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The optimisation of chromatographic conditions for the determination of acceptor-donor properties of graphene oxide and reduced graphene oxide

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Języki publikacji
EN
Abstrakty
EN
The oxidised and reduced graphene samples (having different surface functionalities) were studied by inverse gas chromatography to characterise their acceptor-donor properties. The DN values denoting the donor number in the Gutmann scale and the AN* values denoting the acceptor number in the Riddle-Fowkes scale have been chosen in the estimation of the electron-acceptor parameter KA and electron-donor parameter KD values.
Twórcy
autor
  • Military University of Technology, Institute of Chemistry, ul. Kaliskiego 2, 00-908 Warszawa
autor
  • Military University of Technology, Institute of Chemistry, ul. Kaliskiego 2, 00-908 Warszawa
autor
  • Military University of Technology, Institute of Chemistry, ul. Kaliskiego 2, 00-908 Warszawa
autor
  • Military University of Technology, Institute of Chemistry, ul. Kaliskiego 2, 00-908 Warszawa
autor
  • Military University of Technology, Institute of Chemistry, ul. Kaliskiego 2, 00-908 Warszawa
Bibliografia
  • [1] H.P. Boehm, A. Clauss, G.O. Fischer, U. Hofmann, Dünnste Kohlenstoff-Folien, Zeitsdirift für Naturforschung 17 b, Seite 150-153, 1961 (in German).
  • [2] A.K. Geim, K.S. Novoselov, The rise of graphene, Nature Materials 6 (2007)183-191.
  • [3] S. Mikhailov, Z. Koinov, Physics and applications of graphene theory, InTech, New York, 2011.
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  • [5] A.K. Geim, Graphene prehistory, Phys. Scr. T146 (2012) 014003 (4pp).
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  • [8] A.A. Balandin, S. Ghosh, W. Bao, I. Calizo, D. Teweldebrhan, F. Miao, C.N. Lau, Superior Thermal Conductivity of Single-Layer Graphene, Nano Lett. 8, 3(2008) 902-907.
  • [9] C. Lee, X. Wei, J.W. Kysar, J. Hone, Measurement of the Elastic Properties and Intrinsic Strength of Monolayer Graphene, Science 321, 5887 (2008) 385-388.
  • [10] S. Chowdhury, R. Balasubramanian, Three-dimensional graphene-based macrostructures for sustainable energy applications and climate change mitigation, Progress in Materials Science 90 (2017) 224-275.
  • [11] L.E.F. Foà Torres, S. Roche, J.-C. Charlier, Introduction to graphene-based nanomaterials: from electronic structure to quantum transport, Cambridge University Press, New York, 2014.
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  • [14] TableCurve 2D: Automated curve fitting and equation discovery: version 5.01 for windows; user’s manual. Richmond, CA: SYSTAT, 2002.
  • [15] Ł. Farczak, Chromatograficzne badania zredukowanego i utlenionego grafenu, WAT, Warszawa, 2015.
  • [16] H. Grajek, J. Paciura-Zadrożna, Z. Witkiewcz, Chromatographic characterisation of ordered mesoporous silicas. Part I. Surface free energy of adsorption, J. Chromatogr. A 1217 (2010) 3105-3115.
  • [17] M.C. Gutiérrez, S. Osuna, I. Baráibar, Solid surface mapping by inverse gas chromatography, J. Chromatogr. A 1087, 1-2 (2005) 142-149.
  • [18] M.C. Gutierrez, J. Rubio, F. Rubio, J.L. Oteo, Inverse gas chromatography: a new approach to the estimation of specific interactions, J. Chromatogr. A 845, 1-2 (1999) 53-66.
  • [19] H. Grajek, Ł. Farczak, T. Wawer, P. Jabłoński, M. Purchała, The characteristic of the adsorption and energetic properties of the oxidised and reduced graphene, Aparatura Badawcza I Dydaktyczna, 3 (2015) 224-233.
  • [20] V. Gutmann, The donor-acceptor approach to molecular interactions, Plenum Press, New York, 1978.
  • [21] F.L. Riddle, F.M. Fowkes, Spectral shifts in acid-base chemistry. 1. van der Waals contributions to acceptor numbers, J. Am. Chem. Soc. 112, 9 (1990) 3259-3264.
  • [22] R.S. Drago, G.C. Vogel, T.E. Needham, A Four-Parameter Equation for Predicting Enthalpies of Adduct Formation, Journal of the American Chemical Society 93, 23 (1971) 6014-6026.
  • [23] G.M. Dorris, D.G. Gray, Adsorption of n-alkanes at zero surface coverage on cellulose paper and wood fibers, J. Coll. Interface Sci. 77 (1980) 353.
  • [24] U. Panzer, H.P. Schreiber, On the Evaluation of Surface Interactions by Inverse Gas Chromatography, Macromolecules 25 (1992) 3633-3637.
Uwagi
Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-6ea86618-389f-4d07-a6f4-060a98ffa3cb
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