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Investigation of compositional analysis and physical properties for Ni-Cr-Nb alloys using laser-induced breakdown spectroscopy

Treść / Zawartość
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
In this work, laser-induced breakdown spectroscopy (LIBS) analysis is optimized for direct estimation of elemental composition, thermal conductivity and hardness for Ni-Cr-Nb alloys. These alloys were chosen with a variable elemental content of niobium and chromium. The influence of laser energy and shot numbers on measuring line intensity was investigated. Based on the ratio between two spectral lines, calibration curves were formed to estimate the element concentration and LIBS results were confirmed with related energy-dispersive X-ray spectroscopy (EDS) data. Hardness and thermal conductivity estimation using LIBS were done by measuring the ratio between two spectral lines, plasma excitation temperature and electron density for different samples. Semi-empirical formulas correlated hardness and thermal conductivity with plasma temperature were established.
Słowa kluczowe
Czasopismo
Rocznik
Strony
429--444
Opis fizyczny
Bibliogr. 35 poz., rys., tab.
Twórcy
  • Al-Nahrain Nanorenewable Energy Center, Al-Nahrain University, Iraq
  • Laser and Optoelectronics Department, College of Engineering, Al-Nahrain University, Iraq
Bibliografia
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  • [7] KUZUYA M., A sorting system for aluminum alloy scrap based on laser-induced breakdown spectroscopy, Science Journal of Analytical Chemistry 7(3), 2019, pp. 65–71, DOI: 10.11648/j.sjac.20190703.11.
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  • [11] GAUDIUSO R., UHLIR K., GRIESSER M., Micro-invasive depth profile analysis by laser-induced breakdown spectroscopy (LIBS): the case of mercury layers on Sasanian coins, Journal of Analytical Atomic Spectrometry 34(11), 2019, pp. 2261–2272, DOI: 10.1039/C9JA00165D.
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  • [29] WANG X., ZHANG L., FAN J., LI Y., GONG Y., DONG L., MA W., YIN W., JIA S., Parameters optimization of laser-induced breakdown spectroscopy experimental setup for the case with beam expander, Plasma Science and Technology 17(11), 2015, pp. 914–918, DOI: 10.1088/1009-0630/17/11/04.
  • [30] ABDEL-SALAM Z., ABDELHAMID M., KHALIL S.M., HARITH M.A., LIBS new application: determination of metallic alloys surface hardness, AIP Conference Proceedings 1172(1), 2009, pp. 49–52, DOI: 10.1063/1.3250114.
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Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-6c1994c7-c5ab-48c0-8f14-84b071bc4dd9
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