Synthesis and 3D-AFM surface topology of nanographene-like material extracted from sulfonated tri-, di- and monochloroacetic acid

Elsabawy, K. M.

doi:10.1515/msp-2016-0081

Artykuł - szczegóły

Tytuł artykułu

Synthesis and 3D-AFM surface topology of nanographene-like material extracted from sulfonated tri-, di- and monochloroacetic acid

Autorzy

Elsabawy K. M.

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.1515/msp-2016-0081

Warianty tytułu

Języki publikacji

Abstrakty

In this study a graphene-like material was synthesized by chemical exfoliation of sieved graphite powder with an average particles size ≤100 µm in dispersing medium from tri-, di- and monochloroacetic acid sulfonated with 55 % H₂SO₃. The results indicated that the yield of graphene-like material was the best in case of trichloroacetic 55 % H₂SO₃, taking into account structure quality and amount of obtained material. Layered graphene-like material was carefully collected after reduction of GO formed by 50 % dimethylhydrazine. AFM-investigations were performed to characterize nanostructural features of produced graphene and expected surface area which is surface topology dependent. Furthermore, Raman spectra were measured to confirm graphene formation.

Słowa kluczowe

synthesis dispersion AFM graphene Raman spectra

Wydawca

De Gruyter

Czasopismo

Materials Science Poland

Rocznik

2016

Tom

Vol. 34, No. 3

Strony

627--632

Opis fizyczny

Bibliogr. 33 poz., rys.

Twórcy

autor

Elsabawy K. M.

Chemistry Department, Faculty of Science, Tanta University, Tanta-31725, Egypt
Chemistry Department, Faculty of Science, Materials Science Unit, Taif University, 888-Alhawya, Taif City, Kingdom of Saudi Arabia

Bibliografia

1. Soldano C., Mahmood A., Dujardin E., Carbon, 48 (2010), 2127.
2. Geim A.K., Novoselov K.S., Nat. Mater., 6 (2007), 183.
3. Park S., Ruoff, R.D., Nat. Nanotechnol., 4(2009), 217.
4. Novoselov K.S., Geim A.K., Morozov S.V., Jiang D., Zhang Y., Dubonos S.V., Grigorieva I.V., Firsov A.A., Science, 306 (2004), 666.
5. Hummers W.S., Offeman R.E., J. Am. Chem. Soc., 80 (6) (1958), 1339.
6. Dressehaus M.S., Dressehaus D., Adv. Phys., 51 (1) (2009), 186.
7. Schniepp H.C., Li J.L., Mcallister M.J., Sai H., Herrera-Alonso M., Adamson D.H., J. Phys. Chem. B, 110 (17) (2006), 8535.
8. Mac A.M.J., Li J.L., Adamson D.H., Schniepp H.C., Abdala A.A., Liu J., Chem. Mater., 19 (18) (2007), 4396.
9. Li D., Muller M.B. Gilje S., Kaner R.B., Wallace G.G., Nat. Nanotechnol., 3 (2) (2008), 101.
10. Chen Y., Qi Y., Tai Z., Yan X., Zhu F., Eur. Polym. J., 48 (2012), 1026.
11. Zhou X.Z., Huang X., Qi X.Y., Wu S.X., Xue C., Boey F.Y.C., Yan Q., Chen P., Zhang H., J. Phys. Chem. C, 113 (2007), 10842.
12. Stankovich S., Dikin, D.A., Compton O.C., Dommett G.H.B., Ruoff R.S., Nguyen S.T., Chem. Mater., 22 (2010), 4153.K. M. Elsabawy
13. Hernandez Y., Nicolosi V., Lotya M., Blighe F.M., Sun Z., De S., Nat. Nanotechnol., 3 (9) (2008), 563.
14. Shen J., Hu Y., Shi M., Lu X., Li C., Ye M., Chem. Mater., 21 (2009), 3514.
15. Choi B.G., Park H., Park T.J., Yang M.H., Kim J.S., Jang S.Y., Heo N.S., Lee S.Y., Kong J., Hong W.H., ACS Nano, 4 (2010), 2910.
16. Hummers W.S., Offeman R.E., J. Am. Chem. Soc., 80 (1958), 1339.
17. Zhu Y., Murali S., Ca W.I., Li X., Suk J.W., Potts J.R., Ruoff R.S., Adv. Mater., 22 (2010), 3906.
18. Zhang Y., Ren L., Wang S., Marathe A., Chaudhuri J., Li G., J. Mater. Chem., 21 (2011), 5386.
19. Jalili R., Aboutalebi S., Esrafilzadeh D., Konstantinov K.K., Moulton S.E., Razal J.M., Wallace G.G., ACS Nano, 7 (5) (2013), 3981.
20. GREAVES T.L.; Weerawardena A., Drummond C.J., Phys. Chem. Chem. Phys., 13 (2011), 9180.
21. Greaves T.L., Drummond C.J., Chem. Soc. Rev., 37 (2008), 1709.
22. Ray A., J. Am. Chem. Soc., 91(1969), 6511.
23. Greaves T.L., Weerawardena A., Fong C., Drummond C.J., Langmuir, 23 (2006), 402.
24. Alhuthali A., El-Nahass M.M., Atta A.A., El-Raheem A.M.M., Elsabawy K.M., Hassanien A.M., J. Lumin., 158 (2015), 165.
25. Elsabawy K.M., Int. J. Chem. Concept., 1 (2015), 38.
26. Elsabawy K.M., World Sci. News, 30 (2016), 57.
27. Elsabawy K.M., RSC Adv., 1 (2011), 964.
28. Saito R., Hofmann M., Dresselhaus G., Jorio A., Dresselhaus M.S., Adv. Phys., 30 (2011), 413.
29. Ferrari A.C., Solid State Commun, 143 (2007), 47.
30. Ferrari A.C., Robertson J., Phys. Rev. B, 61 (2000), 14095.
31. Changjing F., Guogang Z., Haijun Z., Int. J. Electrochem. Sc., 8 (2013), 6269.
32. Geim A.K., Novoselov K.S., Nat. Mater., 8 (2009), 183.
33. Park S., Ruoff R.D., Nat. Nanotechnol., 4 (2009), 217.

Uwagi

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.

Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-87a527b7-a7f8-4e36-9d01-02b9c11db01c