Spark Plasma Sintering of Mn-Zn Ferrite Powders by High Energy Ball Milling

• Autorzy: Suh Jun Young , Song Yo-Seung , Chang Si Young

Identyfikatory

DOI

10.24425/amm.2019.127579

• Języki publikacji: EN

Abstrakty

EN

The Mn-Zn ferrite powders prepared by high energy ball milling were heat-treated, subsequently compacted and sintered by spark plasma sintering (SPS). Based on the observation of microstructure, the characteristics of samples after SPS were investigated and compared with ones after conventional sintering. The size of initial powders was approximately 650 nm and decreased to 230 nm after milling at 300 rpm for 3 h. After heat treatment at 973 K for 1 h, the milled powders became larger to approximately 550 nm in size again and the peaks of Mn₂ O₃ disappeared in XRD patterns. In the samples after SPS, the Fe₂ O₃ and MnZnFe₂ O₄ phases decomposed at the higher temperatures than 1173 K and 1373 K, respectively, while only MnZnFe₂ O₄ phase was detected in the samples conventionally sintered at 1273~1673 K. As the sintering temperature increased, the relative density after SPS increased more quickly than that after conventional sintering. In particular, it reached approximately 99% after SPS at 1473 K.

Słowa kluczowe

EN

high energy ball milling; nano-sized particles; SPS; conventional sintering; density

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2019
• Tom: Vol. 64, iss. 2
• Strony: 565--569
• Opis fizyczny: Bibliogr. 16 poz., fot., rys.

Twórcy

autor

Suh Jun Young

• Korea Aerospace University, Department of Materials Engineering, Goyang 10540, Korea

autor

Song Yo-Seung

• Korea Aerospace University, Department of Materials Engineering, Goyang 10540, Korea

autor

Chang Si Young

• Korea Aerospace University, Department of Materials Engineering, Goyang 10540, Korea

Bibliografia

• [1] P. Hu, H. Yang, D. Pan, H. Wang, J. Tian, S. Zhang, X. Wang, A. A. Volinsky, J. Magn. Magn. Mater. 322, 173-177 (2010).
• [2] S. K. Pradhan, S. Bid, M. Gateshki, V. Petkov, J. Mater. Chem. Phys. 93, 224-230 (2005).
• [3] S. Dasgupta, J. Das, J. Eckert, I. Manna, J. Magn. Magn. Mater. 306, 9-15 (2006).
• [4] S. J. Park, Y. S. Song, K. S. Nam, S. Y. Chang, J. Kor. Powd. Met. Inst. 19, 122-126 (2012).
• [5] S. M. Hong, E. K. Park, K. Y. Kim, J. J. Park, M. K. Lee, C. K. Rhee, J. K. Lee, Y. S. Kwon, J. Kor. Powd. Met. Inst. 19, 32-39 (2012).
• [6] H. P. Klug, L. E. Alexander, Joohn Wiley and Sons, X-ray Diffraction Procedures for Polycrystalline and Amorphous Materials, New York 1997.
• [7] L. Gao, H. Miyamoto, J. Inorg. Mater. 12, 129-133 (1997).
• [8] M. Tokita, J. Soc. Powder Technol. 30, 790-804 (1993).
• [9] T. Takeuchi, M. Tabuchi, H. Kageyama, Y. Suyama, J. Am. Ceram. Soc. 82, 939-943 (1999).
• [10] Z. J. Shen, M. Johnsson, Z. Zhao, M. Nygren, J. Am. Ceram. Soc. 85, 1921-1927 (2002).
• [11] G. D. Zhan, J. D. Kuntz, J. L. Wan, A. K. Mukherjee, Nat. Mat. 2, 38-42 (2003).
• [12] S. I. Cha, S. H. Hong, B. K. Kim, Mater. Sci. Eng. A 351, 31-38 (2003).
• [13] M. Yue, J. X. Zhang, Y. F. Xiao, G. P. Wang, T. Li, IEEE Trans. Magn. 39, 3551-3553 (2003).
• [14] S. Y. Chang, S. T. Oh, M. J. Suk, C. S. Hong, J. Kor. Powd. Met. Inst. 21, 97-101 (2014).
• [15] L. Zhao, H. Yang, L. Yu, Y. Cui, X. Zhao, B. Zou, S. Feng, J. Magn. Magn. Mater. 301, 445-451 (2006).
• [16] D. J. Kim et al., Korean Powder Metallurgy Inst, Powder Metallurgy & Particulate Materials Processing, Seoul 2010.

Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).