Effect of reaction time on the structure and optical properties of P3HT/MWCNT-OH nanocomposites

• Autorzy: Nurazzi, Norizan Mohd , Abdullah Norli , Ngah Demon Siti Zulaikha , Halim Norhana Abdul , Sa'aya Nurul Syahirah Nasuha , Mohamad Imran Syakir

Identyfikatory

DOI

10.14314/polimery.2022.5.3

Warianty tytułu

PL

Wpływ czasu reakcji na strukturę i właściwości optyczne nanokompozytów P3HT/MWCNT-OH

• Języki publikacji: EN

Abstrakty

EN

In the present study, regioregular poly(3-hexylthiophene-2,5-diyl) (P3HT) coated hydroxylated multi-walled carbon nanotubes (MWCNT-OH) nanocomposites were prepared over different reaction times of non-covalent functionalization. The reaction time was set as 24, 48, 72, 96, and 120 hours. The structure and optical characteristics of nanocomposites were analyzed using Fourier-transform infrared (FTIR) and ultraviolet-visible (UV-Vis) spectroscopy, respectively. Reaction time affected prepared nanocomposites by decreasing the intensity of the P3HT/MWCNT-OH peaks gradually with increasing of the reaction time. Comparing with the pure P3HT and MWCNT-OH, the calculated energy band gap and the Urbach energy of the nanocomposites were reduced proportionally as the reaction time reached 120 hours and achieved 2.60 and 0.329 eV, respectively.

PL

Syntetyzowano hydroksylowane wielościenne nanorurki węglowe (MWCNT-OH) pokryte stereoregularnym poli(3-heksylotiofen-2,5-diylu) (P3HT) oraz zbadano wpływ czasu reakcji niekowalencyjnej funkcjonalizacji na strukturę i właściwości optyczne otrzymanego nanokompozytu. Czas reakcji wynosił 24, 48, 72, 96 i 120 godzin. W badaniach wykorzystano spektroskopię w podczerwieni z transformacją Fouriera (FTIR) oraz ultrafioletową UV-Vis. Wraz ze wzrostem czasu reakcji następowało stopniowe zmniejszenie intensywności pików P3HT/MWCNT-OH. W porównaniu z P3HT i MWCNT-OH obliczona przerwa energetyczna i energia Urbacha zmniejszały się wraz z wydłużeniem czasu reakcji i osiągnęły odpowiednio 2,60 i 0,329 eV przy czasie reakcji 120 godzin.

Słowa kluczowe

EN

carbon nanotubes; energy band gap; P3HT; MWCNT-OH; UV-Vis; FTIR; Urbach energy

PL

nanorurki węglowe; przerwa energetyczna; P3HT; MWCNT-OH; UV-Vis; FTIR; energia Urbacha

• Wydawca: Sieć Badawcza Łukasiewicz – Instytut Chemii Przemysłowej
• Czasopismo: Polimery
• Rocznik: 2022
• Tom: Vol. 67, nr 5
• Strony: 205--211
• Opis fizyczny: Bibliogr. 59 poz., rys., tab.

Twórcy

autor

Nurazzi, Norizan Mohd

• Centre for Defence Foundation Studies, National Defence University of Malaysia, Kem Sungai Besi, 57000 Kuala Lumpur, Malaysia

• https://orcid.org/0000-0001-7697-0511

autor

Abdullah Norli

• Centre for Defence Foundation Studies, National Defence University of Malaysia, Kem Sungai Besi, 57000 Kuala Lumpur, Malaysia

• https://orcid.org/0000-0002-8519-3379

autor

Ngah Demon Siti Zulaikha

• Centre for Defence Foundation Studies, National Defence University of Malaysia, Kem Sungai Besi, 57000 Kuala Lumpur, Malaysia

• https://orcid.org/0000-0001-6706-7216

autor

Halim Norhana Abdul

• Centre for Defence Foundation Studies, National Defence University of Malaysia, Kem Sungai Besi, 57000 Kuala Lumpur, Malaysia

• https://orcid.org/0000-0001-8077-824X

autor

Sa'aya Nurul Syahirah Nasuha

• Centre for Defence Foundation Studies, National Defence University of Malaysia, Kem Sungai Besi, 57000 Kuala Lumpur, Malaysia

autor

Mohamad Imran Syakir

• Faculty of Mechanical Engineering, Universiti Teknikal Malaysia Melaka, Hang Tuah Jaya, 76100 Durian Tunggal, Melaka, Malaysia

• https://orcid.org/0000-0002-3805-9919

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Uwagi

Opracowanie rekordu ze środków MEiN, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2022-2023).