Effects of different Sn contents on formation of Ti2SnC by self-propagating high-temperature synthesis method in Ti-Sn-C and Ti-Sn-C-TiC systems

• Autorzy: Sun H Y , Kong X , Sen W , Yi Z Z , Wang B S , Liu G Y

Identyfikatory

DOI

10.2478/s13536-014-0252-7

• Języki publikacji: EN

Abstrakty

EN

Effect of different Sn contents on combustion synthesis of Ti2SnC was studied using elemental Ti, Sn, C and TiC powders as raw materials in the Ti–Sn–C and Ti–Sn–C–TiC system, in which the molar ratio of Ti/C was set as 2:1. The reaction mechanism for the formation of Ti2SnC was also investigated. The results showed that the amount of Ti2SnC in combustion products firstly increased with increasing of Sn content (0.6 to 0.8 mol), and then decreased with further increasing of Sn content (1.0 to 1.2 mol). Upon addition of 15 % TiC instead of Ti and C, the optimum addition of Sn decreased to 0.7 mol and a higher purity of Ti2SnC was obtained. The Ti2SnC powders were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD).

Słowa kluczowe

EN

Ti2SnC; self-propagating high-temperature synthesis; TiC; Sn; reaction mechanism

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2014
• Tom: Vol. 32, No. 4
• Strony: 696--701
• Opis fizyczny: Bibliogr. 15 poz., rys., wykr.

Twórcy

autor

Sun H Y

• College of Science, Honghe University, Mengzi 661100, China

autor

Kong X

• College of Science, Honghe University, Mengzi 661100, China

autor

Sen W

• Yunnan Tin Company Limited, Gejiu 661000, China

autor

Yi Z Z

• College of Science, Honghe University, Mengzi 661100, China

autor

Wang B S

• College of Science, Honghe University, Mengzi 661100, China

autor

Liu G Y

• College of Science, Honghe University, Mengzi 661100, China

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