Microwave-assisted preparation of sinter samples for chemical composition analysis by IPC-OES technique

• Autorzy: Knapik Piotr , Latacz Aleksandra , Kubecki Michał

Identyfikatory

DOI

10.32730/mswt.2023.67.5-6.2

Warianty tytułu

PL

Opracowanie metody mineralizacji mikrofalowej przygotowania roztworów próbek spiekalniczych do badań składu chemicznego techniką ICP-OES

• Języki publikacji: EN

Abstrakty

EN

The article discusses tests aimed to develop a method enabling the preparation of iron ore sinters applying microwave-assisted mineralisation and subsequently used in the ICP-OES technique-based chemical composition analysis. The tests involved the use of various mineralising mixtures, one of which was selected to prepare specimens of sinters used in the ICP-OES technique-based chemical composition analysis. The repeatability of the microwave-assisted mineralisation of sinters was investigated through the repeated mineralisation of the same sinter specimen performed under the same conditions. The test results revealed that the microwave-assisted mineralisation technique could be used routinely in ICP-OES technique-based sinter analytics. The preparation of the sinters performed using the abovenamed technique was less laborious and involved the use of small amounts of chemical reagents.

PL

Celem badań było opracowanie metody roztwarzania spieków rud żelaza z użyciem mineralizacji mikrofalowej na potrzeby analizy składu chemicznego techniką ICP-OES. Badania przeprowadzono z użyciem różnych mieszanin mineralizujących i spośród nich wybrano jedną, która posłużyła do przygotowania próbek spieków do badań składu chemicznego techniką ICP-OES. Następnie, w celu zbadania powtarzalności procesu mineralizacji mikrofalowej spieków, przeprowadzono badania wielokrotnej mineralizacji tej samej próbki spieku, w tych samych warunkach. Przeprowadzone badania wykazały, że technika mineralizacji mikrofalowej może znaleźć rutynowe zastosowanie w analityce próbek spieków techniką ICP-OES. Przygotowanie próbki spieków tą techniką było mniej pracochłonne i wymagało użycia niewielkiej ilości odczynników chemicznych.

Słowa kluczowe

EN

ICP-OES; microwave mineralization; iron ores; sinters

PL

ICP-OES; mineralizacja mikrofalowa; rudy żelaza; spieki

• Wydawca: Sieć Badawcza Łukasiewicz - Górnośląski Instytut Technologiczny
• Czasopismo: Materials Science and Welding Technologies / Technologie Materiałowe i Spawalnicze
• Rocznik: 2023
• Tom: Vol. 67, No. 5-6
• Strony: art. no. 2
• Opis fizyczny: Bibliogr. 29 poz., tab.

Twórcy

autor

Knapik Piotr

• Łukasiewicz Research Network – Upper Silesian Institute of Technology [Sieć Badawcza Łukasiewicz – Górnośląski Instytut Technologiczny, Centrum Badań Materiałów i Centrum Technologii Metalurgicznych]

• https://orcid.org/0000-0003-3894-3592

autor

Latacz Aleksandra

• Łukasiewicz Research Network – Upper Silesian Institute of Technology [Sieć Badawcza Łukasiewicz – Górnośląski Instytut Technologiczny, Centrum Badań Materiałów i Centrum Technologii Metalurgicznych]

• https://orcid.org/0009-0007-0608-9164

autor

Kubecki Michał

• Łukasiewicz Research Network – Upper Silesian Institute of Technology [Sieć Badawcza Łukasiewicz – Górnośląski Instytut Technologiczny, Centrum Badań Materiałów i Centrum Technologii Metalurgicznych]

• https://orcid.org/0000-0001-9836-802X

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