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The SEM and EDS results of porous coatings formed on pure titanium by Plasma Electrolytic Oxidation (Micro Arc Oxidation) under DC regime of voltage in the electrolytes containing of 500 g zinc nitrate Zn(NO3)2·6H2O in 1000 mL of concentrated phosphoric acid H3PO4 at three voltages, i.e. 450 V, 550 V, 650 V for 3 minutes, are presented. The PEO coatings with pores, which have different shapes and the diameters, consist mainly of phosphorus, titanium and zinc. The maximum of zinc-to-phosphorus (Zn/P) ratio was found for treatment at 650 V and it equals 0.43 (wt%) | 0.20 (at%), while the minimum of that coefficient was recorded for the voltage of 450 V and equaling 0.26 (wt%) | 0.12 (at%). Performed studies have shown a possible way to form the porous coatings enriched with zinc by Plasma Electrolytic Oxidation in electrolyte containing concentrated phosphoric acid H3PO4 with zinc nitrate Zn(NO3)2·6H2O.
Wydawca
Czasopismo
Rocznik
Strony
41--54
Opis fizyczny
Bibliogr. 60 poz., rys., wykr., tab.
Twórcy
autor
- Koszalin University of Technology, Faculty of Mechanical Engineering, Department of Engineering and Informatics Systems, Division of Bioengineering and Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland
autor
- Koszalin University of Technology, Faculty of Mechanical Engineering, Department of Engineering and Informatics Systems, Division of Bioengineering and Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland
autor
- Koszalin University of Technology, Faculty of Mechanical Engineering, Department of Engineering and Informatics Systems, Division of Bioengineering and Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland
autor
- Hochschule Wismar-University of Applied Sciences Technology, Business and Design, Faculty of Engineering, D 23966 Wismar, Germany
Bibliografia
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- 25. Hryniewicz T., Rokosz K., Valiček J., Rokicki R., Effect of magnetoelectropolishing on nanohardness and Young’s modulus of titanium biomaterial, Materials Letters, 83 (2012), 69-72.
- 26. Hryniewicz T., Rokosz K., Rokicki R., Prima F., Nanoindentation and XPS Studies of Titanium TNZ Alloy after Electrochemical Polishing in a Magnetic Field, Materials, 8 (2015), 205-215.
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- 28. Rokosz K., Hryniewicz T., XPS Analysis of nanolayers obtained on AISI 316L SS after Magnetoelectropolishing, World Scientific News, 37 (2016), 232-248.
- 29. Rokicki R., Hryniewicz T., Konarski P., Rokosz K., The alternative, novel technology for improvement of surface finish of SRF niobium cavities, World Scientific News, 74 (2017), 152-163.
- 30. Rokosz K., Hryniewicz T., Simon F., Rzadkiewicz S., Comparative XPS analysis of passive layers composition formed on AISI 304 L SS after standard and high-current density electropolishing, Surface and Interface Analysis, 47(1) (2015), 87-92.
- 31. Rokosz K., Lahtinen J., Hryniewicz T., Rzadkiewicz S., XPS depth profiling analysis of passive surface layers formed on austenitic AISI 304L and AISI 316L SS after high-current-density electropolishing, Surface and Coatings Technology, 276 (2015), 516-520.
- 32. Rokosz K., Hryniewicz T., Simon F., Rzadkiewicz S., Comparative XPS analyses of passive layers composition formed on duplex 2205 SS after standard and high-current-density electropolishing, Tehničkivjesnik - Technical Gazette, 23(3) (2016), 731-735.
- 33. Gnedenkov S.V., Sharkeev Y.P., Sinebryukhov S.L., Khrisanfova O.A., Legostaeva E.V., Zavidnaya A.G., Puz’ A.V., Khlusov I.A., Opra D.P., Functional coatings formed on the titanium and magnesium alloys as implant materials by plasma electrolytic oxidation technology: fundamental principles and synthesis conditions, Corrosion Review, 34(1-2) (2016), 65-83.
