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A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
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Rocznik
Tom
Strony
1287--1291
Opis fizyczny
Bibliogr. 22 poz., rys.
Twórcy
autor
- Sejong University, Faculty of Nanotechnology and Advanced Materials Engineering, Seoul 05000, Korea
autor
- Sejong University, Faculty of Nanotechnology and Advanced Materials Engineering, Seoul 05000, Korea
autor
- Wonkwang Health Science University, Department of Dental Laboratory, Iksan 54538, Korea
autor
- Korea Aerospace University, Department of Materials Engineering, Goyang-Si 10510, Korea
autor
- Uiduk University, Division of Green Energy Engineering, Kyeongju 38004, Korea
autor
- Uiduk University, Division of Green Energy Engineering, Kyeongju 38004, Korea
autor
- Colorado School of Mines, Department of Metallurgical and Materials Engineering, Golden 80401, United States of America
autor
- Sejong University, Faculty of Nanotechnology and Advanced Materials Engineering, Seoul 05000, Korea
Bibliografia
- [1] M.M. Dewidar, J.K. Lim, J. Alloys Comp. 454, 442 (2008).
- [2] H.R. Choi, J.M. Byun, M.J. Suk, S.T. Oh, Y.D. Kim, J. Korea Powder Metall. Inst. 23, 235, (2016).
- [3] B. Otsuki, M. Takemoto, S. Fujibayashi, M. Neo, T. Kokubo, T. Nakamura, Biomater. 27, 5892 (2006).
- [4] K. Gomi, J.E. Davies, J. Biomed. Mater. Res. A 27, 429 (1993).
- [5] F.J.C. Braga, R.F.C. Marques, E. de A. Filho, A.C. Guastaldi, Appl. Surf. Sci. 253, 9203, (2007).
- [6] H.C. Man, M. Bai, F.T. Cheng, Appl. Surf. Sci. 258, 436 (2011).
- [7] S.Y. Kwak, H.G. Kim, J.M. Byun, J.H. Park, M.J. Suk, S.T. Oh, Y.D. Kim, J. Korea Powder Metall. Inst. 21, 28 (2014).
- [8] S. Gokul Lakshami, D. Arivuoli, B. Ganguli, Mater. Chem. Phys. 76, 187 (2002).
- [9] M. Rahman, I. Reid, P. Duggan, D.P. Dowling, G. Hughes, M.S.J. Hashmi, Surf. Coat. Technol. 210, 4865 (2007).
- [10] W.H. Lee, Y.J. Jo, Y.H. Kim, Y.H. Jo, J.G. Seong, C.J. Van Tyne, S.Y. Chang, Arch. Metall. Mater. 60, 1185 (2015).
- [11] Y.J. Jo, Y.H. Kim, Y.H. Jo, J.G. Seong, S.Y. Chang, P.J. Reucroft, S.B. Kim, W.H. Lee, Metals Mater. Int., 21, 337 (2015).
- [12] M. Donachie, Titanium, A technical guide, Ohio ASM International; 2000 p. 14.
- [13] G. Soto, Appl. Surf. Sci. 233, 115 (2004).
- [14] J.Y. Kim, P.J. Reucroft, M. Taghiei, V.R. Pradhan, I. Wender, Energy and Fuels 8, 886 (1994).
- [15] Y.J. Jo, Y.H. Kim, Y.H. Jo, J.G. Seong, Y.K. Ko, S.B. Kim, S.Y. Chang, W.H. Lee, Metals Mater. Int. 21, 159 (2015).
- [16] Y.J. Jo, Y.H. Jo, J.G. Seong, Y.H. Kim, S.Y. Chang, M.S. Noh, H.G. Jeong, W.H. Lee, Surf. Eng. 31, 885 (2015).
- [17] L. Liuhe, X. Lifang, M. Xinxin, Surf. Coat. Technol. 120, 618 (1999).
- [18] Y.J. Jo, Y.H. Kim, Y.H. Jo, J.G. Seong, S.Y. Chang, C.J. Van Tyne, W.H. Lee, J. Nanosci. Nanotechnol. 14, 8429 (2014).
- [19] M. Rahman, I. Reid, P. Duggan, D.P. Dowling, G. Hughes, M.S.J. Hashimi, Surf. Coat. Technol. 210, 4865 (2007).
- [20] O.I. Yaskiv, I.M. Pohrelyuk, V.M. Fedirko, D.B. Lee, O.V. Tkachuk, Thin Solid Films 519, 6508 (2011).
- [21] Y.J. Jo, Y.H. Jo, J.G. Seong, Y.H. Kim, S.Y. Chang, W.H. Lee, Mater. Sci. Technol. 31, 989 (2015).
- [22] D. Georgiev, R.J. Baird, G. Newaz, G. Auner, R. Witte, H. Herfurth, Appl. Surf. Sci. 236, 71 (2004).
Uwagi
EN
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017)
Typ dokumentu
Bibliografia
Identyfikator YADDA
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