Influence of Milling Time on Amorphization of Mg-Zn-Ca Powders Synthesized by Mechanical Alloying Technique

Lesz, S.; Kremzer, M.; Gołombek, K.; Nowosielski, R.

doi:10.24425/122413

Artykuł - szczegóły

Tytuł artykułu

Influence of Milling Time on Amorphization of Mg-Zn-Ca Powders Synthesized by Mechanical Alloying Technique

Autorzy

Lesz S. , Kremzer M. , Gołombek K. , Nowosielski R.

Treść / Zawartość

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DOI

10.24425/122413

Warianty tytułu

Języki publikacji

Abstrakty

Mg₆₀ Zn₃₅ Ca₅ amorphous powder alloys were synthesized by mechanical alloying (MA) technique. The results of the influence of high-energy ball-milling time on amorphization of the Mg₆₀ Zn₃₅ Ca₅ elemental blend (intended for biomedical application) were presented in the study. The amorphization process was investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM). Initial elemental powders were mechanically alloyed in a Spex 8000 high-energy ball mill at different milling times (from 3 to 24 h). Observation of the powder morphology after various stages of milling leads to the conclusion that with the increase of the milling time the size of the powder particles as well as the degree of aggregation change. The partially amorphous powders were obtained in the Mg₆₀ Zn₃₅ Ca₅ alloy after milling for 13-18h. The results indicate that this technique is a powerful process for preparing Mg₆₀ Zn₃₅ Ca₅ alloys with amorphous and nanocrystalline structure.

Słowa kluczowe

Mg-based powders transmission electron microscopy scanning electron microscopy mechanical alloying

Wydawca

Institute of Metallurgy and Materials Science of Polish Academy of Sciences
Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences

Czasopismo

Archives of Metallurgy and Materials

Rocznik

2018

Tom

Vol. 63, iss. 2

Strony

845--851

Opis fizyczny

Bibliogr. 39 poz., fot., wykr.

Twórcy

autor

Lesz S.

sabina.lesz@polsl.pl

Silesian University of Technology, Faculty of Mechanical Engineering, Institute of Engineering Materials and Biomaterials, 18a Konarskiego Str., 44-100 Gliwice, Poland

autor

Kremzer M.

Silesian University of Technology, Faculty of Mechanical Engineering, Institute of Engineering Materials and Biomaterials, 18a Konarskiego Str., 44-100 Gliwice, Poland

autor

Gołombek K.

Silesian University of Technology, Faculty of Mechanical Engineering, Institute of Engineering Materials and Biomaterials, 18a Konarskiego Str., 44-100 Gliwice, Poland

autor

Nowosielski R.

Silesian University of Technology, Faculty of Mechanical Engineering, Institute of Engineering Materials and Biomaterials, 18a Konarskiego Str., 44-100 Gliwice, Poland

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Uwagi

1. The work was supported by National Science Centre under research Project No.: 2013/09/B/ST8/02129.

2. Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).

Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-6f09b4c1-4be2-46be-aad4-16f1086b8c18