Multi-objective optimization of the green extraction conditions of bio-active compounds from a levisticum officinale WDJ Koch: Pareto optimality and compromise solutions for process management

• Autorzy: Plawgo Michał , Kocira Sławomir , Bohata Andrea

Identyfikatory

DOI

10.2478/agriceng-2024-0010

Warianty tytułu

PL

Wieloobiektowa optymalizacja warunków zielonej ekstrakcji związków bioaktywnych z Levisticum officinale WDJ Koch: optymalność Pareto i rozwiązania kompromisowe w zarządzaniu procesami

• Języki publikacji: EN

Abstrakty

EN

Plants belonging to the Apiaceae family (including Levisticum officinale WDJ Koch) are rich sources of phytochemicals and secondary metabolites, with possible health-promoting and agrochemical potential. The objective of this work was to provide important guidelines for controlling conventional aqueous extraction to obtain Levisticum officinale root extracts with maximised levels of bioactive compounds. The ultimate goal was to optimise the total phenolic compounds, flavonoid content, sugars, and total antioxidant capacity to identify the process conditions necessary to produce highly bioactive extracts that could be used in a wide range of industries. Biomass extraction of lovage root was carried out using water as the extraction solvent. To perform the optimisation of the aqueous extraction, multivariate regression models were used and multi-criteria analysis was performed using Pareto set navigation. Pareto front analysis showed that for the maximum extraction efficiency of bioactive compounds from Levisticum officinale, the optimal extraction process parameters were 0.0714 g⸱mL^-1 as biomass/water ratio and a time of 35.7142 min, at the highest analysed temperature. For the highest analysed value of plant biomass/solvent ratio (0.075 g⸱mL^-1) and maximum process temperature (95ºC), extraction could be carried out for 20 min or in the range 37.1429-38.5714 min. On the other hand, if the extraction time reaches 40 min and the sam-ple/solvent ratio 0.075 g⸱mL^-1, the optimum process temperature is be-tween 75ºC and 95ºC.

PL

Rośliny należące do rodziny Apiaceae (w tym Levisticum officinale WDJ Koch) są bogatym źródłem fitochemikaliów i metabolitów wtórnych o potencjalnym potencjale prozdrowotnym i agrochemicznym. Celem niniejszej pracy było dostarczenie ważnych wytycznych dotyczących kontrolowania konwencjonalnej ekstrakcji wodnej w celu uzyskania ekstraktów z korzenia Levisticum officinale o zmaksymalizowanych poziomach związków bioaktywnych. Dlatego też w niniejszym badaniu oceniono i zoptymalizowano potencjał przeciwutleniający wodnych ekstraktów z Levisticum officinale pod kątem analizy wpływu parametrów procesu ekstrakcji, tj. temperatury, czasu i stosunku biomasy roślinnej do rozpuszczalnika. Ostatecznym celem była optymalizacja całkowitej zawartości związków fenolowych, flawonoidów, cukrów i całkowitej zdolności przeciwutleniającej w celu zidentyfikowania warunków procesu niezbędnych do wytworzenia wysoce bioaktywnych ekstraktów, które mogłyby być stosowane w wielu gałęziach przemysłu. Ekstrakcję biomasy korzenia lubczyku przeprowadzono przy użyciu wody jako rozpuszczalnika ekstrakcyjnego. Aby przeprowadzić optymalizację ekstrakcji wodnej, zastosowano wielowymiarowe modele regresji i przeprowadzono analizę wielokryterialną przy użyciu nawigacji zestawu Pareto.Procedury optymalizacyjne wykazały dużą złożoność rozważanego problemu badawczego, co bezpośrednio utrudnia wybór jednego najlepszego rozwiązania. W związku z tym wyznaczono zbiory rozwiązań. Analiza frontu Pareto wykazała, że dla maksymalnej wydajności ekstrakcji związków bioaktywnych z Levisticum officinale, optymalnymi parametrami procesu ekstrakcji były 0,0714 g⸱ml^-1 jako stosunek biomasy do wody oraz czas 35,7142 min, w najwyższej analizowanej temperaturze. Dla najwyższej analizowanej wartości stosunku biomasy roślinnej do rozpuszczalnika (0,075 g⸱ml^-1) i maksymalnej temperatury procesu (95ºC), ekstrakcję można było prowadzić przez 20 min lub w zakresie 37,1429-38,5714 min. Z drugiej strony, jeśli czas ekstrakcji osiągnie 40 min, a stosunek próbki do rozpuszczalnika 0,075 g⸱ml^-1, optymalna temperatura procesu wynosi od 75ºC do 95ºC.

Słowa kluczowe

EN

water extraction; modeling; optimization; Pareto optimality; lovage

PL

ekstrakcja wodą; modelowanie; optymalizacja; optymalność Pareto; lubczyk

• Wydawca: Polskie Towarzystwo Inżynierii Rolniczej
• Czasopismo: Agricultural Engineering
• Rocznik: 2024
• Tom: Vol. 28, No. 1
• Strony: 137--165
• Opis fizyczny: Bibliogr. 55 poz., rys., tab.

Twórcy

autor

Plawgo Michał

• Future Production AS, Svanedamsveien 10, 4621 Kristiansand, Norway

• https://orcid.org/0009-0004-2902-285X

autor

Kocira Sławomir

• Department of Machinery Exploitation and Management of Production Processes, University of Life Sciences in Lublin, Akademicka 13, 20-950 Lublin, Poland
• Department of Landscape Management, Faculty of Agriculture and Technology, University of South Bohe-mia in České Budějovice, České Budějovice, 370 05, Czech Republic

• https://orcid.org/0000-0002-2888-3023

autor

Bohata Andrea

• Department of Plant Production, Faculty of Agriculture and Technology, University of South Bohemia in České Budějovice, České Budějovice, 370 05, Czech Republic

• https://orcid.org/0000-0002-3646-5366

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