Effect of sintering parameters using the central composite design method, electronic structure and physical properties of yttria-partially stabilized ZrO2 commercial ceramics

Mendes, A. M.; Costa, M. C. B.; Araújo, V. D.; Motta, F. V.; Paskocimas, C. A.; Acchar, W.; Longo, E.; Bomio, M. R. D.; Cavalcante, L. S.

doi:10.1515/msp-2017-0035

Artykuł - szczegóły

Tytuł artykułu

Effect of sintering parameters using the central composite design method, electronic structure and physical properties of yttria-partially stabilized ZrO2 commercial ceramics

Autorzy

Mendes A. M. , Costa M. C. B. , Araújo V. D. , Motta F. V. , Paskocimas C. A. , Acchar W. , Longo E. , Bomio M. R. D. , Cavalcante L. S.

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.1515/msp-2017-0035

Warianty tytułu

Języki publikacji

Abstrakty

In this work, the effect of sintering parameters on electronic structure and physical properties of yttria-partially stabilized ZrO₂ (YPSZ) commercial ceramics has been studied using the central composite design (CCD) method. The CCD method allows using empirical modelling with better fitting, by considering the interaction between both factors. Different temperature ranges and sintering times for processing of YPSZ ceramics have been used in order to evaluate the grain growth, hardness and volumetric shrinkage by the CCD method. X-ray diffraction patterns and Rietveld refinement data indicate that non-sintered YPSZ ceramics exhibits two phases related to tetragonal and monoclinic structures, while the sintered YPSZ ceramics exhibits a single phase related to a tetragonal structure. Moreover, the monoclinic structure presents zirconium (Zr) atoms coordinated to seven oxygen (O) atoms, while in the tetragonal structure Zr atoms are coordinated to eight O atoms. Field emission scanning electron microscopy images were employed to monitor the sintering and growth process. In addition, the response surfaces obtained from calculations presented the effect of thermal and kinetic variables on the physical properties such as average grain size, volumetric shrinkage and hardness of YPSZ ceramics.

Słowa kluczowe

YPSZ ceramics electronic structure central composite design hardness shrinkage

Wydawca

De Gruyter

Czasopismo

Materials Science Poland

Rocznik

2017

Tom

Vol. 35, No. 1

Strony

225--238

Opis fizyczny

Bibliogr. 77 poz., rys., tab.

Twórcy

autor

Mendes A. M.

LSQM-Laboratório de Síntese Química de Materiais-DEMat, Universidade Federal do Rio Grande do Norte-UFRN, P.O. Box 1524, 59078-970, Natal, RN, Brazil

autor

Costa M. C. B.

LSQM-Laboratório de Síntese Química de Materiais-DEMat, Universidade Federal do Rio Grande do Norte-UFRN, P.O. Box 1524, 59078-970, Natal, RN, Brazil

autor

Araújo V. D.

LSQM-Laboratório de Síntese Química de Materiais-DEMat, Universidade Federal do Rio Grande do Norte-UFRN, P.O. Box 1524, 59078-970, Natal, RN, Brazil

autor

Motta F. V.

LSQM-Laboratório de Síntese Química de Materiais-DEMat, Universidade Federal do Rio Grande do Norte-UFRN, P.O. Box 1524, 59078-970, Natal, RN, Brazil

autor

Paskocimas C. A.

LSQM-Laboratório de Síntese Química de Materiais-DEMat, Universidade Federal do Rio Grande do Norte-UFRN, P.O. Box 1524, 59078-970, Natal, RN, Brazil

autor

Acchar W.

Departamento de Física, Universidade Federal do Rio Grande do Norte-UFRN, P.O. Box 1524, 59078-970, Natal, RN, Brazil

autor

Longo E.

laeciosc@bol.com.br

LIEC, Departamento de Química-Universidade Federal de Sao Carlos-UFSCar, P.O. Box 676, 13565-905, Sao Carlos, SP, Brazil

autor

Bomio M. R. D.

LSQM-Laboratório de Síntese Química de Materiais-DEMat, Universidade Federal do Rio Grande do Norte-UFRN, P.O. Box 1524, 59078-970, Natal, RN, Brazil

autor

Cavalcante L. S.

PPGQ-DQ-CCN-GERATEC-Universidade Estadual do Piauí, Joao Cabral, N. 2231, P.O. Box 381, 64002-150 Teresina, PI, Brazil

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Uwagi

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017).

Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-7e4d5994-be07-4967-9358-39350a03d8bf