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Models of damage mechanism of glidcop Cu-Al2O3 micro and nanomaterials

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose:of this paper was to analyze the fracture mechanism before and after ECAP in the Glidcop AL-60 grade (with 1.1 wt. % of Al2O3) system and to propose damage and/or fracture mechanisms models by means of the method “in situ tensile test in SEM”. Design/methodology/approach: The method of “in-situ tensile testing in SEM” was used for investigations of fracture mechanisms because it enables to observe and document deformation processes directly, thank to which the initiation and development of plastic deformation and fracture can be reliably described. Analyses of microstructure and fracture surfaces were carried out by means of the scanning electrone microscope JEM 100 C. Findings: The deformation and fracture mechanisms of Glidcop AL-60 grade with 1.1 wt. % of Al2O3 phase (1.62 vol. % of Al2O3) were analyzed before and after ECAP (Equal Channel Angular Pressing). Before ECAP it was shown that the deformation process causes increasing of pores and formation of cracks. Decohesion of small Al2O3 particles and clusters occurs and the final fracture path is influenced by coalescence of cracks originated in such. The principal crack propagates towards the sample exterior surface. After ECAP initial cracks were formed in the middle of the specimen first of all in the triple junctions of nanograins and together with decohesion of Al2O3 particles and clusters at small strains lead to the failure. Research limitations/implications: To develop more complex knowledge about the objective material further studies are necessary to focus also on the other factors which besides the secondary phase amount can influence the failure mechanism, e.g. strain rate, temperature and others. Complex analysis allows better understanding of material behavior at different conditions and possibilities of application of products from these materials will be thereby improved. Practical implications: This article completes knowledge about damage/fracture mechanisms and processes of the material with 1.1 wt. % of Al2O3 phase. Some materials with the different volume fraction of a secondary phase have been studied. This concrete one with 1.1% clarifies the fracture process of Glidcop AL-60 material not only after mechanical alloying process but also after ECAP treatment. An effect of the ECAP process on the final material was crucial because not only microstructure but also failure mechanism have been changed. Originality/value: Based on the experimental observations original models of damage and/or fracture mechanisms were proposed.
Rocznik
Strony
79--85
Opis fizyczny
Bibliogr. 21 poz., rys.
Twórcy
autor
  • Institute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 043 53 Košice, Slovak Republic
  • Institute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 043 53 Košice, Slovak Republic
  • Institute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 043 53 Košice, Slovak Republic
  • Department of Materials Science, Faculty of Metallurgy, Technical University in Košice, Letná 9, 042 00 Košice, Slovak Republic
Bibliografia
  • [1] GLIDCOP (SCM Product Literature, 1994)", SCM Metal Products. Retrieved 2012-02-12. http://www.aps.anl.gov/APS_Engineering_Support_Division/Mechanical_Operations_and_Maintenance/Miscellaneous/tech_info/Glidcop/SCM_Glidcop_product_info.pdf ,
  • [2] M. Besterci, K. Sülleiová, T. Kvakaj, Fracture micromechanisms of Cu nanomaterials prepared by ECAP, Kovove materialy 46 (2008) 309-311.
  • [3] M. Besterci, J. Ivan, Mechanizmus porušovania disperzne spevnenej sústavy Cu- Al2O3, Kovove Materialy 35 (1997) 278-284.
  • [4] M. Besterci, J. Ivan, L. Ková, T. Weissgaerber, C. Sauer, Strain and fracture mechanism of Cu-TiC, Materials Letters 38 (1999) 270-274.
  • [5] M. Besterci, J. Ivan, L. Ková, Influence of Al2O3 particles volume fraction on fracture mechanism in the Cu–Al2O3 system, Materials Letters 46 (2000) 181-184.
  • [6] Z. Ma, H. Zhao, H. Huang, L Zhang, K. Wang, X. Zhou, Experimental Techniques 2012 doi: 10.1111/j.1747-1567.2012.00868.x.
  • [7] L.L. Mishnaevsky, N. Lippmann, S. Schmauder, P. Gumbsch, In-situ observation of damage evolution and fracture in AlSi7Mg0.3 cast alloys, Engine Fracture Mechanics 63 (1999) 395-411.
  • [8] M. Besterci, J. Ivan, Failure mechanism of dispersion strengthened Al-Al4C3 systems, Journal of Materials Science Letters15 (1996) 2071-2074.
  • [9] W. Zhou, W. Hu, D. Zhang, Metal-matrix interpenetrating phase composite and its in-situ fracture observation, Materials Letters 40 (1999) 156-160.
  • [10] M. Besterci, J. Ivan, The Mechanism of the Failure of the Dispersion-strengthened Cu-Al2O3 System, Journal of Materials Science Letters 17 (1998) 773-776.
  • [11] X.J. Wang, K. Wu, W.X. Huang, H.F. Zhang, D.L. Peng, Study on fracture behavior of particulate reinforced magnesium matrix composite using in-situ SEM, Composites Science and Technology 67 (2007) 2253-2260.
  • [12] M.J. Vratnica, In-situ observation of the fracture process in Al–Zn–Mg–Cu alloys, International Journal of Materials Research 103/5 (2012) 624–632.
  • [13] M.Y. Zheng, W.C. Zhang, K. Wu, C.K. Yao, The deformation and fracture behavior of SiCw/AZ91 magnesium matrix composite during in-situ TEM straining, Materials Science 38 (2003) 2647-2654.
  • [14] W.G. Zhang, Y. Zhang, G.J. Hao, J.P. Lin, A comparison of the nucleation and growth of shear bands in Ti and Zr-based bulk metallic glasses by in-situ tensile tests, Materials Science and Engineering A 516 (2009) 148-153.
  • [15] W. Luoyi, Y. Zhong, H. En, The tensile properties at 448 K and the fracture behaviors under in situ transmission electron microscope strain for the Mg–6.0Gd–1.2Zn–0.15Y alloy, Materials and Design 40 (2012) 199-204.
  • [16] Z. Cvijovi, M. Vratnica, I. Cvijovi-Alagi, The influences of multiscale-sized second-phase particles on fracture behaviour of overaged 7000 alloys, Procedia Engineering 1 (2009) 35-38.
  • [17] G.G. Sozhamannan, P.S. Balasivanandha, R. Paskaramoorthy, Failures analysis of particle reinforced metal matrix composites by microstructure based models, Materials and Design 31 (2010) 3785-3790.
  • [18] A, Mocelin, F. Fougerest, P. F. J. Gobin, A study of damage under tensile loading in a new Al-Si-Fe alloy processed by the Osprey route, Materials Science 28 (1993) 4855-4861.
  • [19] R. Velísek, J. Ivan, Mechanism of “in-situ deformation in SEM” Al-Si system, Metallic Materals 32 (1994) 531-539.
  • [20] T.W. Clyne, P.J. Withers, An Introduction to Metal Matrix Composites. Cambridge University Press, 1993.
  • [21] P.B. Prangnell, S.J. Barnes, S.M. Roberts, P.J. Withers, The effect of particle distribution on damage formation in particulate reinforced metal matrix composites deformed in compression, Materials Science and Engineering A 220 (1996) 41-56.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-6be94434-9e6a-4347-9f8e-7a1928f0370d
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