Evaluation of the Possibility of Applying Spatial 3D Imaging Using X-Ray Computed Tomography Reconstruction Methods for Quantitative Analysis of Multiphase Materials

• Autorzy: Matysik P. , Chojnacki M. , Jóźwiak S. , Czujko T. , Lipiński S.

Identyfikatory

DOI

10.1515/amm-2015-0430

Warianty tytułu

PL

Rentgenowska analiza ilościowa materiałów wielofazowych z wykorzystaniem przestrzennego obrazowania (3D) przy użyciu metod rekonstrukcji tomografii komputerowej

• Języki publikacji: EN

Abstrakty

EN

In this paper the possibility of using X-ray computed tomography (CT) in quantitative metallographic studies of homogeneous and composite materials is presented. Samples of spheroidal cast iron, Fe-Ti powder mixture compact and epoxy composite reinforced with glass fibers, were subjected to comparative structural tests. Volume fractions of each of the phase structure components were determined by conventional methods with the use of a scanning electron microscopy (SEM) and X-ray diffraction (XRD) quantitative analysis methods. These results were compared with those obtained by the method of spatial analysis of the reconstructed CT image. Based on the comparative analysis, taking into account the selectivity of data verification methods and the accuracy of the obtained results, the authors conclude that the method of computed tomography is suitable for quantitative analysis of several types of structural materials.

PL

W pracy przedstawiono możliwość wykorzystania rentgenowskiej tomografii komputerowej (CT) w ilościowych badaniach metalograficznych materiałów jednorodnych oraz kompozytowych. Badaniom porównawczym poddano wypraskę mieszaniny proszkowej Fe – Ti, żeliwo sferoidalne, a także kompozyt epoksydowy zbrojony włóknami szklanymi. Udział objętościowy poszczególnych składników strukturalnych określano za pomocą klasycznych metod stereologicznych z wykorzystaniem skaningowej mikroskopii elektronowej (SEM) oraz metodami rentgenowskiej analizy ilościowej (XRD). Uzyskane typowymi metodykami wyniki porównano z rezultatami otrzymanymi za pomocą metody przestrzennej analizy obrazu tomografii komputerowej. Na podstawie przeprowadzonych analiz, biorąc pod uwagę selektywny sposób weryfikacji danych oraz dokładność uzyskiwanych wyników, można stwierdzić przydatność wykorzystania metody tomografii komputerowej, w obszarze ilościowej analizy strukturalnej szerokiego spektrum materiałów konstrukcyjnych.

Słowa kluczowe

EN

computed tomography; electron microscopy; X-ray diffraction; stereology; phase analysis; quantitative research

PL

tomografia komputerowa; mikroskopia elektronowa; dyfrakcja rentgenowska; stereologia; analiza fazy; badania ilościowe

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2015
• Tom: Vol. 60, iss. 4
• Strony: 2663--2670
• Opis fizyczny: Bibliogr. 22 poz., rys.

Twórcy

autor

Matysik P.

• Military University of Technology, Department of Advanced Materials and Technologies, Faculty of Advanced Technologies and Chemistry ,2 Gen. S. Kaliskiego Str., 00-908 Warsaw, Poland

autor

Chojnacki M.

• Institute of Physics of the Polish Academy of Sciences, Group of Spectroscopy and Thermal Properties of Magnetic Materials, Division of Physics of Magnetism, 32/46 Lotników Av., 02-668 Warsaw, Poland

autor

Jóźwiak S.

• Military University of Technology, Department of Advanced Materials and Technologies, Faculty of Advanced Technologies and Chemistry, 2 Gen. S. Kaliskiego Str., 00-908 Warsaw, Poland

autor

Czujko T.

• Military University of Technology, Department of Advanced Materials and Technologies, Faculty of Advanced Technologies and Chemistry, 2 Gen. S. Kaliskiego Str., 00-908 Warsaw, Poland

autor

Lipiński S.

• Military University of Technology, Department of Advanced Materials and Technologies, Faculty of Advanced Technologies and Chemistry, 2 Gen. S. Kaliskiego Str., 00-908 Warsaw, Poland

Bibliografia

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Uwagi

PL

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.