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The basic factor limiting the use of glasses is their unsatisfactory mechanical strength. The improvement of the mechanical strength of glasses is usually obtained by applying their respective thin surface layers. The object of the research was glass coated with zirconium oxide. For the application of zirconium oxide layer, dip-coating method was used. The resulting materials were subjected to detailed examination of the microstructure (SEM), and mechanical tests (Vickers hardness and modulus of elasticity). In order to evaluate the optical characteristics, the tests were performed by UV/VIS. The thickness of the overlying layers were determined using the method of ellipsometry. The study showed that the obtained sol-gel layer of zirconium oxide (IV) on glasses influence the improvement of the mechanical properties. It has been shown that the applied layers have high adhesion to the substrate.
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1747--1752
Opis fizyczny
Bibliogr. 28 poz., rys., tab., wykr., wzory
Twórcy
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, Al. Mickiewicza 30, 30-059 Kraków
autor
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, Al. Mickiewicza 30, 30-059 Kraków
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, Al. Mickiewicza 30, 30-059 Kraków
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, Al. Mickiewicza 30, 30-059 Kraków
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, Al. Mickiewicza 30, 30-059 Kraków
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, Al. Mickiewicza 30, 30-059 Kraków
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, Al. Mickiewicza 30, 30-059 Kraków
autor
- Cracow University of Technology, Institute of Physics, Ul. Podchorazych 1, 30-084 Cracow, Poland
Bibliografia
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- [2] F. M. Ernsberger, Glass Ind., 47, 422-427 (1966).
- [3] G. Macrelli, Riv. Stn. Sper. Vetro 31, 69-76 (2001).
- [4] R. F. Bartholomew & H. M. Garfinkel, Chemical strengthening of glass. Glass Science and Technology. Vol. 5. Elasticity and Strength in Glasses. 1980, Academic Press, New York.
- [5] R. Gardon, Thermal tempering of glass. D.R. Uhlmann & N.J. Kreidl (eds), 1980, Academic Press, New York.
- [6] A. K. Varshneya, Glass Res. 21, 10-11 (2001).
- [7] M. Drajewicz, J. Wasylak, Optica Applicata 38, 421-430 (2008).
- [8] B. D. Fabes, D. R. A. Uhlmann, J. Am. Ceram. Soc. 73, 978-988 (1990).
- [9] C. Ronald, G. Nicholson, P. S. Nicholson, J. Am. Ceram. Soc. 55, 152-157 (1972).
- [10] H. G. Scott, J. Mat. Sci. 10, 1527-1535 (1975).
- [11] C. J. Brinker, G.W. Scherer, Sol-gel science – The physics and chemistry of sol-gel science. 1990, Academic Press, Boston.
- [12] L. Kurpaska, J. Favergeon, L. Lahoche, G. Moulin, J-M. Roelandt, Materials Science Forum 696, 176-182 (2011).
- [13] L. Kurpaska, J. Favergeon, L. Lahoche, G. Moulin, M. El Marssi, J-M. Roelandt, Oxidation of Metals 79, 261-277 (2013).
- [14] L. Kurpaska, J. Favergeon, L. Lahoche, M. El Marssi, J-L. Grosseau-Poussard, G. Moulin, J-M. Roelandt Journal of Nuclear Materials 466, 460-467 (2015).
- [15] D. Fettre, S. Bouvier, J. Favergeon, L. Kurpaska, Applied Surface Science 357, 777-786 (2015).
- [16] H. J. Conrad, W. J. Seong, I. J. Pesun. J. Prosthet. Dent. 98, 389-404 (2007).
- [17] L. Kurpaska, J. Jagielski, K. Nowakowska-Langier, Nuclear Instruments and Methods in Physics B doi 10.1016/j.nimb.2016.03.030.
- [18] K. Kato, A. Tsuzuki, H. Taoda, Y. Torii, Y. Butsugan, J. Mat. Sci. 29, 5911-5915 (1994).
- [19] C. J. Brinker, G. C. Frye, A. J. Hurd, C. S. Ashley, Thin solid films, 201, 97-108 (1991).
- [20] C. Löser, C. Rüssel, Glastech. Ber. Glass Sci. Technol. 73, 270-275 (2000).
- [21] S. Karlsson, B. Jonson, C. Stålhandske, Glass Technol. Eur. J. Glass Sci. Technol. A 51 41-54 (2010).
- [22] Y. Natsume, H. Sakata, Thin Solid Films 372, 30-36 (2000).
- [23] J. F. Chang, B. Sun, D. W. Breiby, M. M. Nielsen, T. I. Solling, M. Giles, I. McCulloch, H. Sirringhaus, Chem. Mater. 16, 4772-4776 (2004).
- [24] J. Gong, J. W Guan, Z. Guan, J. Europ. Ceram. Soc. 19, 2625-2631(1999).
- [25] T. Sugimoto, T. Kawaguchi, Development of an automatic Vickers hardness testing system using image processing technology, IEEE transactions on industrial electronics 44, 696-702 (1997).
- [26] M. Reben, J. Wasylak, J. Jaglarz, Photonics Letters of Poland 2, 13-15 (2010).
- [27] B. Burtan, M. Reben, J. Cisowski, J. Wasylak, N. Nosidlak, J. Jaglarz, Acta Physica Polonica A 120, 579-581 (2011).
- [28] P. Karasinski, J. Jaglarz, M. Reben, E. Skoczek, J. Mazur, Optical Materials 33, 1989-1994 (2011).
Typ dokumentu
Bibliografia
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