Surface modification of nano-TiN by using silane coupling agent

• Autorzy: Cheng G. , Luo J. , Qian J. , Miao J

Identyfikatory

DOI

10.2478/s13536-013-0175-8

• Języki publikacji: EN

Abstrakty

EN

Titanium nitride (TiN) nano-particles were subjected to graft modification by silane coupling agent (KH-570) via a direct blending method. The hydroxyl groups on the surface of TiN nano-particles can interact with silanol groups [–Si–OCH3] of KH-570 forming an organic coating layer. The covalent bonds (Ti–O–Si) formation was testified by Fourier transform infrared spectra (FTIR) and X-ray photoelectron spectroscopy (XPS). Through transmission electron micrograph (TEM) observations, it was found that KH-570 could improve the dispersibility of nano-TiN particles in ethyl acetate. Thermo gravimetric analysis (TGA) and contact angle measurements indicated that KH-570 molecules were adsorbed or anchored on the surface of nano-TiN particle and the net efficiency of it was 22.76 %, which facilitated to hinder the aggregation of nano-TiN particles.

Słowa kluczowe

EN

nano titanium nitride; silane coupling agents; surface modification; dispersion

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2014
• Tom: Vol. 32, No. 2
• Strony: 214--219
• Opis fizyczny: Bibliogr. 32 poz., rys., wykr.

Twórcy

autor

Cheng G.

• School of Chemistry and Chemical Engineering, Anhui University
• School of Materials Science and Engineering, Anhui Uniersity of Science and Technology

autor

Luo J.

• School of Chemistry and Chemical Engineering, Anhui University

autor

Qian J.

• School of Chemistry and Chemical Engineering, Anhui University

autor

Miao J

• School of Chemistry and Chemical Engineering, Anhui University

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