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Aluminum and fumed silica as solid industrial wastes were converted to zeolite NaPas a value-addedproduct without any template. The hydrothermal process was optimized using static autoclave. The crystallization was carried out at 100, 120 and 150°C for 24, 48 and 72 h. The prepared zeolite of Si:Al ratio of 1.2 was characterized using X-ray Diffraction (XRD), Scanning Electron Microscope (SEM) provided with Energy Dispersive Spectroscopy (EDS), Surface Area, Fourier Transmitted Infra-Red (FTIR) and Thermal Analysis (TG-DSC). The crystalline phase was formed at 100°Cafter 72 hours and at 120°C after 48 hours, while it was formed after 24 honlyat 150°C. Increasing temperature and time lead to the conversion of the prismatic gibbsite crystals into plate-like structure of zeolitewhich is then formedcauliflower-like structure.The prepared zeolite was employed as adsorbent for Ni2+and Cu2+ions from aqueous solution.The kinetic studies of adsorption processes were performed.
Słowa kluczowe
Rocznik
Tom
Strony
87--99
Opis fizyczny
Bibliogr. 49 poz., fot., rys., wykr.
Twórcy
- Central Metallurgical Research and Development Institute (CMRDI)
autor
- Central Metallurgical Research and Development Institute (CMRDI)
autor
- Central Metallurgical Research and Development Institute (CMRDI)
autor
- Central Metallurgical Research and Development Institute (CMRDI)
autor
- Central Metallurgical Research and Development Institute (CMRDI)
autor
- Chemistry Department, Faculty of Science, Ain shams University, Cairo, Egypt
autor
- Chemistry Department, Faculty of Science, Ain shams University, Cairo, Egypt
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Uwagi
Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2021).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-83cec868-11e2-4458-bea4-215d1967d946