Identyfikatory
Warianty tytułu
Języki publikacji
Abstrakty
In this work, laser-induced breakdown spectroscopy (LIBS) analysis is optimized for direct estimation of elemental composition, thermal conductivity and hardness for Ni-Cr-Nb alloys. These alloys were chosen with a variable elemental content of niobium and chromium. The influence of laser energy and shot numbers on measuring line intensity was investigated. Based on the ratio between two spectral lines, calibration curves were formed to estimate the element concentration and LIBS results were confirmed with related energy-dispersive X-ray spectroscopy (EDS) data. Hardness and thermal conductivity estimation using LIBS were done by measuring the ratio between two spectral lines, plasma excitation temperature and electron density for different samples. Semi-empirical formulas correlated hardness and thermal conductivity with plasma temperature were established.
Słowa kluczowe
Czasopismo
Rocznik
Tom
Strony
429--444
Opis fizyczny
Bibliogr. 35 poz., rys., tab.
Twórcy
autor
- Al-Nahrain Nanorenewable Energy Center, Al-Nahrain University, Iraq
autor
- Laser and Optoelectronics Department, College of Engineering, Al-Nahrain University, Iraq
Bibliografia
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- [5] WANG S., TIAN D., XU M., LIN Q., WANG J., GUO G., YANG G., DUAN Y., Elemental analysis of cemented carbides by calibration-free portable laser-induced breakdown spectroscopy, Instrumentation Science & Technology 46(3), 2018, pp. 277–291, DOI: 10.1080/10739149.2017.1380663.
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- [7] KUZUYA M., A sorting system for aluminum alloy scrap based on laser-induced breakdown spectroscopy, Science Journal of Analytical Chemistry 7(3), 2019, pp. 65–71, DOI: 10.11648/j.sjac.20190703.11.
- [8] VARELA J.A., AMADO J.M., TOBAR M.J., MATEO M.P., YAÑEZ A., NICOLAS G., Characterization of hard coatings produced by laser cladding using laser-induced breakdown spectroscopy technique, Applied Surface Science 336, 2015, pp. 396–400, DOI: 10.1016/j.apsusc.2015.01.037.
- [9] KASHIWAKURA S., WAGATSUMA K., Characteristics of the calibration curves of copper for the rapid sorting of steel scrap by means of laser-induced breakdown spectroscopy under ambient air atmospheres, Analytical Sciences 29(12), 2013, pp. 1159–1164, DOI: 10.2116/analsci.29.1159.
- [10] ARARAT-IBARGUEN C., CORVALÁN C., DI LALLA N., IRIBARREN M., PÉREZ R., VICENTE E., Application of the LIBS technique to the study of fast impurities diffusion in Zr based alloys, Procedia Materials Science 8, 2015, pp. 1004–1013, DOI: 10.1016/j.mspro.2015.04.162. Investigation of compositional analysis and physical properties... 443
- [11] GAUDIUSO R., UHLIR K., GRIESSER M., Micro-invasive depth profile analysis by laser-induced breakdown spectroscopy (LIBS): the case of mercury layers on Sasanian coins, Journal of Analytical Atomic Spectrometry 34(11), 2019, pp. 2261–2272, DOI: 10.1039/C9JA00165D.
- [12] LI J., LU J., DAI Y., DONG M., ZHONG W., YAO S., Correlation between aging grade of T91 steel and spectral characteristics of the laser-induced plasma, Applied Surface Science 346, 2015, pp. 302–310, DOI: 10.1016/j.apsusc.2015.03.186.
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- [17] LABUTIN T.A., POPOV A.M., LEDNEV V.N., ZOROV N.B., Correlation between properties of a solid sample and laser-induced plasma parameters, Spectrochimica Acta Part B: Atomic Spectroscopy 64(10), 2009, pp. 938–949, DOI: 10.1016/j.sab.2009.07.033.
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- [20] HAMAD T.K., JASIM A.S., SALLOOM H.T., Characterizing laser-induced plasma generated from MgO/PVA solid targets, Optics and Spectroscopy 127(1), 2019, pp. 153–158, DOI: 10.1134/S0030400X19070099.
- [21] FIKRY M., TAWFIK W., OMAR M.M., Investigation on the effects of laser parameters on the plasma profile of copper using picosecond laser induced plasma spectroscopy, Optical and Quantum Electronics 52(5), 2020, article 249, DOI: 10.1007/s11082-020-02381-x.
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- [29] WANG X., ZHANG L., FAN J., LI Y., GONG Y., DONG L., MA W., YIN W., JIA S., Parameters optimization of laser-induced breakdown spectroscopy experimental setup for the case with beam expander, Plasma Science and Technology 17(11), 2015, pp. 914–918, DOI: 10.1088/1009-0630/17/11/04.
- [30] ABDEL-SALAM Z., ABDELHAMID M., KHALIL S.M., HARITH M.A., LIBS new application: determination of metallic alloys surface hardness, AIP Conference Proceedings 1172(1), 2009, pp. 49–52, DOI: 10.1063/1.3250114.
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- [32] KHALIL O.M., MINGAREEV I., BONHOFF T., EL-SHERIF A.F., RICHARDSON M.C., HARITH M.A., Studying the effect of zeolite inclusion in aluminum alloy on measurement of its surface hardness using laser-induced breakdown spectroscopy technique, Optical Engineering 53(1), 2014, article 014106, DOI: 10.1117/1.OE.53.1.014106.
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- [34] GUO K., CHEN A., XU W., ZHANG D., JIN M., Effect of sample temperature on time-resolved laser-induced breakdown spectroscopy, AIP Advances 9(6), 2019, article 065214, DOI: 10.1063/1.5097301.
- [35] COWPE J.S., MOOREHEAD R.D., MOSER D., ASTIN J.S., KARTHIKEYAN S., KILCOYNE S.H., CROFTS G., PILKINGTON R.D., Hardness determination of bio-ceramics using laser-induced breakdown spectroscopy, Spectrochimica Acta Part B: Atomic Spectroscopy 66(3–4), 2011, pp. 290–294, DOI: 10.1016/j.sab.2011.03.007.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-6c1994c7-c5ab-48c0-8f14-84b071bc4dd9