Substrates with different magnetic properties versus iron-nickel film electrodeposition

• Autorzy: Białostocka Anna M. , Klekotka Marcin , Klekotka Urszula , Żabiński Piotr R. , Kalska-Szostko Beata

Identyfikatory

DOI

10.2478/cdem-2023-0009

• Języki publikacji: EN

Abstrakty

EN

The hereby work presents the iron-nickel alloys electroplated on the different metallic substrates (aluminium, silver, brass) using galvanostatic deposition, with and without presence of the external magnetic field (EMF). The films were obtained in the same electrochemical bath composition - mixture of iron and nickel sulphates (without presence of additives) in the molar ratio of 2 : 1 (Ni : Fe), the electric current density (50.0 mA/cm2), and the time (3600 s). The mutual alignment of the electric (E) and magnetic field (B) was changeable - parallel and perpendicular. The source of EMF was a set of two permanent magnets (magnetic field strength ranged from 80 mT to 400 mT). It was analysed the surface microstructure, composition, morphology, thickness and the mechanical properties (roughness, work of adhesion). The surface morphology and the thickness of films were observed by Scanning Electron Microscopy (SEM) and Confocal Laser Scanning Microscopy (CLSM). The elemental composition of all FeNi films was measured using Wavelength Dispersive X-Ray Fluorescence (WDXRF). The crystalographic analysis of the deposits was carried out by X-Ray Diffraction. Depending on the used substrate, modified external magnetic field orientation influenced the tribological and physio-chemical properties of the deposited layers. The diamagnetic substrates and EMF application reduced the FeNi thickness and the average crystallites size, in contrast to the paramagnetic substrate. Parallel EMF increased the value of the tribological parameters for CuZn and Ag but decreased for Al. The content of FeNi structure was rising in the case of diamagnetic substrate and the dependence was opposite on the paramagnetic substrate.

Słowa kluczowe

EN

electrodeposition; magnetic field; magnetohydrodynamics; substrate; thin films; iron-nickel alloys

PL

elektroosadzanie; pole magnetyczne; magnetohydrodynamika; substrat; cienkie warstwy; stopy żelazo-nikiel

• Wydawca: Towarzystwo Chemii i Inżynierii Ekologicznej
• Czasopismo: Chemistry-Didactics-Ecology-Metrology
• Rocznik: 2023
• Tom: R. 28, NR 1-2
• Strony: 157--170
• Opis fizyczny: Bibliogr. 31 poz., rys., wykr.

Twórcy

autor

Białostocka Anna M.

• Faculty of Electrical Engineering, Bialystok University of Technology, ul. Wiejska 45D, 15-351 Białystok, Poland, phone [phone], fax [phone]

• https://orcid.org/0000-0002-7684-2357

autor

Klekotka Marcin

• Faculty of Mechanical Engineering, Bialystok University of Technology, ul. Wiejska 45C, 15-351 Białystok, Poland

• https://orcid.org/0000-0002-9751-2939

autor

Klekotka Urszula

• Faculty of Chemistry, University of Bialystok, ul. K. Ciołkowskiego 1K, 15-245 Białystok, Poland

• https://orcid.org/0000-0002-1594-5889

autor

Żabiński Piotr R.

• Faculty of Non-Ferrous Metals, AGH University of Science and Technology in Kraków, al. A. Mickiewicza 30, 30-059 Kraków, Poland

• https://orcid.org/0000-0002-5085-2645

autor

Kalska-Szostko Beata

• Faculty of Chemistry, University of Bialystok, ul. K. Ciołkowskiego 1K, 15-245 Białystok, Poland

• https://orcid.org/0000-0002-6353-243X

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Uwagi

Opracowanie rekordu ze środków MNiSW, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2024).