Exploration of the possibility of combined HS-GC-MS and 13C NMR spectroscopic investigation of the composition of the essential oils of selected sage (Salvia) species

• Autorzy: Sajewicz M. , Matlengiewicz M. , Rzepa J. , Wojtal Ł. , Hajnos M. , Waksmundzka-Hajnos M. , Kowalska T.
• Języki publikacji: EN

Abstrakty

EN

The objective of this study was to explore the possibility of combining headspace gas chromatography with mass spectrometric detection (HS-GC-MS) and ¹³C NMR spectroscopy to enhance the detectability of components of the essential oils of medicinal plants of the Salvia genus. Preliminary investigations were performed with two sage species, Salvia lavandulifolia and Salvia triloba, known for particularly abundant yields of their respective essential oils. By use of HS-GC-MS, characteristic fingerprints of the volatile fractions were obtained for plant species from two different vegetation seasons (2007 and 2008). Partial identification of the components of these volatile fractions was performed, and comparison of the chromatographic fingerprints confirmed seasonal fingerprint similarity within the same species. Preliminary ¹³C NMR measurements resulted in well shaped spectra with an abundance of regularly distributed signals. This suggested the possibility of using ¹³C NMR spectroscopy in phytochemical research, in parallel with HS-GC-MS, to enhance the detectability of volatile components of plant species belonging to this genus.

Słowa kluczowe

EN

essential oils; Salvia lavandulifolia; Salvia triloba; headspace-gas chromatography-mass spectrometry; 13C NMR spectroscopy

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2011
• Tom: Vol. 23, no. 1
• Strony: 181--190
• Opis fizyczny: Bibliogr. 16 poz., rys., tab.

Twórcy

autor

Sajewicz M.

• University of Silesia Institute of Chemistry 9 Szkolna Street 40-006 Katowice Poland

autor

Matlengiewicz M.

• University of Silesia Institute of Chemistry 9 Szkolna Street 40-006 Katowice Poland
• Centre of Polymer and Carbon Materials Polish Academy of Sciences 5 Sowińskiego Street 44-121 Gliwice Poland

autor

Rzepa J.

• University of Silesia Institute of Chemistry 9 Szkolna Street 40-006 Katowice Poland

autor

Wojtal Ł.

• University of Silesia Institute of Chemistry 9 Szkolna Street 40-006 Katowice Poland

autor

Hajnos M.

• Medical University of Lublin Department of Pharmacognosy 1 Chodźki Street 20-093 Lublin Poland

autor

Waksmundzka-Hajnos M.

• Medical University of Lublin Department of Inorganic Chemistry 6 Staszica Street 20-081 Lublin Poland

autor

Kowalska T.

• University of Silesia Institute of Chemistry 9 Szkolna Street 40-006 Katowice Poland

Bibliografia

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