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Preparation of α-alumina particles from alunite ores by using dry caustic assisted roasting

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
In this study, the production of α-alumina particles from alunite ore was carried out through roasting-leaching and precipitation tests. The effects of parameters such as temperature, stirring speed, solid ratio, and leaching time on Al yield% were investigated in leaching tests using the response surface methodology (RSM) and central composite design (CCD). As a result of the experiments, the highest Al yield ratio as 86.06% was achieved in water leaching under conditions of 100°C, 900 rpm, 15% as solid ratio, and 65 min. as time after roasting at 600°C with NaOH. The experimental results revealed that temperature and solid ratio% were more influential than other parameters. To precipitate Al(OH)3 from the loaded solution, HCl was used to reduce the pH. The precipitate was roasted in a muffle furnace at 1100°C (±50°C) for 240 min. Then, α-alumina particles were obtained with an efficiency of 89.89% and purity of 91.24%. The morphological properties of the final product were confirmed by TGA-DTA, SEM/EDX and X-ray diffraction analyses.
Słowa kluczowe
Rocznik
Strony
art. no. 202256
Opis fizyczny
Bibliogr. 30 poz., rys., tab., wykr.
Twórcy
autor
  • Department of Mining and Mining Extraction, Vocational school of Aladag, Cukurova University, Adana/Türkiye
  • Department of Mining Engineering, Cukurova University, Adana/Türkiye
  • Department of Mining Engineering, Cukurova University, Adana/Türkiye
Bibliografia
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  • MOHAMMADI M., SALARIRAD, M. 2013. KINETICS OF DIRECT LEACHING OF NATURAL ALUNITE IN KOH. Ind. Eng. Chem. Res. 52 (40), 14359–14365.
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  • MATORI, K., WAH, L., HASHIM, M., ISMAIL, I., MOHD ZAID, M., 2012. Phase transformations of a-alumina made from waste aluminum via a precipitation technique. Int J Mol Sci 13, 16812–16821
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Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-7c436055-c99d-444b-857b-dd71568ca5cd
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