Multiresidue determination of antibiotics in preserved eggs using a QuEChERS-based procedure by ultrahigh-performance liquid chromatography tandem mass spectrometry

• Autorzy: Li Y. , Chen Z. , Wen S. , Hou X. , Zhang R. , Ma M.

Identyfikatory

DOI

10.1556/1326.2017.29211

• Języki publikacji: EN

Abstrakty

EN

A modified QuEChERS (quick, easy, cheap, effective, rugged, and safe) method and ultrahigh-performance liquid chromatography coupled to tandem mass spectrometry (UHPLC–MS/MS) were optimized and validated for 16 antibiotics belonging to three families (macrolides, quinolones, and sulfonamides) that were found in preserved eggs. Samples were extracted in 4 mL water and 10 mL acetonitrile with 1% acetic acid and subjected to a cleanup procedure using dispersive solid-phase extraction with C18 and primary secondary amine sorbents, prior to detection by UHPLC–MS/MS. Matrix-matched calibration was used for quantification to reduce the matrix effect with limits of quantification in the range of 0.3–3.0 μg/kg. Validation of the method was conducted by recovery and precision experiments. Recoveries of the spiked samples ranged from 73.8% to 127.4%, and the intra- and inter-day relative standard deviations were lower than 21.2% and 22.3%, respectively. This method was successfully applied to the analysis of antibiotics in preserved egg samples.

Słowa kluczowe

EN

QuEChERS; UHPLC-MS/MS; antibiotics; macrolides; quinolones; sulfonamides

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2018
• Tom: Vol. 30, no. 1
• Strony: 9--16
• Opis fizyczny: Bibliogr. 33 poz., rys., tab.

Twórcy

autor

Li Y.

• School of Environment, Beijing Normal University, State Key Laboratory of Water Environment Simulation/Key Laboratory of Water and Sediment Sciences of Ministry of Education, Beijing 100875, China
• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Center for Disease Control and Prevention Wuhan 430079, China

autor

Chen Z.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Center for Disease Control and Prevention Wuhan 430079, China

autor

Wen S.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Center for Disease Control and Prevention Wuhan 430079, China

autor

Hou X.

• Department of Biotechnology, Delft University of Technology, Delft 2624BC, Netherlands

autor

Zhang R.

• Hubei Provincial Key Laboratory for Applied Toxicology, Hubei Provincial Center for Disease Control and Prevention Wuhan 430079, China

autor

Ma M.

• School of Environment, Beijing Normal University, State Key Laboratory of Water Environment Simulation/Key Laboratory of Water and Sediment Sciences of Ministry of Education, Beijing 100875, China

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).