Energy-dispersive X-Ray spectroscopy mapping of porous coatings obtained on Titanium by plasma electrolytic oxidation in a solution containing concentrated phosphoric acid with copper nitrate

Rokosz, K.; Hryniewicz, T.; Dudek, Ł.; Schütz, A.; Heeg, J.; Wienecke, M.

doi:10.1515/adms-2016-0013

Artykuł - szczegóły

Tytuł artykułu

Energy-dispersive X-Ray spectroscopy mapping of porous coatings obtained on Titanium by plasma electrolytic oxidation in a solution containing concentrated phosphoric acid with copper nitrate

Autorzy

Rokosz K. , Hryniewicz T. , Dudek Ł. , Schütz A. , Heeg J. , Wienecke M.

Wybrane pełne teksty z tego czasopisma

http://content.sciendo.com/view/journals/adms/adms-overview.xml

Identyfikatory

DOI

10.1515/adms-2016-0013

Warianty tytułu

Języki publikacji

Abstrakty

The SEM and EDS study results of coatings obtained on titanium by Plasma Electrolytic Oxidation (PEO) in the electrolytes containing of 600 g copper nitrate in 1 liter of concentrated phosphoric acid at 450 V for 1 and 3 minutes, are presented. The obtained coatings are porous and consist mainly of phosphorus within titanium and copper. It was found that the time of PEO oxidation has impact on the chemical composition of the coatings. The longer time of PEO treatment, the higher amount of copper inside coating. The PEO oxidation of titanium for 1 minute has resulted in the creation of coating, on which 3 phases where found, which contained up to 13.4 wt% (9 at%) of copper inside the phosphate structure. In case of 1 minute PEO treatment of titanium, the 2 phases were found, which contained up to 13 wt% (8 at%) of copper inside the phosphate structure. The copper-to-phosphorus ratios after 1 minute processing belong to the range from 0.28 by wt% (0.14 by at%) to 0.47 by wt% (0.23 by at%), while after 3 minutes the same ratios belong to the range from 0.27 by wt% (0.13 by at%) to 0.35 by wt% (0.17 by at%). In summary, it should be stated that the higher amounts of phosphorus and copper were recorded on titanium after PEO oxidation for 3 minutes than these after 1 minute.

Słowa kluczowe

Plasma Electrolytic Oxidation PEO micro arc oxidation MAO SEM titanium H3PO4 Cu(NO3)2

PEO MAO SEM Tytan H3PO4 Cu(NO3)2

Wydawca

Politechnika Gdańska

Czasopismo

Advances in Materials Science

Rocznik

2016

Tom

Vol. 16, nr 3(49)

Strony

15--25

Opis fizyczny

Bibliogr. 60 poz., rys., wykr., tab.

Twórcy

autor

Rokosz K.

rokosz@tu.koszalin.pl

Koszalin University of Technology, Faculty of Mechanical Engineering, Department of Engineering and Informatics Systems, Division of Bioengineering and Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland

autor

Hryniewicz T.

Tadeusz.Hryniewicz@tu.koszalin.pl

Koszalin University of Technology, Faculty of Mechanical Engineering, Department of Engineering and Informatics Systems, Division of Bioengineering and Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland

autor

Dudek Ł.

lukasz.dudek@tu.koszalin.pl

Koszalin University of Technology, Faculty of Mechanical Engineering, Department of Engineering and Informatics Systems, Division of Bioengineering and Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland

autor

Schütz A.

antje.schuetz@hs-wismar.de

Hochschule Wismar-University of Applied Sciences Technology, Business and Design, Faculty of Engineering, DE 23966 Wismar, Germany

autor

Heeg J.

jan.heeg@hs-wismar.de

autor

Wienecke M.

marion.wienecke@hs-wismar.de

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Uwagi

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.

Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-7e206ef6-a618-4291-9866-4f246b10960a