Development of ultrasound-assisted extraction followed by solid-phase extraction followed by dispersive liquid–liquid microextraction followed by gas chromatography for the sensitive determination of diazinon in garden parsley as vegetable samples

• Autorzy: Rezaee Mohammad , Khalilian Faezeh , Pourjavid Mohammad Reza

Identyfikatory

DOI

10.1556/1326.2022.01086

• Języki publikacji: EN

Abstrakty

EN

A new pretreatment method termed ultrasound-assisted extraction (UAE) which is combined with solid-phase extraction which is combined with dispersive liquid-liquid microextraction (SPE-DLLME) followed by gas chromatography-flame ionization detector (GC-FID) analysis has been developed for the determination of diazinon in garden parsley as vegetable samples. The analyte was extracted from garden parsley sample using ultrasound-assisted extraction followed by solid-phase extraction followed by dispersive liquid-liquid microextraction. Various parameters that affect the efficiency of the extraction techniques have been optimized. The calibration plot was linear in the range of 5.0–1,000 μg kg⁻¹ with detection limit of 1.0 μg kg⁻¹ for diazinon in garden parsley samples. The results confirm the suitability of the UAE-SPE-DLLME-GC-FID as a sensitive method for the analysis of the targeted analyte in garden parsley samples.

Słowa kluczowe

EN

diazinon; ultrasound-assisted extraction; dispersive liquid-liquid microextraction; gas chromatography; garden parsley samples

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2023
• Tom: Vol. 35, no. 4
• Strony: 347--353
• Opis fizyczny: Bibliogr. 20 poz., rys., tab., wykr.

Twórcy

autor

Rezaee Mohammad

• Nuclear Fuel Cycle Research School, Nuclear Science and Technology Research Institute, Tehran, Iran

• https://orcid.org/0000-0002-8093-4588

autor

Khalilian Faezeh

• Department of Chemistry, College of Basic Science, Yadegar -e- Imam Khomeini (RAH) Shahre Rey Branch, Islamic Azad University, Tehran, Iran

autor

Pourjavid Mohammad Reza

• Nuclear Fuel Cycle Research School, Nuclear Science and Technology Research Institute, Tehran, Iran

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