Effect of Reaction Time and Heat Treatment in the Production of Hydroxyapatite by Hydrothermal Synthesis

• Autorzy: Kati Nida , Ozan Sermin , Yildiz Tülay , Arslan Mehmet

Identyfikatory

DOI

10.24425/amm.2022.141070

• Języki publikacji: EN

Abstrakty

EN

In the present work, Hydroxyapatite synthesis was carried out using hydrothermal method with calcium nitrate tetrahydrate (Ca(NO₃)₂.4H₂O) and fosfor pentaoksit (P₂O₅) as precursors. For the hydrothermal method, constant reaction temperature (180°C) and different reaction times (6 hours, 12 hours, 18 hours and 24 hours) were determined. The samples produced were divided into two groups. Four samples were not heat treatment; four samples were heat treatment at 700°C for 1 hour. The obtained products were characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) techniques, X-ray diffraction (XRD) and UV-Vis spectrometer. SEM photos showed that the Hydroxyapatite powders produced are in the form of the agglomerate. According to EDS results, Hydroxyapatite samples are of high purity. XRD’s findings confirm that the diffraction peaks correspond to the pure phase of Hydroxyapatite. A general decrease was observed in the energy band gap of the samples with increasing hydrothermal reaction time.

Słowa kluczowe

EN

Hydroxyapatite; hydrothermal; heat treatment; reaction time; XRD/SEM; optical properties

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2022
• Tom: Vol. 67, iss. 4
• Strony: 1427--1434
• Opis fizyczny: Bibliogr. 28 poz., fot., rys., tab., wzory

Twórcy

autor

Kati Nida

• Fırat Unıversity, Faculty of Technology, Metallurgical and Materials Engineering Department, 23200, Elazığ, Turkiye

• https://orcid.org/0000-0001-7953-1258

autor

Ozan Sermin

• Fırat Unıversity, Faculty of Technology, Metallurgical and Materials Engineering Department, 23200, Elazığ, Turkiye

• https://orcid.org/0000-0002-8557-7428

autor

Yildiz Tülay

• Fırat Unıversity, Faculty of Technology, Metallurgical and Materials Engineering Department, 23200, Elazığ, Turkiye

• https://orcid.org/0000-0001-9665-7733

autor

Arslan Mehmet

• Fırat Unıversity, Faculty of Technology, Metallurgical and Materials Engineering Department, 23200, Elazığ, Turkiye

• https://orcid.org/0000-0001-6237-1999

Bibliografia

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Uwagi

1. This study was supported by the Fırat University Scientific Research Projects Unit (Project No: TEKF.18.25).

2. Opracowanie rekordu ze środków MEiN, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2022-2023).