One step paired electrochemical synthesis of iron and iron oxide nanoparticles

• Autorzy: Ordoukhanian J. , Karami H. , Nezhadali A.

Identyfikatory

DOI

10.1515/msp-2016-0090

• Języki publikacji: EN

Abstrakty

EN

In this study, a new one step paired electrochemical method is developed for simultaneous synthesis of iron and iron oxide nanoparticles. iron and iron oxide are prepared as cathodic and anodic products from iron (ii) sulfate aqueous solution in a membrane divided electrolytic cell by the pulsed current electrosynthesis. Because of organic solvent-free and electrochemical nature of the synthesis, the process could be considered as green and environmentally friendly. The reduction of energy consumption and low cost are the other significant advantages of this new method that would have a great application potential in the chemical industry. The nanostructure of prepared samples was characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The magnetic properties were studied by vibrating sample magnetometer (VsM).

Słowa kluczowe

EN

nanoparticles; electrodeposition; pulsed current method; paired electrosynthesis; magnetic materials

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2016
• Tom: Vol. 34, No. 3
• Strony: 655--658
• Opis fizyczny: Bibliogr. 19 poz., rys., tab.

Twórcy

autor

Ordoukhanian J.

• DepartmentofChemistry,PayameNoorUniversity,POBox19395-3697,Tehran,Iran

autor

Karami H.

• DepartmentofChemistry,PayameNoorUniversity,POBox19395-3697,Tehran,Iran
• NanoResearchLaboratory,DepartmentofChemistry,PayameNoorUniversity,Abhar,Iran

autor

Nezhadali A.

• DepartmentofChemistry,PayameNoorUniversity,POBox19395-3697,Tehran,Iran

Bibliografia

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Uwagi

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.