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Optimization and Characterization Pectin Extraction from Rosy-Pulped Pomelo Using Ethanol Precipitation Method

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The goal of this study is to use a simple approach to synthesize pectin from grapefruit peel, an agricultural waste common in tropical regions. Additionally, the study employed optimization techniques to identify the ideal conditions for the maximum extraction efficiency while also determining the importance of studying factors. Besides, extracted pectin characteristics are also presented in this research. Under several analysis, some chemical groups for pectin were presented in extracted pectin by Fourier transform infrared spectroscopy analysis (FTIR). For instance, C-H methyl groups at the peak 1442 cm-1; methyl ester groups C=O appears at the wavelength 1747 cm-1 and aliphatic C-H groups and hydroxyl groups. Furthermore, under three major conditions acid (%); temperature and time extraction, an optimization study was conducted to figure out the optimal conditions for pectin extraction efficiency. Under optimal conditions acid 10%; 77.5 °C and 80 mins is the favorable condition for obtaining pectin extraction efficiency. Basically, this study is the first one extracting pectin from rosy-pulp pomelo peel by sulfuric acid-ethanol precipitation method. This is a preliminary that lays the foundation for purifying extracted pectin from rosy-pulp pomelo, also solving this agricultural waste bring higher economic values.
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Twórcy
autor
  • HaUI Institute of Technology, Hanoi University of Industry, No. 298 Cau Dien Street, Bac Tu Liem District, Hanoi, Vietnam
  • HaUI Institute of Technology, Hanoi University of Industry, No. 298 Cau Dien Street, Bac Tu Liem District, Hanoi, Vietnam
Bibliografia
  • 1. Analese R.B., Carolia A.C., Man-Wah L., Hon-Ming L., Kong A.H., Pilar E.U., Maria C.R. 2023. Pectin: An overview of sources, extraction and application in food products, biomedical, pharmaceutical, and environmental issues. Food Chemistry Advances, 2, 100192. https://doi.org/10.1016/j.focha.2023.100192
  • 2. Ana K.T., Luis A.G., Fabricio E., Rosa M.R.Z., Irma R. 2019. Optimization of the integral valorization process for orange peel waste using a design of experiments approach: production of high-quality pectin and activated carbon. Waste Management, 85, 202–213. https://doi.org/10.1016/j.wasman.2018.12.029
  • 3. Didem D., Seda C., Dilek G., Nimet B. 2021. Extraction of pectin from albedo of lemon peels for preparation of tissue engineering scaffolds. Polymer Bulletin, 78, 4. https://link.springer.com/article/10.1007/s00289-020-03208-1
  • 4. Elnaz C., Faramarz K., Seyed S.H. 2017. Optimization of pectin extraction from pistachio green hull as a new source. Carbohydrate Polymers, 173, 107– 113. https://doi.org/10.1016/j.carbpol.2017.05.047
  • 5. Licelander H., Walter M.A., Juliana V.C., Isabel C.P.A. 2021. Enzymatic extraction and characterization of pectin from cocoa pod husks (Theobroma cacao L.) using celluclast 1.5L. Melocules, 26(5), 1473. http://dx.doi.org/10.3390/molecules26051473
  • 6. Luiz B.S.F., Ronaldo C.C., Edvani C.M., Herbert D.S.B. 2022. Optimization of pectin extraction using response surface methodology: A bibliometric analysis. Carbohydrate Polymer Technologies and Applications, 4, 100229. https://doi.org/10.1016/j.carpta.2022.100229
  • 7. Nasrul W., Chu Y.S., Wong Y S., Tina R., Bayu I., Rimadani P., Muchtaridi M. 2019. Characterization, and antioxidant activity of pectin from Indonesian magosteen (Garcinia mangostana L.) rind. Heliyon, 5(8), e02299. http://dx.doi.org/10.1016/j.heliyon.2019.e02299
  • 8. Muhammad H.S., Rizana Y., Chee Y.G. 2019. Deep eutectic solvents (DES) mediated: extraction of pectin from Averrhoa bilimbi: Optimization and characterization studies. Carbohydrate Polymers, 216, 303–311. https://doi.org/10.1016/j.carbpol.2019.04.007
  • 9. Sayed S.H., Faramarz K., Mohammad S.Y. 2016. Aqueous extraction of pectin from sour orange peel and its preliminary physicochemical properties. International Journal of Biological Macromolecules, 82, 920–926. https://doi.org/10.1016/j.ijbiomac.2015.11.007
  • 10. Seyed H.P., Maryam J.M., Mirian P., Jose M.L., Ruben D.V. 2021. Physicochemical, thermal, and rheological properties of pectin extracted from sugar beet pulp using subcritical water extraction process. Molecules, 26(5), 1413.
  • 11. Ricardo F.C., Boeun K., Paloma A. S., Jens A., Jay H.L., Jakob K.H. 2019. Analysis and model-based optimization of a pectin extraction process. Journal of Food Engineering, 224, 159–169. https://doi.org/10.1016/j.jfoodeng.2018.09.016
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-8fe1d485-c758-46ec-b232-9924d38292b4
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