/methodology/approach: Specimens in hydrogenated and non-hydrogenated state were tested by means of isothermal compression at 800°C and strain rate of 0.005 s-1 on a Gleeble-3800 machine. Thermal hydrogen treatment of specimens in flowing hydrogen consisted of annealing 1 h at 600°C, 0.5 h at 850°C and aging 4 h at 590°C. Findings: Hydrogen contents in specimens at conditions as-received, heat treated in argon and in hydrogen and after isothermal compression test were measured using an analyzer LECO RH600. Thermal hydrogen treatment resulted in amount of hydrogen as high as 0.98 wt. %. After isothermal compression test the hydrogen content of 0.46 wt. % was retained in the specimens. Practical implications: The THT technology allows improving of fatigue and strength properties through microstructure refinement. Reversible hydrogen alloying provides decreasing flow stress and increasing hot workability of titanium alloys at lowers temperatures. Originality/value: The special heat treatment technology of Ti-based alloys, so-called the thermo hydrogen treatment (THT), employs the reversible reaction of hydrogen with titanium in order to modify phase compositions, evolution of metastable phases and kinetics of phase transformations in titanium alloys.
Wydawca
Rocznik
Tom
Strony
62--66
Opis fizyczny
Bibliogr. 9 poz.
Twórcy
autor
- Faculty of Metallurgy and Materials Engineering, VŠB - Technical University of Ostrava, Ostrava - Poruba, Czech Republic
autor
- Faculty of Metallurgy and Materials Engineering, VŠB - Technical University of Ostrava, Ostrava - Poruba, Czech Republic
autor
- Faculty of Metallurgy and Materials Engineering, VŠB - Technical University of Ostrava, Ostrava - Poruba, Czech Republic
Bibliografia
- [1] M. Niiomi, Mechanical biocompatibilities of titanium alloys for biomedical applications, Journal of the Mechanical Behavior of Biomedical Materials 1/1 (2008) 30-42.
- [2] O.N. Senkov, F.H. Froes, Thermohydrogen processing of titanium alloys, International Journal of Hydrogen Energy 24 (1999) 565-576.
- [3] J.I. Qazi, O.N. Senkov, J. Rahim, A. Genc, F.H. Froes, Phase Transformations in Ti-6Al-4V-xH Alloys, Metallurgical and Materials Transactions A32/10 (2001) 2453-2463.
- [4] N. Eliaz, D. Elizier, D.L. Olson, Hydrogen-assisted processing of materials, Materials Science and Engineering A289/1-2 (2000) 41-53.
- [5] M.Q. Li, J. Luo, Y. Niu, Effect of the hydrogen content on the deformation behavior in the isothermal compression of Ti600 alloy, Materials Science and Engineering A527/24-25 (2010) 6626-6632.
- [6] J. Zhao, H. Ding, Y. Wang, H. Hou, Influence of thermo hydrogen treatment on hot deformation behavior of Ti600 alloy. Transactions of Nonferrous Metals Society of China 19/1 (2009) 65-71.
- [7] D.L. Sun, Q. Wang, X.L. Han, J.X. Xiao, D.P. Jiang, Influence of hydrogen on hot deformation behavior and microstructure of pure titanium, Proceedings of the 11th International Conference “Mechanical Behavior of Materials” ICM11, in: Procedia Engineering 10 (2011) 42-47.
- [8] M.A. Murzinova, M.I. Mazurski, G.A. Salishchev, D.D. Afonichev, Application of reversible hydrogen alloying for formation of submicrocrystalline structure in (alpha + beta) titanium alloys, Proceedings of the Selected Papers of the 1st International Conference “Hydrogen Treatment of Materials”, in: International Association for Hydrogen Energy 22/2-3 (1997) 201-204.
- [9] T.Y. Fang, W.H. Wang, Microstructural features of thermo mechanical processing in a Ti-6Al-4V alloy, Materials Chemistry and Physics 56 (1998) 35-47.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-9d0c857b-2f3f-4fd5-a0c7-acdb6805c76b