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Materiały kompozytowe umacniane preformami wytworzonymi w procesie wysokotemperaturowej syntezy w polu mikrofalowym

Autorzy
Naplocha K.
Identyfikatory
Warianty tytułu
EN
Composite materials reinforced with preforms manufactured by high temperature synthesis in microwave field
Języki publikacji
PL
Abstrakty
PL
Przedstawiono problematykę wytwarzania materiałów kompozytowych metodą infiltracji ciśnieniowej obejmującą przygotowanie porowatych preform, nagrzewanie mikrofalowe, prasowanie ze stanu ciekłego oraz badania podstawowych właściwości mechanicznych. Zaadaptowano samorozprzestrzeniającą się syntezę wysokotemperaturową SHS do wytwarzania preform z faz międzymetalicznych typu Al-Ni, Al-Cr, Al-Ti, związków zawierających tlenowęgliki Ti-O-C, węgliki TiC oraz fazy Ti-C-Al. Przeprowadzono badania możliwości wykorzystania nagrzewania mikrofalowego do inicjowania i wspomagania syntezy. Zaprojektowano i zbudowano prototypowy rektor mikrofalowy umożliwiający intensywne nagrzewanie rozdrobnionych materiałów meta-liczno-ceramicznych wraz z precyzyjnym pomiarem temperatury zachodzących zjawisk fizykochemicznych. Opracowano parametry syntezy objętościowej oraz syntezy w strumieniu reaktywnego gazu materiałów porowatych, analizując sposób kształtowania struktury i zachodzących przemian fazowych. Określono wpływ ziarnistości proszków, składu chemicznego mieszaniny wyjściowej oraz mocy promieniowania mikrofalowego na przebieg syntezy i mikrostrukturę produktów. Przedstawiono metody rozwinięcia porowatości otwartej dla wybranych układów. Przeprowadzono analizę parametrów prasowania ze stanu ciekłego (ang. squeeze casting), dobierając je do infiltracji preform o małej porowatości i wytrzymałości. Prowadzono badana mikroskopowe połączone z identyfikacją fazową preform oraz materiałów kompozytowych. Analizowano stopień jednorodności struktury, rodzaj porowatości oraz jakość połączenia umocnienia z osnową. Opracowano parametry obróbki cieplnej mającej na celu ujednorodnienie struktury, a także przekształcenie nasyconych faz umacniających. Materiały kompozytowe umocnione wyselekcjonowanymi preformami poddano badaniom twardości, wytrzymałości na rozciągane, rozszerzalności cieplnej i odporności na zużycie. Przede wszystkim zaobserwowano istotny wzrost twardości, poprawę stabilności wymiarowej oraz odporności na ścieranie w warunkach tarcia suchego.
EN
Researches of pressure infiltrated composite materials included preparation of porous preform, mi-crowave heating, squeeze casting and determination of fundamental mechanical properties was presented. Self-propagation high temperature synthesis SHS was adopted for production of preforms from Al-Ni, Al-Cr, Al-Ti intermetallic phases, compounds containing Ti-O-C oxycarbides, TiC carbides and Ti-C-Al phases. The possibility of using microwave heating to initiate and support synthesis was studied. Designed and built a prototype microwave rector allows intense heating of powdered metallic-ceramic materials with precise temperature measurement of proceeded physical and chemical phenomena. Parameters of volume synthesis and synthesis in reactive gas stream for porous materials were elaborated with simultaneous analysis of structure development and phase transitions. Moreover influence of particle size powders, the chemical composition of the starting mixture and the power of microwave radiation on the course of the synthesis and microstructure of the products were determined. For selected systems to develop open porosity appropriate method was applied. Next squeeze casting parameters were established to infiltrate preform characterised low porosity and strength. In this area investigation related to the micro-structure homogeneity, porosity and reinforcement-matrix interface analysis. Elaborated heat treatment parameters allows improving microstructure and transforming infiltrated reinforcing phases. Composite materials reinforced with selected preforms were subjected to hardness, tensile strength, thermal expansion and wear examinations. First of all significant increase of hardness, where resistance and thermal stability were observed.
Słowa kluczowe
PL
Wydawca
Oficyna Wydawnicza Politechniki Wrocławskiej
Czasopismo
Prace Naukowe Instytutu Technologii Maszyn i Automatyzacji Politechniki Wrocławskiej. Monografie
Rocznik
2013
Tom
Vol. 89, nr 29
Strony
164--164
Opis fizyczny
Bibliogr. 174 poz., tab., rys.
Twórcy
autor
Naplocha K.
krzysztof.naplocha@pwr.wroc.pl
  • Instytut Technologii Maszyn i Automatyzacji Politechniki Wrocławskiej, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław
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