Development of HPLC method for determination of phenolic compounds on a core shell column by direct injection of wine samples

• Autorzy: Krstonošić Milica , Hogervorst Jelena , Mikulić Mira , Gojković-Bukarica Ljiljana

Identyfikatory

DOI

10.1556/1326.2019.00611

• Języki publikacji: EN

Abstrakty

EN

Phenolic compounds are frequently present in various natural products, and they can have different beneficial biological potentials. The most widely used method for determination of individual phenolic compounds is high-performance liquid chromatography (HPLC). In this paper, a method for simultaneous determination of 16 phenolic compounds (gallic acid, p-hydroxybenzoic acid, catechin, syringic acid, trans-cinnamic acid, hesperetin, naringenin, vanillic acid, benzoic acid, coumaric acid, resveratrol, chlorogenic acid, caffeic acid, rutin, quercetin, and kaempferol) on a core–shell column was developed. The separation method conducted on a standard ODS (250 mm) column was transferred to Poroshell column and optimized using non-ultra-high-performance liquid chromatography (UHPLC) apparatus. Phenolic compounds were separated fast and efficiently during 30-min analysis, and validation parameters were determined. The developed method was successfully applied on the analysis of phenolic content after direct injection of red wines from three different grape varieties.

Słowa kluczowe

EN

HPLC; core shell column; phenolies; wine

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2020
• Tom: Vol. 32, no. 2
• Strony: 134--138
• Opis fizyczny: Bibliogr. 35 poz., rys.

Twórcy

autor

Krstonošić Milica

• University of Novi Sad, Hajduk Veljkova 3, 21000 Novi Sad, Serbia

autor

Hogervorst Jelena

• University of Novi Sad, Hajduk Veljkova 3, 21000 Novi Sad, Serbia

autor

Mikulić Mira

• University of Novi Sad, Hajduk Veljkova 3, 21000 Novi Sad, Serbia

autor

Gojković-Bukarica Ljiljana

• University of Belgrade, P.O. Box 840, 11129 Belgrade, Serbia

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Uwagi

PL

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).