- 34. Simka W., Sadowski A., Warczak M., Iwaniak A., Dercz G., Michalska J., Maciej A., Modification of titanium oxide layer by calcium and phosphorus, ElectrochimicaActa, 56(24) (2011), 8962-8968.
- 35. Han Y., Hong S.H., Xu K.W., Synthesis of nanocrystallinetitania films by micro-arc oxidation, Materials Letters, 56 (2002), 744-747.
- 36. Han Y., Hong S.H., Xu K.W., Structure and in vitro bioactivity of titania-based films by microarc oxidation, Surface and Coatings Technology, 168 (2003), 249-258.
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- 38. Aliasghari S., Plasma Electrolytic Oxidation of Titanium, PhD Thesis of Faculty of Engineering and Physical Sciences, The University of Manchester School of Materials, (2014), 223 pages.
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- 40. Krzakala A., Mlynski J., Dercz G., Michalska J., Maciej A., Nieuzyla L., Simka W, Modification of Ti-6Al-4V alloy surface by EPD-PEO process in ZrSiO4 suspension, Archives of Metallurgy and Materials, 59(1) (2014), 199-204.
- 41. Simka W., Nawrat G., Chlode J., Maciej A., Winiarski A., Szade J., Radwanski K., Gazdowicz J., Electropolishing and anodic passivation of Ti6Al7Nb alloy, PrzemysłChemiczny, 90(1) (2011), 84-90.
- 42. Wang Y., Jiang B., Lei T., Guo L., Dependence of growth features of microarc oxidation coatings of titanium alloy on control modes of alternate pulse, Materials Letters, 58 (2004), 1907-1911.
- 43. Rokosz K., Hryniewicz T., Raaen S., Development of Plasma Electrolytic Oxidation for improved Ti6Al4V biomaterial surface properties, The International Journal of Advanced Manufacturing Technology, 85 (2016), 2425-2437.
- 44. Rokosz K., Hryniewicz T., Raaen S., Chapon P., Investigation of porous coatings obtained on Ti-Nb-Zr-Sn alloy biomaterial by Plasma Electrolytic Oxidation: Characterisation and Modelling, The International Journal of Advanced Manufacturing Technology, 87(9) (2016), 3497–3512.
- 45. Rokosz K., Hryniewicz T., Raaen S., Chapon P., Development of copper-enriched porous coatings on ternary Ti-Nb-Zr alloy by Plasma Electrolytic Oxidation, The International Journal of Advanced Manufacturing Technology, 89(9) (2017), 2953–2965.
- 46. Rokosz K., Hryniewicz T., Characteristics of porous and biocompatible coatings obtained on Niobium and Titanium-Niobium-Zirconium (TNZ) alloy by Plasma Electrolytic Oxidation, Mechanik, 12 (2015),15-18.
- 47. Rokosz K., Hryniewicz T., Dudek Ł., Matysek D., Valiček J., Harničarova M., SEM and EDS Analysis of Surface Layer Formed on Titanium After Plasma Electrolytic Oxidation in H3PO4 with the Addition of Cu(NO3)2, Journal of Nanoscience and Nanotechnology, 16(8) (2016), 7814-7817.
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- 49. Rokosz K., Hryniewicz T., Raaen S., Chapon P., Dudek Ł., GDOES, XPS and SEM with EDS analysis of porous coatings obtained on Titanium after Plasma Electrolytic Oxidation, Surface and Interface Analysis, 49(4) (2016), 303-315.
- 50. Rokosz K., Hryniewicz T., Chapon P., Dudek Ł., A new approach to porous PEO coating sublayers determination on the basis of GDOES signals, World Scientific News, 57 (2016), 289-299.
- 51. Rokosz K., Hryniewicz T., Chapon P., Raaen S., ZschommlerSandim H.R., XPS and GDOES characterisation of porous coating enriched with copper and calcium obtained on Tantalum via Plasma Electrolytic Oxidation, Journal of Spectroscopy, Article ID 7093071 (2016) (7 pages); http://dx.doi.org/10.1155/2016/7093071
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Uwagi
PL
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-8a00de8f-4d1a-48c8-88b4-c5619f6d010d